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MB Sample ID: SA174917
Local Sample ID: | 20210513_ColmIM1_1.cdf |
Subject ID: | SU001956 |
Subject Type: | Plant |
Subject Species: | Saccharum spp |
Species Group: | Plants |
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Combined analysis:
Analysis ID | AN003039 |
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Analysis type | MS |
Chromatography type | GC |
Chromatography system | Agilent 7890A |
Column | Agilent DB5 (20m x 0.18 mm i.d. x 0.18 μm) |
MS Type | EI |
MS instrument type | GC x GC-TOF |
MS instrument name | Leco Pegasus 4D GCxGC TOF |
Ion Mode | UNSPECIFIED |
Units | relative intensity |
Chromatography:
Chromatography ID: | CH002254 |
Chromatography Summary: | One microliter of each derivatized sample was injected splitless into a gas chromatograph 7890A (Agilent Technologies, Santa Clara, USA) coupled with a Comb-xt Autosampler (Leap Technologies, Carrboro, USA). A 20m x 0.18 mm i.d. x 0.18 μm film thickness, DB5 GC capillary column (Agilent Technologies) was used as the primary column and the secondary GC columns was a 0.69 m x 0.1 mm i.d. x 0.1 μm film thickness (Rxi-17 Restek, Bellefonte, USA). The injector temperature was 280°C, the septum purge flow rate was 20 ml min-1 and the purge was turned on after 60 s. The gas helium flow rate through the column was 1 ml min-1, the column temperature was held at 80°C for 2 min, then increased by 15°C min-1 to 305°C, and held there for 10 min. |
Instrument Name: | Agilent 7890A |
Column Name: | Agilent DB5 (20m x 0.18 mm i.d. x 0.18 μm) |
Chromatography Type: | GC |