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MB Sample ID: SA178409

Local Sample ID:Bov2_3
Subject ID:SU002005
Subject Type:Fungi
Subject Species:Beauveria bassiana
Genotype Strain:GenBank: KU751847; KU751848

Select appropriate tab below to view additional metadata details:


Combined analysis:

Analysis ID AN003133 AN003134 AN003135
Analysis type MS MS MS
Chromatography type GC Reversed phase Reversed phase
Chromatography system Agilent 7890A Waters Acquity UPLC Waters Acquity UPLC
Column Agilent DB-5 (20m x 0.18mm, 0.18um); Restek RX-T 17 (0.9m x 0.10mm, 0.10um) Waters Acquity UPLC HSS (100 x 2.1mm, 1.7um) Waters Acquity UPLC HSS (100 x 2.1mm, 1.7um)
MS Type EI ESI ESI
MS instrument type GC x GC-TOF QTOF QTOF
MS instrument name Leco Pegasus 4D GCxGC TOF Waters Ultima QTOF Waters Ultima QTOF
Ion Mode UNSPECIFIED POSITIVE NEGATIVE
Units Relative intensity Relative intensity

Chromatography:

Chromatography ID:CH002315
Chromatography Summary:(.cdf)
Methods Filename:LCMSMS
Instrument Name:Agilent 7890A
Column Name:Agilent DB-5 (20m x 0.18mm, 0.18um); Restek RX-T 17 (0.9m x 0.10mm, 0.10um)
Column Temperature:70 - 320 ºC
Flow Rate:1 mL.min-1
Injection Temperature:280 ºC
Sample Injection:1 uL
Oven Temperature:70°C for 2 min, increasing by 15°C·min-1 until it reached 320°C and then held at this temperature for 4 min.
Chromatography Type:GC
  
Chromatography ID:CH002316
Chromatography Summary:Positive Mode (.raw)
Methods Filename:LCMSMS
Instrument Name:Waters Acquity UPLC
Column Name:Waters Acquity UPLC HSS (100 x 2.1mm, 1.7um)
Column Temperature:35 ºC
Flow Gradient:95% solvent A and 5% B. The gradient increased linearly to 75% A and 25% B over the next 6 min. The polarity was reversed to 25% A and 75% B for 6 min, and finally 5% A and 95% B for 1 min
Flow Rate:0.5 mL·min-1
Solvent A:Water; formic acid
Solvent B:100% acetonitrile; formic acid.
Chromatography Type:Reversed phase
  
Chromatography ID:CH002317
Chromatography Summary:Negative mode (.raw)
Methods Filename:LCMSMS
Instrument Name:Waters Acquity UPLC
Column Name:Waters Acquity UPLC HSS (100 x 2.1mm, 1.7um)
Column Temperature:35 ºC
Flow Gradient:95% solvent A and 5% B. The gradient increased linearly to 75% A and 25% B over the next 6 min. The polarity was reversed to 25% A and 75% B for 6 min, and finally 5% A and 95% B for 1 min
Flow Rate:0.5 mL·min-1
Solvent A:Water; formic acid
Solvent B:100% acetonitrile; formic acid.
Chromatography Type:Reversed phase
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