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MB Sample ID: SA385750
| Local Sample ID: | HSA-000019594 |
| Subject ID: | SU003630 |
| Subject Type: | Mammal |
| Subject Species: | Mus musculus |
| Taxonomy ID: | 10090 |
| Age Or Age Range: | 15 mo |
| Gender: | Male |
| Species Group: | Mammals |
Select appropriate tab below to view additional metadata details:
Combined analysis:
| Analysis ID | AN005746 | AN005747 | AN005748 | AN005749 |
|---|---|---|---|---|
| Analysis type | MS | MS | MS | MS |
| Chromatography type | Reversed phase | Reversed phase | HILIC | Ion exchange |
| Chromatography system | Agilent 1290 Infinity II | Agilent 1290 Infinity II | Agilent 1290 Infinity II | Agilent 1290 Infinity II |
| Column | Waters ACQUITY UPLC BEH C18 (100 x 2.1mm,1.7um) | Waters ACQUITY UPLC BEH C18 (100 x 2.1mm,1.7um) | Waters ACQUITY UPLC BEH Amide (150 x 2.1mm,1.7um) | Imtakt Intrada Organic Acid (150 x 2mm, 3um) ) |
| MS Type | ESI | ESI | ESI | ESI |
| MS instrument type | Triple quadrupole | Triple quadrupole | Triple quadrupole | Triple quadrupole |
| MS instrument name | ABI Sciex 6500+ Qtrap | ABI Sciex 6500+ Qtrap | ABI Sciex 6500+ Qtrap | ABI Sciex 6500+ Qtrap |
| Ion Mode | POSITIVE | POSITIVE | POSITIVE | NEGATIVE |
| Units | log2(area) | log2(area) | log2(area) | log2(area) |
MS:
| MS ID: | MS005469 |
| Analysis ID: | AN005746 |
| Instrument Name: | ABI Sciex 6500+ Qtrap |
| Instrument Type: | Triple quadrupole |
| MS Type: | ESI |
| MS Comments: | Curtain gas at 40 psi (positive mode); collision gas was set at medium; ion spray voltage at 5500 V (positive mode); temperature at 250°C (positive mode); ion source Gas 1 at 55 psi; ion source Gas 2 at 60 psi; entrance potential at 10 V (positive mode); and collision cell exit potential at 12.5 V (positive mode). Quantification was performed using MultiQuant 3.02 (Sciex). |
| Ion Mode: | POSITIVE |
| MS ID: | MS005470 |
| Analysis ID: | AN005747 |
| Instrument Name: | ABI Sciex 6500+ Qtrap |
| Instrument Type: | Triple quadrupole |
| MS Type: | ESI |
| MS Comments: | Curtain gas at 40 psi (positive mode); collision gas was set at medium; ion spray voltage at 5500 V (positive mode); temperature at 250°C (positive mode); ion source Gas 1 at 55 psi; ion source Gas 2 at 60 psi; entrance potential at 10 V (positive mode); and collision cell exit potential at 12.5 V (positive mode). Quantification was performed using MultiQuant 3.02 (Sciex). Increased MRM dwell time for specific list of TG transitions. |
| Ion Mode: | POSITIVE |
| MS ID: | MS005471 |
| Analysis ID: | AN005748 |
| Instrument Name: | ABI Sciex 6500+ Qtrap |
| Instrument Type: | Triple quadrupole |
| MS Type: | ESI |
| MS Comments: | curtain gas at 30 psi; collision gas was set at medium; ion spray voltage at 5500 V; temperature at 600°C; ion source Gas 1 at 50 psi; ion source Gas 2 at 60 psi; entrance potential at 10 V; and collision cell exit potential at 12.5 V. |
| Ion Mode: | POSITIVE |
| MS ID: | MS005472 |
| Analysis ID: | AN005749 |
| Instrument Name: | ABI Sciex 6500+ Qtrap |
| Instrument Type: | Triple quadrupole |
| MS Type: | ESI |
| MS Comments: | curtain gas at 40 V; collision gas was set at medium; ion spray voltage at -4500 V; temperature at 600°C; ion source Gas 1 at 50 psi; ion source Gas 2 at 60 psi; entrance potential at -10 V; and collision cell exit potential at -15.0 V. |
| Ion Mode: | NEGATIVE |
