Summary of Study ST000545
This data is available at the NIH Common Fund's National Metabolomics Data Repository (NMDR) website, the Metabolomics Workbench, https://www.metabolomicsworkbench.org, where it has been assigned Project ID PR000399. The data can be accessed directly via it's Project DOI: 10.21228/M8GG6B This work is supported by NIH grant, U2C- DK119886.
See: https://www.metabolomicsworkbench.org/about/howtocite.php
| Study ID | ST000545 |
| Study Title | CHEAR Plasma Reference Material Proficiency Test Biocrates |
| Study Type | Metabolomics |
| Study Summary | CHEAR Reference Material Plasma was provided by Emory University. The material was prepared and analyzed by way of LC-MS and Biocrates workflow employed by the Eastern Regional Metabolomics Resource Core (protocols available in metabolomics workbench). Six samples were injected of the sample reference material prepared in replicate. |
| Institute | RTI International |
| Department | Discovery-Sciences-Technology (DST) |
| Laboratory | RTI CHEAR Analytical Hub - Untargeted Analysis Resource Core |
| Last Name | Fennell |
| First Name | Timothy |
| Address | 3040 E Cornwallis Road, Research Triangle Park, NC 27709 |
| fennell@rti.org | |
| Phone | 919-485-2781 |
| Submit Date | 2016-12-29 |
| Raw Data Available | Yes |
| Raw Data File Type(s) | wiff |
| Chear Study | Yes |
| Analysis Type Detail | LC-MS |
| Release Date | 2024-12-31 |
| Release Version | 1 |
Select appropriate tab below to view additional metadata details:
Combined analysis:
| Analysis ID | AN000829 | AN000830 | AN000831 |
|---|---|---|---|
| Analysis type | MS | MS | MS |
| Chromatography type | Reversed phase | Flow induction analysis | Flow induction analysis |
| Chromatography system | Agilent 1100 | Agilent 1100 | Agilent 1100 |
| Column | Agilent Eclipse XDB-C18 (100 x 3.0mm,3.5um) | No column | No column |
| MS Type | ESI | ESI | ESI |
| MS instrument type | Triple quadrupole | Triple quadrupole | Triple quadrupole |
| MS instrument name | ABI Sciex 4000 QTrap | ABI Sciex 4000 QTrap | ABI Sciex 4000 QTrap |
| Ion Mode | POSITIVE | POSITIVE | NEGATIVE |
| Units | um | um | um |
Chromatography:
| Chromatography ID: | CH000593 |
| Instrument Name: | Agilent 1100 |
| Column Name: | Agilent Eclipse XDB-C18 (100 x 3.0mm,3.5um) |
| Column Pressure: | 30-120 bar |
| Column Temperature: | 50 degrees C |
| Flow Rate: | 0.5mL/min |
| Sample Injection: | 10uL |
| Solvent A: | 100% water; 0.2% formic acid |
| Solvent B: | 100% acetonitrile; 0.2% formic acid |
| Analytical Time: | 9.5 minutes |
| Target Sample Temperature: | 10 degrees C |
| Sample Loop Size: | 100uL |
| Chromatography Type: | Reversed phase |
| Chromatography ID: | CH000594 |
| Instrument Name: | Agilent 1100 |
| Column Name: | No column |
| Column Pressure: | 4-50 bar |
| Sample Injection: | 20uL |
| Solvent B: | 100% methanol |
| Analytical Time: | 3.0 minutes |
| Target Sample Temperature: | 10 degrees C |
| Sample Loop Size: | 100uL |
| Chromatography Type: | Flow induction analysis |
