Summary of Study ST001251
This data is available at the NIH Common Fund's National Metabolomics Data Repository (NMDR) website, the Metabolomics Workbench, https://www.metabolomicsworkbench.org, where it has been assigned Project ID PR000838. The data can be accessed directly via it's Project DOI: 10.21228/M8C671 This work is supported by NIH grant, U2C- DK119886.
See: https://www.metabolomicsworkbench.org/about/howtocite.php
| Study ID | ST001251 |
| Study Title | The effects of a training program encompassing cold exposure, breathing exercises, and meditation on plasma metabomics during experimental human endotoxemia |
| Study Type | Experimental human endotoxemia study |
| Study Summary | Study to investigate the effects of a training program encompassing cold exposure, breathing exercises, and meditation on plasma metabolomic during experimental human endotoxemia. |
| Institute | Radboud University Medical Centre |
| Department | Intensive Care Medicine |
| Laboratory | Metabolomic Discoveries (acquired by Metabolon in September 2017) |
| Last Name | Kox |
| First Name | Matthijs |
| Address | Intensive Care Medicine (710), Geert Grooteplein 10 |
| matthijs.kox@radboudumc.nl | |
| Phone | 243653881 |
| Submit Date | 2019-09-16 |
| Num Groups | 2 |
| Total Subjects | 24 |
| Num Males | 24 |
| Analysis Type Detail | LC-MS |
| Release Date | 2019-10-04 |
| Release Version | 1 |
Select appropriate tab below to view additional metadata details:
Combined analysis:
| Analysis ID | AN002077 |
|---|---|
| Analysis type | MS |
| Chromatography type | Reversed phase |
| Chromatography system | Agilent 1290 |
| Column | Discovery HS F5-3 (15cm x 2.1 mm,3um) Supelco,Sigma Aldrich) |
| MS Type | ESI |
| MS instrument type | QTOF |
| MS instrument name | Agilent 6540 QTOF |
| Ion Mode | UNSPECIFIED |
| Units | relative abundance |
Chromatography:
| Chromatography ID: | CH001514 |
| Instrument Name: | Agilent 1290 |
| Column Name: | Discovery HS F5-3 (15cm x 2.1 mm,3um) Supelco,Sigma Aldrich) |
| Flow Gradient: | 5% B from 0-0.1min to 35% B at 1.5 min, to 95% B at 2.05 min which was kept constant until 3.2 min, to 5% B at 3.21 min and washing until 4.3 min with 5% B. |
| Flow Rate: | The flow rate was kept constant at 700 µL/min from 0 min to 2.2 min, and increased up to 900 µL/min from 2.2 min to 2.5 min, after which flow rate was kept constant until 3.2 min.The flow rate was decreased from 900 µL/min to 800 µL/min from 3.2 min to 3.1 min and kept constant until 3.7 min, when flow rate was changed to 700 µL/min. |
| Injection Temperature: | 40 °C |
| Solvent A: | 95% water/5% acetonitrile; 0.1% formic acid; 10 mM ammonium formate |
| Solvent B: | 95% acetonitrile/5% water; 0.1% formic acid; 10 mM ammonium formate |
| Chromatography Type: | Reversed phase |
