Summary of Study ST003198

This data is available at the NIH Common Fund's National Metabolomics Data Repository (NMDR) website, the Metabolomics Workbench, https://www.metabolomicsworkbench.org, where it has been assigned Project ID PR001988. The data can be accessed directly via it's Project DOI: 10.21228/M8RJ07 This work is supported by NIH grant, U2C- DK119886.

See: https://www.metabolomicsworkbench.org/about/howtocite.php

This study contains a large results data set and is not available in the mwTab file. It is only available for download via FTP as data file(s) here.

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Study IDST003198
Study TitleUQ/RQ panel on human tissue
Study SummaryThe extraction of nonpolar metabolites from the tissues of human for analysis by LCMS to measure levels of Ubiquinone and Rhodoquinone.
Institute
UMass Chan Medical School
DepartmentProgram in Molecular Medicine
LaboratorySpinelli Lab
Last NameJerome
First NameMadison
Address55 N Lake Ave, Worcester, MA 01655
Emailmadison.jerome@umassmed.edu
Phone(508) 856-8989 ext. 68148
Submit Date2024-05-01
Raw Data AvailableYes
Raw Data File Type(s)raw(Thermo)
Analysis Type DetailLC-MS
Release Date2025-02-04
Release Version1
Madison Jerome Madison Jerome
https://dx.doi.org/10.21228/M8RJ07
ftp://www.metabolomicsworkbench.org/Studies/ application/zip

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Combined analysis:

Analysis ID AN005248
Analysis type MS
Chromatography type Reversed phase
Chromatography system Thermo Vanquish
Column Phenomenex Luna PFP(2) (100 x 2mm,3µm)
MS Type ESI
MS instrument type Orbitrap
MS instrument name Thermo Q Exactive Plus Orbitrap
Ion Mode POSITIVE
Units peak area

Chromatography:

Chromatography ID:CH003973
Instrument Name:Thermo Vanquish
Column Name:Phenomenex Luna PFP(2) (100 x 2mm,3µm)
Column Temperature:25
Flow Gradient:0 - 3 min, 30% A; 3 - 3.25 min, 30% - 2% A; 3.25 - 5min, 2% A; 5 - 6min, 2% - 1% A; 6 - 8.75min, 1% A; 8.75 - 9min, 1% - 30% A; 9 - 10min, 30% A
Flow Rate:0.5mL/min
Solvent A:100% water; 0.1% formic acid
Solvent B:100% acetonitrile; 0.1% formic acid
Chromatography Type:Reversed phase
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