Summary of Study ST001789
This data is available at the NIH Common Fund's National Metabolomics Data Repository (NMDR) website, the Metabolomics Workbench, https://www.metabolomicsworkbench.org, where it has been assigned Project ID PR001133. The data can be accessed directly via it's Project DOI: 10.21228/M87X24 This work is supported by NIH grant, U2C- DK119886.
See: https://www.metabolomicsworkbench.org/about/howtocite.php
| Study ID | ST001789 |
| Study Title | Acute metabolomic changes of plasma in response to endurance exercise |
| Study Summary | This study compared the metabolomic differences in plasma of young adult volunteers between before (Pre), immediately after the run (Time 0) and 60 minutes after the 90-min run (Time 60). |
| Institute | University of California, San Diego |
| Department | Department of Medicine |
| Laboratory | The Naviaux Lab |
| Last Name | Naviaux |
| First Name | Robert |
| Address | 214 Dickinson St., Room C-107 |
| rnaviaux@health.ucsd.edu | |
| Phone | 619-543-2904 |
| Submit Date | 2021-04-21 |
| Num Groups | 3 |
| Total Subjects | 19 |
| Num Males | 13 |
| Num Females | 6 |
| Analysis Type Detail | LC-MS |
| Release Date | 2022-01-06 |
| Release Version | 1 |
Select appropriate tab below to view additional metadata details:
Combined analysis:
| Analysis ID | AN002901 | AN002902 |
|---|---|---|
| Analysis type | MS | MS |
| Chromatography type | HILIC | Reversed phase |
| Chromatography system | Shimadzu 20AD | Shimadzu 20AD |
| Column | Shodex NH2P-40 2E (250 x 2mm,4um) | Raptor Biphenyl (150 × 2.1 mm,2.7um) |
| MS Type | ESI | ESI |
| MS instrument type | Triple quadrupole | Triple quadrupole |
| MS instrument name | ABI Sciex 5500 QTrap | ABI Sciex 5500 QTrap |
| Ion Mode | UNSPECIFIED | UNSPECIFIED |
| Units | peak area | peak area |
MS:
| MS ID: | MS002693 |
| Analysis ID: | AN002901 |
| Instrument Name: | ABI Sciex 5500 QTrap |
| Instrument Type: | Triple quadrupole |
| MS Type: | ESI |
| MS Comments: | The MS/MS detection was performed using electrospray ionization (ESI) and advanced scheduled multiple reaction monitoring (MRM) with dynamic windowing and fast polarity switch. The ESI source conditions were set as follows: electrospray voltage of -4500 V for negative mode and 5500 V for positive mode, source temperature of 500 °C, curtain gas of 30, ion source gas 1, and gas 2 of 35 psi, respectively.Peaks were manually inspected and integrated using Multiquant 3.0.2. The peak area was exported to excel for further analysis. |
| Ion Mode: | UNSPECIFIED |
| Collision Energy: | Compound-dependent |
| Ion Source Temperature: | 500 |
| Ion Spray Voltage: | -4500 V for negative and 5500 V for positive |
| Ionization: | ESI |
| Mass Accuracy: | 0.1 Da |
| MS ID: | MS002694 |
| Analysis ID: | AN002902 |
| Instrument Name: | ABI Sciex 5500 QTrap |
| Instrument Type: | Triple quadrupole |
| MS Type: | ESI |
| MS Comments: | The MS/MS detection was performed using electrospray ionization (ESI) and advanced scheduled multiple reaction monitoring (MRM) with dynamic windowing and fast polarity switch. The ESI source conditions were set as follows: electrospray voltage of -4500 V for negative mode and 5500 V for positive mode, source temperature of 500 °C, curtain gas of 30, ion source gas 1, and gas 2 of 35 psi, respectively.Peaks were manually inspected and integrated using Multiquant 3.0.2. The peak area was exported to excel for further analysis. |
| Ion Mode: | UNSPECIFIED |
| Collision Energy: | Compound-dependent |
| Ion Source Temperature: | 500 |
| Ion Spray Voltage: | -4500 V for negative and 5500 V for positive |
| Ionization: | ESI |
| Mass Accuracy: | 0.1 Da |
