Summary of Study ST000536
This data is available at the NIH Common Fund's National Metabolomics Data Repository (NMDR) website, the Metabolomics Workbench, https://www.metabolomicsworkbench.org, where it has been assigned Project ID PR000392. The data can be accessed directly via it's Project DOI: 10.21228/M8CP53 This work is supported by NIH grant, U2C- DK119886.
See: https://www.metabolomicsworkbench.org/about/howtocite.php
| Study ID | ST000536 |
| Study Title | CHEAR Plasma Dilution Reference Material Proficiency Test NMR (Part II) |
| Study Type | Metabolomics |
| Study Summary | CHEAR Reference Material Plasma was provided by Emory University. The material was prepared and analyzed using the NMR metabolomics workflow of the Eastern Regional Metabolomics Resource Core (protocols available in metabolomics workbench). Data of six samples were acquired of the sample reference material prepared in replicate. |
| Institute | RTI International |
| Department | Analytical Chemistry & Pharmaceuticals |
| Laboratory | RTI CHEAR Analytical Hub - Untargeted Analysis Resource Core |
| Last Name | Fennell |
| First Name | Timothy |
| Address | 3040 E Cornwallis Road, Research Triangle Park, NC 27709 |
| fennell@rti.org | |
| Phone | 919-485-2781 |
| Submit Date | 2017-01-19 |
| Raw Data Available | Yes |
| Raw Data File Type(s) | fid |
| Chear Study | Yes |
| Analysis Type Detail | NMR |
| Release Date | 2024-12-31 |
| Release Version | 1 |
Select appropriate tab below to view additional metadata details:
NMR:
| NMR ID: | NM000096 |
| Analysis ID: | AN000815 |
| Instrument Name: | Bruker |
| Instrument Type: | FT-NMR |
| NMR Experiment Type: | 1D 1H |
| Field Frequency Lock: | Deuterium |
| Standard Concentration: | 1mM |
| Spectrometer Frequency: | 700 MHz |
| NMR Probe: | 5mm ATMA Cryoprobe |
| NMR Solvent: | D2O |
| NMR Tube Size: | 5mm |
| Shimming Method: | top shim |
| Pulse Sequence: | cpmgpr1d |
| Water Suppression: | yes |
| Pulse Width: | 12.3s |
| Power Level: | 25.119 W |
| Receiver Gain: | 4 |
| Offset Frequency: | 3299 Hz |
| Chemical Shift Ref Cpd: | Formate |
| Temperature: | 300K |
| Number Of Scans: | 128 |
| Dummy Scans: | 4 |
| Acquisition Time: | 3.9s |
| Relaxation Delay: | 2s |
| Spectral Width: | 12.02ppm |
| Num Data Points Acquired: | 65536 |
| Real Data Points: | 32768 |
| Line Broadening: | 0.5 Hz |
| Zero Filling: | yes |
| Apodization: | Lorentzian |
| Baseline Correction Method: | Polynomial |
| Chemical Shift Ref Std: | Formate |
