Summary of Study ST001159

This data is available at the NIH Common Fund's National Metabolomics Data Repository (NMDR) website, the Metabolomics Workbench, https://www.metabolomicsworkbench.org, where it has been assigned Project ID PR000766. The data can be accessed directly via it's Project DOI: 10.21228/M8P09H This work is supported by NIH grant, U2C- DK119886.

See: https://www.metabolomicsworkbench.org/about/howtocite.php

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Study IDST001159
Study TitleTargeted NHP urine metabolomics (part-II)
Study SummaryHere, we use global metabolomics to differentiate temporal effects (1 – 60 d) found in nonhuman primate (NHP) urine small molecule signatures after a 4 Gy total body irradiation.
Institute
Georgetown University
Last NamePannkuk
First NameEvan
Address3970 Reservoir Rd, NW New Research Build
Emailelp44@georgetown.edu
Phone2026875650
Submit Date2019-02-27
Raw Data AvailableYes
Analysis Type DetailLC-MS
Release Date2019-05-15
Release Version1
Evan Pannkuk Evan Pannkuk
https://dx.doi.org/10.21228/M8P09H
ftp://www.metabolomicsworkbench.org/Studies/ application/zip

Select appropriate tab below to view additional metadata details:

Project:

Project ID:PR000766
Project DOI:doi: 10.21228/M8P09H
Project Title:Nonhuman primate (NHP) radiation metabolomics
Project Summary:Here, we use global metabolomics to differentiate temporal effects (1 – 60 d) found in nonhuman primate (NHP) urine small molecule signatures after a 4 Gy total body irradiation.
Institute:Georgetown University
Last Name:Pannkuk
First Name:Evan
Address:3970 Reservoir Rd, NW New Research Build, washington dc, District of Columbia, 20057, USA
Email:elp44@georgetown.edu
Phone:2026875650

Subject:

Subject ID:SU001224
Subject Type:Mammal
Subject Species:Macaca mulatta
Taxonomy ID:9544

Factors:

Subject type: Mammal; Subject species: Macaca mulatta (Factor headings shown in green)

mb_sample_id local_sample_id Treat
SA080366NHP30control_training
SA080367NHP29control_training
SA080368NHP27control_training
SA080369NHP31control_training
SA080370NHP28control_training
SA080371NHP33control_training
SA080372NHP36control_training
SA080373NHP35control_training
SA080374NHP34control_training
SA080375NHP26control_training
SA080376NHP32control_training
SA080377NHP25control_training
SA080378NHP9control_validation
SA080379NHP14control_validation
SA080380NHP10control_validation
SA080381NHP11control_validation
SA080382NHP12control_validation
SA080383NHP7control_validation
SA080384NHP6control_validation
SA080385NHP2control_validation
SA080386NHP3control_validation
SA080387NHP4control_validation
SA080388NHP5control_validation
SA080389NHP13control_validation
SA080390NHP8control_validation
SA080391NHP16control_validation
SA080392NHP1control_validation
SA080393NHP15control_validation
SA080394NHP42exp_training
SA080395NHP41exp_training
SA080396NHP43exp_training
SA080397NHP45exp_training
SA080398NHP48exp_training
SA080399NHP47exp_training
SA080400NHP46exp_training
SA080401NHP40exp_training
SA080402NHP44exp_training
SA080403NHP38exp_training
SA080404NHP39exp_training
SA080405NHP37exp_training
SA080406NHP22exp_validation
SA080407NHP24exp_validation
SA080408NHP21exp_validation
SA080409NHP23exp_validation
SA080410NHP19exp_validation
SA080411NHP17exp_validation
SA080412NHP18exp_validation
SA080413NHP20exp_validation
Showing results 1 to 48 of 48

Collection:

Collection ID:CO001218
Collection Summary:Urine (10 μl) was diluted with 200 μl cold methanol:acetonitrile:water (80:15:5) spiked with internal standards, vortexed, placed on ice for 10 min, and centrifuged for 10 min (10,000 x g, 4°C)
Sample Type:Urine

Treatment:

Treatment ID:TR001239
Treatment Summary:4 Gy at 0.6 Gy/min with a 60Co γ source

Sample Preparation:

Sampleprep ID:SP001232
Sampleprep Summary:Urine (10 μl) was diluted with 200 μl cold methanol:acetonitrile:water (80:15:5) spiked with internal standards, vortexed, placed on ice for 10 min, and centrifuged for 10 min (10,000 x g, 4°C)

Combined analysis:

Analysis ID AN001917
Analysis type MS
Chromatography type Reversed phase
Chromatography system Waters ACQUITY UPLC
Column Acquity BEH amide (100 x 2.1mm,1.7um)
MS Type ESI
MS instrument type Triple quadrupole
MS instrument name Waters Xevo-TQ-S
Ion Mode UNSPECIFIED
Units ng/ml

Chromatography:

Chromatography ID:CH001390
Instrument Name:Waters ACQUITY UPLC
Column Name:Acquity BEH amide (100 x 2.1mm,1.7um)
Chromatography Type:Reversed phase

MS:

MS ID:MS001773
Analysis ID:AN001917
Instrument Name:Waters Xevo-TQ-S
Instrument Type:Triple quadrupole
MS Type:ESI
MS Comments:None
Ion Mode:UNSPECIFIED
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