Summary of study ST001284

This data is available at the NIH Common Fund's National Metabolomics Data Repository (NMDR) website, the Metabolomics Workbench, https://www.metabolomicsworkbench.org, where it has been assigned Project ID PR000862. The data can be accessed directly via it's Project DOI: 10.21228/M8896R This work is supported by NIH grant, U2C- DK119886.

See: https://www.metabolomicsworkbench.org/about/howtocite.php

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Study IDST001284
Study TitlePseudoexfoliation Aqueous Humor Metabolites from Veterans Affairs Patients NMR (part-II)
Study SummaryThe PEX patient AH samples were subjected to 1H-NMR spectroscopy for the identification of metabolites using HSQC and TOCSY techniques.
Institute
University of Miami
DepartmentOphthalmology, Bascom Palmer Eye Institute
LaboratorySanjoy K. Bhattacharya
Last NameBhattacharya
First NameSanjoy
Address1638 NW 10th Avenue, Miami, FL 33136
EmailSBhattacharya@med.miami.edu
Phone305-482-4103
Submit Date2019-11-26
Num Groups1
Total Subjects31
Raw Data AvailableYes
Raw Data File Type(s).par
Analysis Type DetailNMR
Release Date2020-01-13
Release Version1
Sanjoy Bhattacharya Sanjoy Bhattacharya
https://dx.doi.org/10.21228/M8896R
ftp://www.metabolomicsworkbench.org/Studies/ application/zip

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Project:

Project ID:PR000862
Project DOI:doi: 10.21228/M8896R
Project Title:Pseudoexfoliation Syndrome Humor Metabolites from Veterans Affairs Patients
Project Type:untargeted LC-MS/MS IROA metabolomics
Project Summary:We performed high-performance liquid chromatography-tandem mass spectrometry (LC-MS/MS) Isotopic Ratio Outlier Analysis of aqueous humor samples from patients with pseudoexfoliation syndrome (PEX).
Institute:University of Miami
Department:Ophthalmology, Bascom Palmer Eye Institute
Last Name:Bhattacharya
First Name:Sanjoy
Address:1638 NW 10th Avenue, Miami, Florida, 33136, USA
Email:sbhattacharya@med.miami.edu
Phone:3054824103
Contributors:Leila Abdelrahman

Subject:

Subject ID:SU001356
Subject Type:Human
Subject Species:Homo sapiens
Taxonomy ID:9606
Gender:Male and female

Factors:

Subject type: Human; Subject species: Homo sapiens (Factor headings shown in green)

mb_sample_id local_sample_id Treatment
SA093533Sample026PXE
SA093534Sample027PXE
SA093535Sample025PXE
SA093536Sample023PXE
SA093537Sample022PXE
SA093538Sample028PXE
SA093539Sample024PXE
SA093540Sample030PXE
SA093541Sample034PXE
SA093542Sample035PXE
SA093543Sample033PXE
SA093544Sample032PXE
SA093545Sample021PXE
SA093546Sample031PXE
SA093547Sample029PXE
SA093548Sample020PXE
SA093549Sample010PXE
SA093550Sample011PXE
SA093551Sample009PXE
SA093552Sample008PXE
SA093553Sample006PXE
SA093554Sample007PXE
SA093555Sample012PXE
SA093556Sample013PXE
SA093557Sample018PXE
SA093558Sample019PXE
SA093559Sample017PXE
SA093560Sample016PXE
SA093561Sample014PXE
SA093562Sample015PXE
SA093563Sample005PXE
Showing results 1 to 31 of 31

Collection:

Collection ID:CO001350
Collection Summary:All materials were collected from human donors without identifiers under institutional review board exemption/approval. We acquired 31 aqueous humor (AH) samples from participants at the Veterans Administration (VA) Medical Center (Miami, FL). Patient samples used for NMR consisted of individuals with PEX (n=31).
Sample Type:Eye tissue
Collection Location:1201 NW 16th St, Miami, FL 33125

Treatment:

Treatment ID:TR001371
Treatment Summary:No Treatment

Sample Preparation:

Sampleprep ID:SP001364
Sampleprep Summary:Each NMR sample contained 50 μL of volume (45 μL of liquid sample + 5 μL of D2O containing 1.111 mM DSS), with 10% D2O and 0.111 mM DSS.

Analysis:

Analysis ID:AN002128
Analysis Type:NMR
Num Factors:1
Num Metabolites:38
Units:Arbitrary Unites

NMR:

NMR ID:NM000154
Analysis ID:AN002128
Instrument Name:Bruker
Instrument Type:FT-NMR
NMR Experiment Type:2D-1H-1H
Spectrometer Frequency:600 MHz
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