{
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"PROJECT":{"PROJECT_TITLE":"Metabotypes of Subjects with Adverse Reactions Following Vaccination: A Pilot Study","PROJECT_TYPE":"Metabolomic Profile of Human Serum","PROJECT_SUMMARY":"An Adverse Event Following Immunization (AEFI) is an adverse reaction to a vaccination that goes above and beyond the usual side effects that are known to be associated with vaccinations. AEFIs can vary in clinical severity to very mild to incapacitating and occasionally require lost time from work or even hospitalization. In rare cases, there is an aberrant immune reaction from vaccination resulting in a potentially serious adverse event. One known serious adverse event related to the smallpox vaccine is myocarditis and/or pericarditis (myopericarditis). Metabolomics may help identify a particular metabolic signature “metabotype” in patients who are predisposed to developing AEFI such as a systemic reaction, or myocarditis that currently is difficult or impossible to identify prior to the development of the AEFI. This proposed pilot study looks at the metabolic profiles of a specific population of subjects who received the smallpox vaccine with or without other concomitantly administered vaccines to help determine if a unique metabotype can be identified in subjects who reported systemic reactions following immunization. In addition, this proposed study will look at the metabolic profile of several subjects with subclinical or clinically diagnosed myopericarditis to determine if these subjects have a unique metabotype. The ability to identify a unique metabotype would allow a clinician to potentially mitigate serious AEFI and ultimately improve the quality of immunization healthcare. If identified, these profiles might represent novel biomarkers of risk that can supplement existing clinical decision making for risk stratification or vaccine exemptions.","INSTITUTE":"Defense Health Agency - Immunization Healthcare Branch and Womack Army Medical Center","DEPARTMENT":"Immunization","LAST_NAME":"McClenathan, M.D.","FIRST_NAME":"Bruce","ADDRESS":"1-2532 Armistead Street, Fort Bragg, NC 28310","EMAIL":"bruce.m.mcclenathan.civ@mail.mil","PHONE":"(910) 432-4015"},

"STUDY":{"STUDY_TITLE":"Metabotypes of Subjects with Adverse Reactions Following Vaccination","STUDY_TYPE":"Metabolomic Profile of Human Serum","STUDY_SUMMARY":"Metabolomics may help identify a particular metabolic signature “metabotype” in patients who are predisposed to developing AEFI such as a systemic reaction, or myocarditis that currently is difficult or impossible to identify prior to the development of the AEFI. This proposed pilot study looks at the metabolic profiles of a specific population of subjects who received the smallpox vaccine with or without other concomitantly administered vaccines to help determine if a unique metabotype can be identified in subjects who reported systemic reactions following immunization. In addition, this proposed study will look at the metabolic profile of several subjects with subclinical or clinically diagnosed myopericarditis to determine if these subjects have a unique metabotype. The ability to identify a unique metabotype would allow a clinician to potentially mitigate serious AEFI and ultimately improve the quality of immunization healthcare. If identified, these profiles might represent novel biomarkers of risk that can supplement existing clinical decision making for risk stratification or vaccine exemptions.","INSTITUTE":"RTI International","DEPARTMENT":"RCMRC","LABORATORY":"NIH Eastern Regional Comprehensive Metabolomics Resource Core (RTI RCMRC)","LAST_NAME":"Sumner","FIRST_NAME":"Susan","ADDRESS":"3040, East Cornwallis Road, Research Triangle Park, NC 27709","EMAIL":"ssumner@rti.org","PHONE":"919-541-7479","NUM_GROUPS":"4","TOTAL_SUBJECTS":"200","NUM_MALES":"190","NUM_FEMALES":"10"},

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"Factors":{"Gender":"1","Group Number":"2"},
"Additional sample data":{"Visit Number":"1","Datafile Name":"123"}
},
{
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"Additional sample data":{"Visit Number":"3","Datafile Name":"222"}
},
{
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"Additional sample data":{"Visit Number":"1","Datafile Name":"177"}
},
{
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"Additional sample data":{"Visit Number":"3","Datafile Name":"99"}
},
{
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"Additional sample data":{"Visit Number":"1","Datafile Name":"128"}
},
{
"Subject ID":"-",
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"Additional sample data":{"Visit Number":"3","Datafile Name":"89"}
},
{
"Subject ID":"-",
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"Additional sample data":{"Visit Number":"1","Datafile Name":"69"}
},
{
"Subject ID":"-",
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"Additional sample data":{"Visit Number":"3","Datafile Name":"167"}
},
{
"Subject ID":"-",
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"Factors":{"Gender":"1","Group Number":"1"},
"Additional sample data":{"Visit Number":"3","Datafile Name":"202"}
},
{
"Subject ID":"-",
"Sample ID":"S_41",
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"Additional sample data":{"Visit Number":"1","Datafile Name":"74"}
},
{
"Subject ID":"-",
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"Additional sample data":{"Visit Number":"3","Datafile Name":"85"}
},
{
"Subject ID":"-",
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"Additional sample data":{"Visit Number":"1","Datafile Name":"45"}
},
{
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"Additional sample data":{"Visit Number":"3","Datafile Name":"168"}
},
{
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"Additional sample data":{"Visit Number":"1","Datafile Name":"213"}
},
{
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"Additional sample data":{"Visit Number":"3","Datafile Name":"498"}
},
{
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"Additional sample data":{"Visit Number":"1","Datafile Name":"11"}
},
{
"Subject ID":"-",
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"Additional sample data":{"Visit Number":"3","Datafile Name":"40"}
},
{
"Subject ID":"-",
"Sample ID":"S_49",
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"Additional sample data":{"Visit Number":"1","Datafile Name":"153"}
},
{
"Subject ID":"-",
"Sample ID":"S_5",
"Factors":{"Gender":"1","Group Number":"2"},
"Additional sample data":{"Visit Number":"1","Datafile Name":"44"}
},
{
"Subject ID":"-",
"Sample ID":"S_50",
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"Additional sample data":{"Visit Number":"3","Datafile Name":"124"}
},
{
"Subject ID":"-",
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"Additional sample data":{"Visit Number":"1","Datafile Name":"178"}
},
{
"Subject ID":"-",
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"Additional sample data":{"Visit Number":"3","Datafile Name":"90"}
},
{
"Subject ID":"-",
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"Additional sample data":{"Visit Number":"1","Datafile Name":"35"}
},
{
"Subject ID":"-",
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"Factors":{"Gender":"1","Group Number":"2"},
"Additional sample data":{"Visit Number":"3","Datafile Name":"143"}
},
{
"Subject ID":"-",
"Sample ID":"S_55",
"Factors":{"Gender":"1","Group Number":"2"},
"Additional sample data":{"Visit Number":"1","Datafile Name":"203"}
},
{
"Subject ID":"-",
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"Additional sample data":{"Visit Number":"3","Datafile Name":"6"}
},
{
"Subject ID":"-",
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"Additional sample data":{"Visit Number":"1","Datafile Name":"139"}
},
{
"Subject ID":"-",
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"Additional sample data":{"Visit Number":"3","Datafile Name":"163"}
},
{
"Subject ID":"-",
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"Additional sample data":{"Visit Number":"1","Datafile Name":"10"}
},
{
"Subject ID":"-",
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"Additional sample data":{"Visit Number":"3","Datafile Name":"212"}
},
{
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"Additional sample data":{"Visit Number":"3","Datafile Name":"39"}
},
{
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"Additional sample data":{"Visit Number":"1","Datafile Name":"192"}
},
{
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"Additional sample data":{"Visit Number":"3","Datafile Name":"109"}
},
{
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"Additional sample data":{"Visit Number":"1","Datafile Name":"129"}
},
{
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"Additional sample data":{"Visit Number":"3","Datafile Name":"119"}
},
{
"Subject ID":"-",
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"Additional sample data":{"Visit Number":"1","Datafile Name":"395"}
},
{
"Subject ID":"-",
"Sample ID":"S_66",
"Factors":{"Gender":"2","Group Number":"3"},
"Additional sample data":{"Visit Number":"3","Datafile Name":"55"}
},
{
"Subject ID":"-",
"Sample ID":"S_67",
"Factors":{"Gender":"1","Group Number":"3"},
"Additional sample data":{"Visit Number":"1","Datafile Name":"134"}
},
{
"Subject ID":"-",
"Sample ID":"S_68",
"Factors":{"Gender":"1","Group Number":"3"},
"Additional sample data":{"Visit Number":"3","Datafile Name":"448"}
},
{
"Subject ID":"-",
"Sample ID":"S_69",
"Factors":{"Gender":"1","Group Number":"3"},
"Additional sample data":{"Visit Number":"1","Datafile Name":"173"}
},
{
"Subject ID":"-",
"Sample ID":"S_7",
"Factors":{"Gender":"1","Group Number":"1"},
"Additional sample data":{"Visit Number":"1","Datafile Name":"24"}
},
{
"Subject ID":"-",
"Sample ID":"S_70",
"Factors":{"Gender":"1","Group Number":"3"},
"Additional sample data":{"Visit Number":"3","Datafile Name":"70"}
},
{
"Subject ID":"-",
"Sample ID":"S_71",
"Factors":{"Gender":"1","Group Number":"3"},
"Additional sample data":{"Visit Number":"1","Datafile Name":"193"}
},
{
"Subject ID":"-",
"Sample ID":"S_72",
"Factors":{"Gender":"1","Group Number":"3"},
"Additional sample data":{"Visit Number":"3","Datafile Name":"188"}
},
{
"Subject ID":"-",
"Sample ID":"S_73",
"Factors":{"Gender":"1","Group Number":"3"},
"Additional sample data":{"Visit Number":"1","Datafile Name":"405"}
},
{
"Subject ID":"-",
"Sample ID":"S_74",
"Factors":{"Gender":"1","Group Number":"3"},
"Additional sample data":{"Visit Number":"3","Datafile Name":"21"}
},
{
"Subject ID":"-",
"Sample ID":"S_75",
"Factors":{"Gender":"1","Group Number":"3"},
"Additional sample data":{"Visit Number":"1","Datafile Name":"218"}
},
{
"Subject ID":"-",
"Sample ID":"S_76",
"Factors":{"Gender":"1","Group Number":"3"},
"Additional sample data":{"Visit Number":"3","Datafile Name":"50"}
},
{
"Subject ID":"-",
"Sample ID":"S_77",
"Factors":{"Gender":"1","Group Number":"3"},
"Additional sample data":{"Visit Number":"1","Datafile Name":"208"}
},
{
"Subject ID":"-",
"Sample ID":"S_78",
"Factors":{"Gender":"1","Group Number":"3"},
"Additional sample data":{"Visit Number":"3","Datafile Name":"16"}
},
{
"Subject ID":"-",
"Sample ID":"S_79",
"Factors":{"Gender":"1","Group Number":"3"},
"Additional sample data":{"Visit Number":"1","Datafile Name":"158"}
},
{
"Subject ID":"-",
"Sample ID":"S_8",
"Factors":{"Gender":"1","Group Number":"1"},
"Additional sample data":{"Visit Number":"3","Datafile Name":"118"}
},
{
"Subject ID":"-",
"Sample ID":"S_80",
"Factors":{"Gender":"2","Group Number":"3"},
"Additional sample data":{"Visit Number":"3","Datafile Name":"400"}
},
{
"Subject ID":"-",
"Sample ID":"S_81",
"Factors":{"Gender":"1","Group Number":"3"},
"Additional sample data":{"Visit Number":"1","Datafile Name":"30"}
},
{
"Subject ID":"-",
"Sample ID":"S_82",
"Factors":{"Gender":"2","Group Number":"3"},
"Additional sample data":{"Visit Number":"3","Datafile Name":"25"}
},
{
"Subject ID":"-",
"Sample ID":"S_83",
"Factors":{"Gender":"1","Group Number":"3"},
"Additional sample data":{"Visit Number":"1","Datafile Name":"116"}
},
{
"Subject ID":"-",
"Sample ID":"S_84",
"Factors":{"Gender":"1","Group Number":"3"},
"Additional sample data":{"Visit Number":"3","Datafile Name":"61"}
},
{
"Subject ID":"-",
"Sample ID":"S_85",
"Factors":{"Gender":"1","Group Number":"3"},
"Additional sample data":{"Visit Number":"1","Datafile Name":"199"}
},
{
"Subject ID":"-",
"Sample ID":"S_86",
"Factors":{"Gender":"1","Group Number":"3"},
"Additional sample data":{"Visit Number":"3","Datafile Name":"459"}
},
{
"Subject ID":"-",
"Sample ID":"S_87",
"Factors":{"Gender":"1","Group Number":"3"},
"Additional sample data":{"Visit Number":"1","Datafile Name":"41"}
},
{
"Subject ID":"-",
"Sample ID":"S_88",
"Factors":{"Gender":"1","Group Number":"3"},
"Additional sample data":{"Visit Number":"3","Datafile Name":"154"}
},
{
"Subject ID":"-",
"Sample ID":"S_89",
"Factors":{"Gender":"1","Group Number":"3"},
"Additional sample data":{"Visit Number":"1","Datafile Name":"125"}
},
{
"Subject ID":"-",
"Sample ID":"S_9",
"Factors":{"Gender":"1","Group Number":"2"},
"Additional sample data":{"Visit Number":"1","Datafile Name":"15"}
},
{
"Subject ID":"-",
"Sample ID":"S_90",
"Factors":{"Gender":"1","Group Number":"3"},
"Additional sample data":{"Visit Number":"3","Datafile Name":"214"}
},
{
"Subject ID":"-",
"Sample ID":"S_91",
"Factors":{"Gender":"1","Group Number":"3"},
"Additional sample data":{"Visit Number":"1","Datafile Name":"111"}
},
{
"Subject ID":"-",
"Sample ID":"S_92",
"Factors":{"Gender":"1","Group Number":"3"},
"Additional sample data":{"Visit Number":"3","Datafile Name":"91"}
},
{
"Subject ID":"-",
"Sample ID":"S_93",
"Factors":{"Gender":"1","Group Number":"3"},
"Additional sample data":{"Visit Number":"1","Datafile Name":"22"}
},
{
"Subject ID":"-",
"Sample ID":"S_94",
"Factors":{"Gender":"1","Group Number":"3"},
"Additional sample data":{"Visit Number":"3","Datafile Name":"31"}
},
{
"Subject ID":"-",
"Sample ID":"S_95",
"Factors":{"Gender":"1","Group Number":"3"},
"Additional sample data":{"Visit Number":"1","Datafile Name":"66"}
},
{
"Subject ID":"-",
"Sample ID":"S_96",
"Factors":{"Gender":"1","Group Number":"3"},
"Additional sample data":{"Visit Number":"3","Datafile Name":"401"}
},
{
"Subject ID":"-",
"Sample ID":"S_97",
"Factors":{"Gender":"1","Group Number":"3"},
"Additional sample data":{"Visit Number":"1","Datafile Name":"219"}
},
{
"Subject ID":"-",
"Sample ID":"S_98",
"Factors":{"Gender":"1","Group Number":"3"},
"Additional sample data":{"Visit Number":"3","Datafile Name":"140"}
},
{
"Subject ID":"-",
"Sample ID":"S_99",
"Factors":{"Gender":"1","Group Number":"3"},
"Additional sample data":{"Visit Number":"1","Datafile Name":"120"}
}
],
"COLLECTION":{"COLLECTION_SUMMARY":"Serum was collected in accordance with standard operating procedures."},

"TREATMENT":{"TREATMENT_SUMMARY":"Two-hundred sera samples – 100 baseline (pre-vaccine) and 100 post-smallpox vaccination"},

"SAMPLEPREP":{"SAMPLEPREP_SUMMARY":"A total of 200 study samples were thawed on ice for sample preparation, 400 uL of the thawed serum sample were transferred to labeled tubes on ice where they were mixed with 1200uL of MeOH. Analytical quality control (QC) phenotypic pooled samples (3/Group) were generated by transferring pre-determined volumes of each sample from each respective phenotypic Group’s experimental samples into four different 2.0 mL LoBind tubes. The Phenotypic Pool tubes were vortexed, and 3 aliquots of 400 uL was transferred to Phenotypic Pool tubes for each Group. In addition, a study pool was generated by transferring 200 uL of serum from 25 randomly selected experimental samples into a 10.0 mL tube, vortexed and aliquoted into 10 Study Pool tubes. Methanol was added to all tubes (1200 uL), sample tubes were vortexed for 2 min on a multi-tube vortexer and centrifuged at 16,000 rcf for 5 min. A 1000 µl aliquot of the supernatant was transferred into new pre-labeled 2.0 mL LoBind tubes and lyophilized to complete dryness overnight. Samples were reconstituted with 700 uL of NMR Master Mix solution containing Chenomx ISTD: DSS-d6 and D2O-Phosphate Buffer at 7.4 pH. The tubes were vortexed for 4 min on a multi-tube vortexer and centrifuged at 16,000 rcf for 5 min. A 600 uL of each sample supernatant was transferred into a pre-labeled 5mm 4 NMR tubes for data acquisition on a 700 MHz spectrometer."},

"CHROMATOGRAPHY":{"CHROMATOGRAPHY_TYPE":"-","INSTRUMENT_NAME":"-","COLUMN_NAME":"-"},

"ANALYSIS":{"ANALYSIS_TYPE":"NMR"},

"NM":{"INSTRUMENT_NAME":"Bruker","INSTRUMENT_TYPE":"FT-NMR","NMR_EXPERIMENT_TYPE":"1D-1H","FIELD_FREQUENCY_LOCK":"Deuterium","STANDARD_CONCENTRATION":"0.5mM","SPECTROMETER_FREQUENCY":"700MHz","NMR_PROBE":"5mm ATMA Cryoprobe","NMR_SOLVENT":"D2O","NMR_TUBE_SIZE":"5mm","SHIMMING_METHOD":"Topshim","WATER_SUPPRESSION":"yes","RECEIVER_GAIN":"4.5","OFFSET_FREQUENCY":"3299","CHEMICAL_SHIFT_REF_CPD":"DSS","TEMPERATURE":"298.1K","NUMBER_OF_SCANS":"128","DUMMY_SCANS":"4","ACQUISITION_TIME":"3.893s","RELAXATION_DELAY":"2s","SPECTRAL_WIDTH":"12.0277ppm","NUM_DATA_POINTS_ACQUIRED":"65536","REAL_DATA_POINTS":"65536","LINE_BROADENING":"0.5Hz","ZERO_FILLING":"yes","APODIZATION":"Lorentzian","BASELINE_CORRECTION_METHOD":"Polynomial","CHEMICAL_SHIFT_REF_STD":"DSS-d6","BINNED_INCREMENT":"0.04ppm"},

"Data":[{"Bin range(ppm)":"[0.70 .. 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