{
"METABOLOMICS WORKBENCH":{"STUDY_ID":"ST000487","ANALYSIS_ID":"AN000753","VERSION":"1","CREATED_ON":"October 11, 2016, 12:17 pm"},
"PROJECT":{"PROJECT_TITLE":"Plasma and liver metabolomics studies","PROJECT_TYPE":"NMR multivariate analysis","PROJECT_SUMMARY":"1H NMR-based metabolomics approach reveals metabolic alterations in response to dietary imbalances in Megalobrama amblycephala","INSTITUTE":"Huazhong Agricultural University","DEPARTMENT":"Fisheries","LABORATORY":"Key Lab of Freshwater Animal Breeding","LAST_NAME":"Prathomya","FIRST_NAME":"Panita","ADDRESS":"Huazhong Agricultural University, Shizi Shan Jie, Hongshan District., Wuhan, Hubei, 430070, China","EMAIL":"p_prathomya@yahoo.com","PHONE":"13477033229","FUNDING_SOURCE":"Natural Science Foundation of China (No. 31401976), the earmarked fund for the Fundament Research Funds for the Central Universities (2662015PY019) and Modern Agro-industry Technology Research System entitled ‘‘Staple Freshwater Fishery Industry Technology System"},
"STUDY":{"STUDY_TITLE":"Impacts of high-fat diet (HFD), high-carbohydrate diet (HCD) and high-fat-high-carbohydrate diet (HFHCD) on metabolites in a farmed cyprinid fish Megalobrama amblycephala.","STUDY_TYPE":"Dietary imbalance experiment","STUDY_SUMMARY":"1H NMR-based metabolomic approach to measure the concentrations of metabolites in plasma and liver of four different diet groups: HFD, HCD, HFHCD and control. Multivariate statistical analyses were used to determine significantly changed metabolites between all group-pairs.","INSTITUTE":"Huazhong Agricultural University","DEPARTMENT":"Fisheries","LABORATORY":"Key Lab of Freshwater Animal Breeding","LAST_NAME":"Prathomya","FIRST_NAME":"Panita","ADDRESS":"Huazhong Agricultural University, Shizi Shan Jie, Hongshan District.","EMAIL":"p_prathomya@yahoo.com","PHONE":"+8613477033229"},
"SUBJECT":{"SUBJECT_TYPE":"Animal","SUBJECT_SPECIES":"Megalobrama amblycephala","TAXONOMY_ID":"75352"},
"SUBJECT_SAMPLE_FACTORS":[
{
"Subject ID":"-",
"Sample ID":"A12",
"Factors":{"Treatment":"Control"},
"Additional sample data":{"Length (cm)":"14.50","Weight (cm)":"61.23"}
},
{
"Subject ID":"-",
"Sample ID":"A13",
"Factors":{"Treatment":"Control"},
"Additional sample data":{"Length (cm)":"15.20","Weight (cm)":"67.28"}
},
{
"Subject ID":"-",
"Sample ID":"A14",
"Factors":{"Treatment":"Control"},
"Additional sample data":{"Length (cm)":"15.20","Weight (cm)":"72.59"}
},
{
"Subject ID":"-",
"Sample ID":"A15",
"Factors":{"Treatment":"Control"},
"Additional sample data":{"Length (cm)":"15.38","Weight (cm)":"68.29"}
},
{
"Subject ID":"-",
"Sample ID":"A22",
"Factors":{"Treatment":"Control"},
"Additional sample data":{"Length (cm)":"14.30","Weight (cm)":"62.39"}
},
{
"Subject ID":"-",
"Sample ID":"A23",
"Factors":{"Treatment":"Control"},
"Additional sample data":{"Length (cm)":"14.70","Weight (cm)":"69.58"}
},
{
"Subject ID":"-",
"Sample ID":"A32",
"Factors":{"Treatment":"Control"},
"Additional sample data":{"Length (cm)":"14.50","Weight (cm)":"62.11"}
},
{
"Subject ID":"-",
"Sample ID":"A33",
"Factors":{"Treatment":"Control"},
"Additional sample data":{"Length (cm)":"14.80","Weight (cm)":"59.59"}
},
{
"Subject ID":"-",
"Sample ID":"A34",
"Factors":{"Treatment":"Control"},
"Additional sample data":{"Length (cm)":"15.00","Weight (cm)":"71.88"}
},
{
"Subject ID":"-",
"Sample ID":"A35",
"Factors":{"Treatment":"Control"},
"Additional sample data":{"Length (cm)":"14.00","Weight (cm)":"53.36"}
},
{
"Subject ID":"-",
"Sample ID":"B11",
"Factors":{"Treatment":"High fat diet"},
"Additional sample data":{"Length (cm)":"15.30","Weight (cm)":"76.94"}
},
{
"Subject ID":"-",
"Sample ID":"B13",
"Factors":{"Treatment":"High fat diet"},
"Additional sample data":{"Length (cm)":"15.10","Weight (cm)":"71.65"}
},
{
"Subject ID":"-",
"Sample ID":"B14",
"Factors":{"Treatment":"High fat diet"},
"Additional sample data":{"Length (cm)":"15.10","Weight (cm)":"68.30"}
},
{
"Subject ID":"-",
"Sample ID":"B15",
"Factors":{"Treatment":"High fat diet"},
"Additional sample data":{"Length (cm)":"15.10","Weight (cm)":"69.65"}
},
{
"Subject ID":"-",
"Sample ID":"B21",
"Factors":{"Treatment":"High fat diet"},
"Additional sample data":{"Length (cm)":"15.60","Weight (cm)":"87.75"}
},
{
"Subject ID":"-",
"Sample ID":"B31",
"Factors":{"Treatment":"High fat diet"},
"Additional sample data":{"Length (cm)":"15.50","Weight (cm)":"83.18"}
},
{
"Subject ID":"-",
"Sample ID":"B32",
"Factors":{"Treatment":"High fat diet"},
"Additional sample data":{"Length (cm)":"16.00","Weight (cm)":"83.73"}
},
{
"Subject ID":"-",
"Sample ID":"B33",
"Factors":{"Treatment":"High fat diet"},
"Additional sample data":{"Length (cm)":"15.90","Weight (cm)":"83.76"}
},
{
"Subject ID":"-",
"Sample ID":"B34",
"Factors":{"Treatment":"High fat diet"},
"Additional sample data":{"Length (cm)":"14.60","Weight (cm)":"72.42"}
},
{
"Subject ID":"-",
"Sample ID":"B35",
"Factors":{"Treatment":"High fat diet"},
"Additional sample data":{"Length (cm)":"14.70","Weight (cm)":"80.20"}
},
{
"Subject ID":"-",
"Sample ID":"C11",
"Factors":{"Treatment":"High carbohydrate"},
"Additional sample data":{"Length (cm)":"15.50","Weight (cm)":"80.59"}
},
{
"Subject ID":"-",
"Sample ID":"C12",
"Factors":{"Treatment":"High carbohydrate"},
"Additional sample data":{"Length (cm)":"15.30","Weight (cm)":"74.33"}
},
{
"Subject ID":"-",
"Sample ID":"C13",
"Factors":{"Treatment":"High carbohydrate"},
"Additional sample data":{"Length (cm)":"15.30","Weight (cm)":"68.40"}
},
{
"Subject ID":"-",
"Sample ID":"C21",
"Factors":{"Treatment":"High carbohydrate"},
"Additional sample data":{"Length (cm)":"15.00","Weight (cm)":"65.67"}
},
{
"Subject ID":"-",
"Sample ID":"C22",
"Factors":{"Treatment":"High carbohydrate"},
"Additional sample data":{"Length (cm)":"15.00","Weight (cm)":"62.64"}
},
{
"Subject ID":"-",
"Sample ID":"C31",
"Factors":{"Treatment":"High carbohydrate"},
"Additional sample data":{"Length (cm)":"15.10","Weight (cm)":"72.97"}
},
{
"Subject ID":"-",
"Sample ID":"C32",
"Factors":{"Treatment":"High carbohydrate"},
"Additional sample data":{"Length (cm)":"15.10","Weight (cm)":"70.48"}
},
{
"Subject ID":"-",
"Sample ID":"C33",
"Factors":{"Treatment":"High carbohydrate"},
"Additional sample data":{"Length (cm)":"15.90","Weight (cm)":"80.89"}
},
{
"Subject ID":"-",
"Sample ID":"C34",
"Factors":{"Treatment":"High carbohydrate"},
"Additional sample data":{"Length (cm)":"14.60","Weight (cm)":"60.10"}
},
{
"Subject ID":"-",
"Sample ID":"C35",
"Factors":{"Treatment":"High carbohydrate"},
"Additional sample data":{"Length (cm)":"15.40","Weight (cm)":"76.63"}
},
{
"Subject ID":"-",
"Sample ID":"D11",
"Factors":{"Treatment":"Highfat Highcarbohydrate"},
"Additional sample data":{"Length (cm)":"15.60","Weight (cm)":"80.38"}
},
{
"Subject ID":"-",
"Sample ID":"D13",
"Factors":{"Treatment":"Highfat Highcarbohydrate"},
"Additional sample data":{"Length (cm)":"15.00","Weight (cm)":"64.99"}
},
{
"Subject ID":"-",
"Sample ID":"D14",
"Factors":{"Treatment":"Highfat Highcarbohydrate"},
"Additional sample data":{"Length (cm)":"14.60","Weight (cm)":"68.71"}
},
{
"Subject ID":"-",
"Sample ID":"D15",
"Factors":{"Treatment":"Highfat Highcarbohydrate"},
"Additional sample data":{"Length (cm)":"15.30","Weight (cm)":"79.89"}
},
{
"Subject ID":"-",
"Sample ID":"D21",
"Factors":{"Treatment":"Highfat Highcarbohydrate"},
"Additional sample data":{"Length (cm)":"15.50","Weight (cm)":"85.24"}
},
{
"Subject ID":"-",
"Sample ID":"D22",
"Factors":{"Treatment":"Highfat Highcarbohydrate"},
"Additional sample data":{"Length (cm)":"15.10","Weight (cm)":"73.87"}
},
{
"Subject ID":"-",
"Sample ID":"D23",
"Factors":{"Treatment":"Highfat Highcarbohydrate"},
"Additional sample data":{"Length (cm)":"15.20","Weight (cm)":"77.71"}
},
{
"Subject ID":"-",
"Sample ID":"D24",
"Factors":{"Treatment":"Highfat Highcarbohydrate"},
"Additional sample data":{"Length (cm)":"15.00","Weight (cm)":"71.87"}
},
{
"Subject ID":"-",
"Sample ID":"D31",
"Factors":{"Treatment":"Highfat Highcarbohydrate"},
"Additional sample data":{"Length (cm)":"13.70","Weight (cm)":"51.59"}
},
{
"Subject ID":"-",
"Sample ID":"D32",
"Factors":{"Treatment":"Highfat Highcarbohydrate"},
"Additional sample data":{"Length (cm)":"14.50","Weight (cm)":"58.65"}
}
],
"COLLECTION":{"COLLECTION_SUMMARY":"Blood samples were obtained following the standard protocol, using sodium heparin as anticoagulant. Liver tissue samples were weighed and put in tube then immediately flash-frozen with liquid nitrogen and stored at −80 °C till used for metabolomics analysis.","COLLECTION_PROTOCOL_FILENAME":"Sample collection and NMR protocol.pdf","SAMPLE_TYPE":"Plasma, Liver"},
"TREATMENT":{"TREATMENT_SUMMARY":"Three tanks were randomly assigned to each diet group (3 replicates x 4 diet-groups): control (C; containing 8.0% fat and 26.7% carbohydrates), high fat diet (H.D containing 12.2% fat and 27.8% carbohydrates), high carbohydrate diet (H.D containing 8.3% fat and 34.1% carbohydrates) and high fat high carbohydrate diet (HFH.D containing 10.4% fat and 30.9% carbohydrates."},
"SAMPLEPREP":{"SAMPLEPREP_SUMMARY":"Each plasma sample (170 μL) was mixed with 340 μL phosphate buffer (45 mM, pH 7.47, 50% D2O) containing 0.9% NaCl in a 5 mm NMR tube and used directly for the NMR analysis. Liver tissues (about 50 mg) were homogenized in cold methanol and water (v/v=2:1) using a Qiagen Tissue-Lyser (Retsch GmBH, Germany). The supernatant (550uL) was collected after centrifugation (16 099 g, 4°C, 10 min). The extraction was repeated thrice using the same procedure. The supernatants collected from the above procedure were mixed together and freeze-dried after the removal of methanol in vacuo. Then the residue was dissolved in 600 μL of phosphate buffer (0.15 M, pH 7.38, 80% D2O) containing 0.001% TSP and 0.01% NaN3. The supernatant (550 μL) was transferred into a 5 mm NMR tube."},
"CHROMATOGRAPHY":{"CHROMATOGRAPHY_TYPE":"-","INSTRUMENT_NAME":"-","COLUMN_NAME":"-"},
"ANALYSIS":{"ANALYSIS_TYPE":"NMR"},
"NM":{"INSTRUMENT_NAME":"Bruker AVance III","INSTRUMENT_TYPE":"FT-NMR","NMR_EXPERIMENT_TYPE":"1D-1H","FIELD_FREQUENCY_LOCK":"Deuterium","STANDARD_CONCENTRATION":"0.058mM","SPECTROMETER_FREQUENCY":"600MHz","NMR_PROBE":"cryo, inverse","NMR_SOLVENT":"D2O","NMR_TUBE_SIZE":"5mm x 7 in","SHIMMING_METHOD":"topshim"},
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