{
"METABOLOMICS WORKBENCH":{"STUDY_ID":"ST000508","ANALYSIS_ID":"AN000777","VERSION":"1","CREATED_ON":"December 2, 2016, 11:11 am"},

"PROJECT":{"PROJECT_TITLE":"Metabolic Profiling of Date Palm Fruits","PROJECT_SUMMARY":"The goal of this study was to investigate metabotypes of date palm fruits through global, non-targeted metabolomics of assorted date fruits varieties from different countries of origin.","INSTITUTE":"Weill Cornell Medicine Qatar","DEPARTMENT":"Bioinformatics Core","LABORATORY":"Suhre Lab","LAST_NAME":"Suhre","FIRST_NAME":"Karsten","ADDRESS":"Luqta Street, Education City, Doha, Qatar, 24144, Qatar","EMAIL":"nishastephan@gmail.com","PHONE":"+97444928281","FUNDING_SOURCE":"Funding for this research was provided by Qatar National Research Fund, a member of Qatar Foundation under the National Priorities Research Program – Exceptional Award (NPRP-EP) NPRPX-014-4-001."},

"STUDY":{"STUDY_TITLE":"Metabolic Profiling of Date Palm Fruits","STUDY_SUMMARY":"In this study, two independent large cohorts of mature dates exhibiting substantial diversity in origin, varieties and fruit processing conditions were measured by metabolomics techniques in order to identify major determinants of the fruit metabotype. Additional samples reflecting different stages of date fruit ripening process has been included for 10 different fruit varieties.","INSTITUTE":"Weill Cornell Medicine in Qatar","DEPARTMENT":"Bioinformatics Core","LABORATORY":"Suhre Lab","LAST_NAME":"Suhre","FIRST_NAME":"Karsten","ADDRESS":"Education City","EMAIL":"nis2034@qatar-med.cornell.edu","PHONE":"+97433888408"},

"SUBJECT":{"SUBJECT_TYPE":"Date palm fruit","SUBJECT_SPECIES":"Phoenix dactylifera","TAXONOMY_ID":"42345"},
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"Additional sample data":{"country_of_origin":"Dubai, UAE","brand_name":"Dr Ahmad Saif Al-Fasi farm","collection_info":"Abu Dhabi Date Palm Festival 2012"}
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"Additional sample data":{"country_of_origin":"Iran","brand_name":"Zargarzadeh.com","collection_info":"Abu Dhabi Date Palm Festival 2012"}
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"Additional sample data":{"country_of_origin":"UAE","brand_name":"Date Palm Friends Society","collection_info":"Abu Dhabi Date Palm Festival 2012"}
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{
"Subject ID":"61",
"Sample ID":"61.1",
"Factors":{"date_variety":"Hamrata"},
"Additional sample data":{"country_of_origin":"Tunisia","brand_name":"Personal collection","collection_info":"Eman Mabrook - BCQ"}
},
{
"Subject ID":"61",
"Sample ID":"61.3",
"Factors":{"date_variety":"Hamrata"},
"Additional sample data":{"country_of_origin":"Tunisia","brand_name":"Personal collection","collection_info":"Eman Mabrook - BCQ"}
},
{
"Subject ID":"61",
"Sample ID":"61",
"Factors":{"date_variety":"Hamrata"},
"Additional sample data":{"country_of_origin":"Tunisia","brand_name":"Personal collection","collection_info":"Eman Mabrook - BCQ"}
},
{
"Subject ID":"62",
"Sample ID":"62.2",
"Factors":{"date_variety":"Grenja"},
"Additional sample data":{"country_of_origin":"Tunisia","brand_name":"Personal collection","collection_info":"Eman Mabrook - BCQ"}
},
{
"Subject ID":"64",
"Sample ID":"64.2",
"Factors":{"date_variety":"Deglet Nour"},
"Additional sample data":{"country_of_origin":"Tunisia","brand_name":"Personal collection","collection_info":"Eman Mabrook - BCQ"}
},
{
"Subject ID":"64",
"Sample ID":"64.3",
"Factors":{"date_variety":"Deglet Nour"},
"Additional sample data":{"country_of_origin":"Tunisia","brand_name":"Personal collection","collection_info":"Eman Mabrook - BCQ"}
},
{
"Subject ID":"69",
"Sample ID":"69.3",
"Factors":{"date_variety":"Medjoul"},
"Additional sample data":{"country_of_origin":"California, USA","brand_name":"Spinneys","collection_info":"Spinneys"}
},
{
"Subject ID":"70",
"Sample ID":"70.2",
"Factors":{"date_variety":"Sukkary"},
"Additional sample data":{"country_of_origin":"KSA","brand_name":"Personal collection","collection_info":"Personal collection -Mashael Al Shafai"}
},
{
"Subject ID":"71",
"Sample ID":"71",
"Factors":{"date_variety":"Fegous-ghlid"},
"Additional sample data":{"country_of_origin":"Morocco","brand_name":"Marrakech  Souq","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"72",
"Sample ID":"72",
"Factors":{"date_variety":"Majhool AA"},
"Additional sample data":{"country_of_origin":"Morocco","brand_name":"Marrakech  Souq","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"73",
"Sample ID":"73",
"Factors":{"date_variety":"Jihl"},
"Additional sample data":{"country_of_origin":"Morocco","brand_name":"Marrakech  Souq","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"74",
"Sample ID":"74",
"Factors":{"date_variety":"Tadment"},
"Additional sample data":{"country_of_origin":"Morocco","brand_name":"Ourzazet Souq","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"75",
"Sample ID":"75",
"Factors":{"date_variety":"Sayer"},
"Additional sample data":{"country_of_origin":"Morocco","brand_name":"Ourzazet Souq","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"77",
"Sample ID":"77",
"Factors":{"date_variety":"Hafs"},
"Additional sample data":{"country_of_origin":"Morocco","brand_name":"Ourzazet Souq","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"78",
"Sample ID":"78",
"Factors":{"date_variety":"Bouzagza"},
"Additional sample data":{"country_of_origin":"Morocco","brand_name":"Ourzazet Souq","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"79",
"Sample ID":"79",
"Factors":{"date_variety":"Boukhanda"},
"Additional sample data":{"country_of_origin":"Morocco","brand_name":"Fess Souq","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"80",
"Sample ID":"80",
"Factors":{"date_variety":"Agalid"},
"Additional sample data":{"country_of_origin":"Morocco","brand_name":"Fess Souq","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"81",
"Sample ID":"81",
"Factors":{"date_variety":"Lakhal"},
"Additional sample data":{"country_of_origin":"Morocco","brand_name":"Fess Souq","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"82",
"Sample ID":"82",
"Factors":{"date_variety":"Najda"},
"Additional sample data":{"country_of_origin":"Morocco","brand_name":"Fess Souq","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"83",
"Sample ID":"83",
"Factors":{"date_variety":"Wahardan"},
"Additional sample data":{"country_of_origin":"Morocco","brand_name":"Awfous Souq","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"84",
"Sample ID":"84",
"Factors":{"date_variety":"Bid-djaj"},
"Additional sample data":{"country_of_origin":"Morocco","brand_name":"Awfous Souq","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"85",
"Sample ID":"85",
"Factors":{"date_variety":"Azaghzaw"},
"Additional sample data":{"country_of_origin":"Morocco","brand_name":"Awfous Souq","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"85",
"Sample ID":"85A",
"Factors":{"date_variety":"Azaghzaw"},
"Additional sample data":{"country_of_origin":"Morocco","brand_name":"Awfous Souq","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"85",
"Sample ID":"85C",
"Factors":{"date_variety":"Azaghzaw"},
"Additional sample data":{"country_of_origin":"Morocco","brand_name":"Awfous Souq","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"86",
"Sample ID":"86",
"Factors":{"date_variety":"Bouslikh"},
"Additional sample data":{"country_of_origin":"Morocco","brand_name":"Awfous Souq","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"87",
"Sample ID":"87",
"Factors":{"date_variety":"Tazgaghzt"},
"Additional sample data":{"country_of_origin":"Morocco","brand_name":"Awfous Souq","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"87",
"Sample ID":"87B",
"Factors":{"date_variety":"Tazgaghzt"},
"Additional sample data":{"country_of_origin":"Morocco","brand_name":"Awfous Souq","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"87",
"Sample ID":"87C",
"Factors":{"date_variety":"Tazgaghzt"},
"Additional sample data":{"country_of_origin":"Morocco","brand_name":"Awfous Souq","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"88",
"Sample ID":"88",
"Factors":{"date_variety":"Tamaright 2"},
"Additional sample data":{"country_of_origin":"Morocco","brand_name":"Awfous Souq","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"89",
"Sample ID":"89E",
"Factors":{"date_variety":"khalt-lhammar"},
"Additional sample data":{"country_of_origin":"Morocco","brand_name":"Ourzazet Souq","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"89",
"Sample ID":"89",
"Factors":{"date_variety":"khalt-lhammar"},
"Additional sample data":{"country_of_origin":"Morocco","brand_name":"Ourzazet Souq","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"89",
"Sample ID":"89C",
"Factors":{"date_variety":"khalt-lhammar"},
"Additional sample data":{"country_of_origin":"Morocco","brand_name":"Ourzazet Souq","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"89",
"Sample ID":"89D",
"Factors":{"date_variety":"khalt-lhammar"},
"Additional sample data":{"country_of_origin":"Morocco","brand_name":"Ourzazet Souq","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"89",
"Sample ID":"89A",
"Factors":{"date_variety":"khalt-lhammar"},
"Additional sample data":{"country_of_origin":"Morocco","brand_name":"Ourzazet Souq","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"89",
"Sample ID":"89B",
"Factors":{"date_variety":"khalt-lhammar"},
"Additional sample data":{"country_of_origin":"Morocco","brand_name":"Ourzazet Souq","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"90",
"Sample ID":"90",
"Factors":{"date_variety":"Mejhool"},
"Additional sample data":{"country_of_origin":"Morocco","brand_name":"Awfous Souq","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"90",
"Sample ID":"90A",
"Factors":{"date_variety":"Mejhool"},
"Additional sample data":{"country_of_origin":"Morocco","brand_name":"Awfous Souq","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"90",
"Sample ID":"90B",
"Factors":{"date_variety":"Mejhool"},
"Additional sample data":{"country_of_origin":"Morocco","brand_name":"Awfous Souq","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"90",
"Sample ID":"90C",
"Factors":{"date_variety":"Mejhool"},
"Additional sample data":{"country_of_origin":"Morocco","brand_name":"Awfous Souq","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"91",
"Sample ID":"91F",
"Factors":{"date_variety":"Belahzit"},
"Additional sample data":{"country_of_origin":"Morocco","brand_name":"Awfous Souq","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"91",
"Sample ID":"91",
"Factors":{"date_variety":"Belahzit"},
"Additional sample data":{"country_of_origin":"Morocco","brand_name":"Awfous Souq","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"91",
"Sample ID":"91A",
"Factors":{"date_variety":"Belahzit"},
"Additional sample data":{"country_of_origin":"Morocco","brand_name":"Awfous Souq","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"91",
"Sample ID":"91H",
"Factors":{"date_variety":"Belahzit"},
"Additional sample data":{"country_of_origin":"Morocco","brand_name":"Awfous Souq","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"92",
"Sample ID":"92E",
"Factors":{"date_variety":"Shetwia"},
"Additional sample data":{"country_of_origin":"Morocco","brand_name":"Awfous Souq","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"92",
"Sample ID":"92",
"Factors":{"date_variety":"Shetwia"},
"Additional sample data":{"country_of_origin":"Morocco","brand_name":"Awfous Souq","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"92",
"Sample ID":"92A",
"Factors":{"date_variety":"Shetwia"},
"Additional sample data":{"country_of_origin":"Morocco","brand_name":"Awfous Souq","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"92",
"Sample ID":"92B1",
"Factors":{"date_variety":"Shetwia"},
"Additional sample data":{"country_of_origin":"Morocco","brand_name":"Awfous Souq","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"92",
"Sample ID":"92C",
"Factors":{"date_variety":"Shetwia"},
"Additional sample data":{"country_of_origin":"Morocco","brand_name":"Awfous Souq","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"92",
"Sample ID":"92D",
"Factors":{"date_variety":"Shetwia"},
"Additional sample data":{"country_of_origin":"Morocco","brand_name":"Awfous Souq","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"93",
"Sample ID":"93C",
"Factors":{"date_variety":"Booserdoon"},
"Additional sample data":{"country_of_origin":"Morocco","brand_name":"Awfous Souq","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"93",
"Sample ID":"93",
"Factors":{"date_variety":"Booserdoon"},
"Additional sample data":{"country_of_origin":"Morocco","brand_name":"Awfous Souq","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"93",
"Sample ID":"93D",
"Factors":{"date_variety":"Booserdoon"},
"Additional sample data":{"country_of_origin":"Morocco","brand_name":"Awfous Souq","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"96",
"Sample ID":"96",
"Factors":{"date_variety":"Bekri-khder"},
"Additional sample data":{"country_of_origin":"Morocco","brand_name":"Ourzazet souq","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"97",
"Sample ID":"97A",
"Factors":{"date_variety":"Tahmoot 2"},
"Additional sample data":{"country_of_origin":"Morocco","brand_name":"Arfoud souq","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"97",
"Sample ID":"97B",
"Factors":{"date_variety":"Tahmoot 2"},
"Additional sample data":{"country_of_origin":"Morocco","brand_name":"Arfoud souq","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"97",
"Sample ID":"97C",
"Factors":{"date_variety":"Tahmoot 2"},
"Additional sample data":{"country_of_origin":"Morocco","brand_name":"Arfoud souq","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"98",
"Sample ID":"98",
"Factors":{"date_variety":"Boufegous rqiq"},
"Additional sample data":{"country_of_origin":"Morocco","brand_name":"Mghalba oasis","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"99",
"Sample ID":"99D",
"Factors":{"date_variety":"Maajoun"},
"Additional sample data":{"country_of_origin":"Morocco","brand_name":"Mghalba oasis","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"99",
"Sample ID":"99B",
"Factors":{"date_variety":"Maajoun"},
"Additional sample data":{"country_of_origin":"Morocco","brand_name":"Mghalba oasis","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"99",
"Sample ID":"99C",
"Factors":{"date_variety":"Maajoun"},
"Additional sample data":{"country_of_origin":"Morocco","brand_name":"Mghalba oasis","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"99",
"Sample ID":"99A",
"Factors":{"date_variety":"Maajoun"},
"Additional sample data":{"country_of_origin":"Morocco","brand_name":"Mghalba oasis","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"100",
"Sample ID":"100",
"Factors":{"date_variety":"Boussakri"},
"Additional sample data":{"country_of_origin":"Morocco","brand_name":"Mghalba oasis","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"101",
"Sample ID":"101",
"Factors":{"date_variety":"Admoo"},
"Additional sample data":{"country_of_origin":"Morocco","brand_name":"Mghalba oasis","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"103",
"Sample ID":"103B",
"Factors":{"date_variety":"Tarzawa"},
"Additional sample data":{"country_of_origin":"Morocco","brand_name":"Mghalba oasis","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"103",
"Sample ID":"103C",
"Factors":{"date_variety":"Tarzawa"},
"Additional sample data":{"country_of_origin":"Morocco","brand_name":"Mghalba oasis","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"103",
"Sample ID":"103A",
"Factors":{"date_variety":"Tarzawa"},
"Additional sample data":{"country_of_origin":"Morocco","brand_name":"Mghalba oasis","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"104",
"Sample ID":"104",
"Factors":{"date_variety":"Boozekri"},
"Additional sample data":{"country_of_origin":"Morocco","brand_name":"Mghalba oasis","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"105",
"Sample ID":"105",
"Factors":{"date_variety":"Zaghlool"},
"Additional sample data":{"country_of_origin":"Egypt","brand_name":"Hyat Plaza mall, Doha","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"108",
"Sample ID":"108",
"Factors":{"date_variety":"Deglet Bayda"},
"Additional sample data":{"country_of_origin":"Algeria","brand_name":"-","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"109",
"Sample ID":"109",
"Factors":{"date_variety":"Deglet Nour Hourra"},
"Additional sample data":{"country_of_origin":"Algeria","brand_name":"-","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"112",
"Sample ID":"112",
"Factors":{"date_variety":"Adam adaalee"},
"Additional sample data":{"country_of_origin":"Algeria","brand_name":"-","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"113",
"Sample ID":"113",
"Factors":{"date_variety":"Tantebouchte"},
"Additional sample data":{"country_of_origin":"Algeria","brand_name":"-","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"114",
"Sample ID":"114",
"Factors":{"date_variety":"Fegous"},
"Additional sample data":{"country_of_origin":"Algeria","brand_name":"-","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"117",
"Sample ID":"117",
"Factors":{"date_variety":"Deglet Nour"},
"Additional sample data":{"country_of_origin":"Algeria","brand_name":"-","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"119",
"Sample ID":"119",
"Factors":{"date_variety":"Telemsoua"},
"Additional sample data":{"country_of_origin":"Algeria","brand_name":"-","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"120",
"Sample ID":"120",
"Factors":{"date_variety":"Adam bujamaa"},
"Additional sample data":{"country_of_origin":"Algeria","brand_name":"-","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"122",
"Sample ID":"122",
"Factors":{"date_variety":"Tamjhourt"},
"Additional sample data":{"country_of_origin":"Algeria","brand_name":"-","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"124",
"Sample ID":"124",
"Factors":{"date_variety":"Gharss"},
"Additional sample data":{"country_of_origin":"Algeria","brand_name":"-","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"125",
"Sample ID":"125",
"Factors":{"date_variety":"Ddagla"},
"Additional sample data":{"country_of_origin":"Algeria","brand_name":"-","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"126",
"Sample ID":"126",
"Factors":{"date_variety":"Tagarbushet"},
"Additional sample data":{"country_of_origin":"Algeria","brand_name":"-","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"128",
"Sample ID":"128",
"Factors":{"date_variety":"Deglet"},
"Additional sample data":{"country_of_origin":"Algeria","brand_name":"-","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"129",
"Sample ID":"129",
"Factors":{"date_variety":"Adam admaan"},
"Additional sample data":{"country_of_origin":"Algeria","brand_name":"-","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"131",
"Sample ID":"131",
"Factors":{"date_variety":"Hameera"},
"Additional sample data":{"country_of_origin":"Algeria","brand_name":"-","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"133",
"Sample ID":"133",
"Factors":{"date_variety":"Hamray"},
"Additional sample data":{"country_of_origin":"Algeria","brand_name":"-","collection_info":"Morocco Trip 2013"}
},
{
"Subject ID":"136",
"Sample ID":"136",
"Factors":{"date_variety":"Zehdi"},
"Additional sample data":{"country_of_origin":"Jordan","brand_name":"-","collection_info":"Abu Dhabi Date Palm Festival 2013"}
},
{
"Subject ID":"137",
"Sample ID":"137",
"Factors":{"date_variety":"Lulu"},
"Additional sample data":{"country_of_origin":"Jordan","brand_name":"-","collection_info":"Abu Dhabi Date Palm Festival 2013"}
},
{
"Subject ID":"139",
"Sample ID":"139",
"Factors":{"date_variety":"Siwa"},
"Additional sample data":{"country_of_origin":"Egypt","brand_name":"-","collection_info":"Abu Dhabi Date Palm Festival 2013"}
},
{
"Subject ID":"141",
"Sample ID":"141",
"Factors":{"date_variety":"Saeedi"},
"Additional sample data":{"country_of_origin":"Libya","brand_name":"-","collection_info":"Abu Dhabi Date Palm Festival 2013"}
},
{
"Subject ID":"142",
"Sample ID":"142",
"Factors":{"date_variety":"Kulma soda"},
"Additional sample data":{"country_of_origin":"Sudan","brand_name":"-","collection_info":"Abu Dhabi Date Palm Festival 2013"}
},
{
"Subject ID":"143",
"Sample ID":"143",
"Factors":{"date_variety":"Grundeela/Qundeil"},
"Additional sample data":{"country_of_origin":"Sudan","brand_name":"-","collection_info":"Abu Dhabi Date Palm Festival 2013"}
},
{
"Subject ID":"144",
"Sample ID":"144",
"Factors":{"date_variety":"Barakawi"},
"Additional sample data":{"country_of_origin":"Sudan","brand_name":"-","collection_info":"Abu Dhabi Date Palm Festival 2013"}
},
{
"Subject ID":"145",
"Sample ID":"145",
"Factors":{"date_variety":"Sultana Bedeen"},
"Additional sample data":{"country_of_origin":"Sudan","brand_name":"-","collection_info":"Abu Dhabi Date Palm Festival 2013"}
},
{
"Subject ID":"146",
"Sample ID":"146",
"Factors":{"date_variety":"Aydea Al Qaseem"},
"Additional sample data":{"country_of_origin":"KSA","brand_name":"-","collection_info":"Abu Dhabi Date Palm Festival 2013"}
},
{
"Subject ID":"147",
"Sample ID":"147",
"Factors":{"date_variety":"Qatarah/Kattara"},
"Additional sample data":{"country_of_origin":"UAE","brand_name":"-","collection_info":"Abu Dhabi Date Palm Festival 2013"}
},
{
"Subject ID":"148",
"Sample ID":"148",
"Factors":{"date_variety":"Msalla"},
"Additional sample data":{"country_of_origin":"UAE","brand_name":"-","collection_info":"Abu Dhabi Date Palm Festival 2013"}
},
{
"Subject ID":"149",
"Sample ID":"149",
"Factors":{"date_variety":"Dabbas"},
"Additional sample data":{"country_of_origin":"UAE","brand_name":"-","collection_info":"Abu Dhabi Date Palm Festival 2013"}
},
{
"Subject ID":"150",
"Sample ID":"150",
"Factors":{"date_variety":"Sillege"},
"Additional sample data":{"country_of_origin":"UAE","brand_name":"-","collection_info":"Abu Dhabi Date Palm Festival 2013"}
},
{
"Subject ID":"151",
"Sample ID":"151",
"Factors":{"date_variety":"Harmayi Sadrati"},
"Additional sample data":{"country_of_origin":"Iran","brand_name":"-","collection_info":"Abu Dhabi Date Palm Festival 2013"}
}
],
"COLLECTION":{"COLLECTION_SUMMARY":"In the present study, 123 unique date varieties (Phoenix dactylifera) from 14 countries were collected in two separate occasions: A first collection took part in 2012 (DS1) and the second one in 2013 (DS2). The term variety is used here to describe a distinct phenotypic class of dates and if the same variety was collected from different countries, a different sample ID was assigned to each collected sample per country. Overall, dates from the first sample collection were mostly from the Gulf region obtained in a fairly dried condition from shops and festivals whilst the second sample collection was dominated by North African dates obtained mostly fresh from the palm trees. For the second collection of dates, field work permissions were obtained verbally from owners of visited oases. The marketed versus fresh nature of dates between the two sample collections implies varying post-harvest conditions. All collected dates with homogenous brown color were further dried by exposing them to open air for two weeks before further processing. With the second sample collection, while harvesting ripened fruits from the palm trees, immature fruits still undergoing ripening activity and occasionally late green Kimri fruits from the pre-ripening stage were collected when available. In total, 37 immature date fruits, corresponding to 10 date samples, were collected. With each of the 10 samples, the immature fruits were ranked by their extent of ripening based on visual assessment of color change and skin wrinkling. Each fruit was given an ID based on a combination of the sample number and a letter reflecting the fruit rank within the sample. In general, dates were considered mature if the low moisture prevented any further change in their appearance. Notably, maturity is attained naturally with the dry class of dates but often artificially with the soft class of dates owing to intrinsically higher moisture levels.","SAMPLE_TYPE":"Date palm fruit","COLLECTION_LOCATION":"Differnt locations specified in the","COLLECTION_DURATION":"2012 - 2013","STORAGE_CONDITIONS":"-80C"},

"TREATMENT":{"TREATMENT_SUMMARY":"The aim of this study was to determine metabolic phenotype of the date palm fruits without any treatment at the baseline."},

"SAMPLEPREP":{"SAMPLEPREP_SUMMARY":"Sample pre-processing for DS1: 50 mg of the peel and flesh of the date fruits were flash frozen in liquid nitrogen and extracted as previously described (PMID:21699588). Sample pre-processing for DS2 The beads were added to the pre-weighed frozen samples together with water (8 µL of per mg of sample) for homogenisation. The samples were continuously stirred on the GenoGrinder (Glen Mills GenoGrinder 2000, Germany) at 1000 strokes per minute for five minutes, to ensure complete homogenization. 100 µL of aliquot from each sample was transferred to the plates. The samples were loaded on three plates. To each sample, 450 µL of extraction solvent (MeOH with 10 µL /ml chlorophenylalanine, 2.5 µL /ml 2-fluorophenylglycine, 25 µg/ml d-6 cholestrol and 25 µL /ml tridecanoic acid) was added. The samples were then shaken on the GenoGrinder (GenoGrinder, Spex, USA) at 675 strokes per min for two minutes and centrifuged at 2000 rpm for 5 minutes on a Beckman centrifuge (Beckman GS-6R Centrifuge, USA) at 40C. The extracted samples were divided into equal parts for metabolomics analysis on the Gas Chromatography Mass Spectrometry (GC/MS) and the Orbitrap Elite accurate Liquid Chromatography Mass Spectrometry2 (LC-MS-MS) platforms. Four sets of samples were prepared by the Hamilton robot (Hamilton Star, Germany) by transferring 110 µL aliquots from each well to three PCR plates, each for LC positive, LC negative, replicate set and one to 250 µL auto sampler vial inserts for GC. All samples were dried for 120 minutes by using a Zymark Turbovap 96 (Zymark Turbovap, USA) followed by overnight incubation in a drybox to ensure optimal dryness of the sample. Sample processing DS1 and DS2 Metabolite measurements with Ultrahigh Performance Liquid Chromatography/Mass Spectroscopy (UPLC/MS/MS): The UPLC/MS/MS analysis was based on the Waters ACUITY ultra performance liquid chromatography (Waters Corporation, USA) and the ThermoFischer Scientific Orbitrap Elite high-resolution accurate mass spectrometer (Thermo Fischer Scientific Inc., USA) equipped with a heated electrospray ionization (HESI) source and an Orbitrap mass analyzer. The dried sample extracts for the LC positive and LC negative mode were reconstituted in acidic and basic LC- compatible solvents. Two independent injections were performed on each sample using separate dedicated columns for optimized acidic positive ions and the other for optimized basic negative ions. The acidic samples were reconstituted by gradient elution of water and methanol containing 0.1 % formic acid whereas; the basic samples were reconstituted by gradient elution of water and methanol containing 6.5mM ammonium bicarbonate (PMID: 19624122). The mass spectra analysis alternated between MS and data dependent MS2 scans using dynamic exclusion. Metabolite measurements with GC/MS: The samples assigned for the GC/MS analysis were further dried under vacuum desiccation for an entire day and derivatized under dried nitrogen using bistrimethyl-silyl-trifluoroacetamide (BSTFA). The GS/MS analysis was based on a Thermo FinniganTM TRACETM DSQTM (ThermoFinnigan, USA) fast-scanning single –quadrupole mass spectrophotometer using electron impact ionization source. The GC column was 5% phenyl and the temperature ramp range was from 40 to 3000 C in a time span of 16 minutes."},

"CHROMATOGRAPHY":{"CHROMATOGRAPHY_SUMMARY":"The 5% diphenyl/ 95% dimethyl polysiloxane GC column and the temperature ramp was from 40° to 300° C in a 16 minute period. Samples were analyzed on a Thermo-Finnigan Trace DSQ fast-scanning single-quadrupole mass spectrometer using electron impact ionization. The instrument was tuned and calibrated for mass resolution and mass accuracy on a daily basis.","CHROMATOGRAPHY_TYPE":"GC","INSTRUMENT_NAME":"Thermo-Finnigan Trace DSQ fast-scanning single-quadrupole mass spectrometer","COLUMN_NAME":"5% diphenyl/ 95% dimethyl polysiloxane GC column"},

"ANALYSIS":{"ANALYSIS_TYPE":"MS","LABORATORY_NAME":"Metabolon, Inc."},

"MS":{"MS_COMMENTS":"-","INSTRUMENT_NAME":"Thermo Trace DSQ","INSTRUMENT_TYPE":"Single quadrupole","MS_TYPE":"EI","ION_MODE":"POSITIVE"},

"MS_METABOLITE_DATA":{
"Units":"Counts per second (cps)",

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}

}