#METABOLOMICS WORKBENCH wpathmasiri_20230301_124535 DATATRACK_ID:3770 STUDY_ID:ST002501 ANALYSIS_ID:AN004110 VERSION 1 CREATED_ON 01-29-2024 #PROJECT PR:PROJECT_TITLE The ECHO Cohort Exposome: First Steps using HHEAR Analysis – An Opportunity PR:PROJECT_TITLE for ALL ECHO Cohorts to Contribute Type A Samples – Untargeted Analysis PR:PROJECT_TITLE (ReCHARGE Cohort) PR:PROJECT_TYPE C18 Reversed-Phase Broad Spectrum Metabolomics PR:PROJECT_SUMMARY This project was funded by the NIH Environmental influences on Child Health PR:PROJECT_SUMMARY Outcomes (ECHO) Program. Untargeted metabolomics profiling data was acquired PR:PROJECT_SUMMARY from urine samples provided by 14 ECHO cohorts. PR:INSTITUTE NC HHEAR Hub PR:DEPARTMENT Untargeted Analysis PR:LABORATORY Sumner Lab PR:LAST_NAME Rushing PR:FIRST_NAME Blake PR:ADDRESS Nutrition Research Institute, UNC-CH, 500 Laureate Way, Kannapolis, NC 28081 PR:EMAIL blake_rushing@unc.edu PR:PHONE (704) 282-9838 PR:FUNDING_SOURCE This research was supported by the Environmental influences on Child Health PR:FUNDING_SOURCE Outcomes (ECHO) program, Office of The Director, National Institutes of Health. PR:FUNDING_SOURCE The content is solely the responsibility of the authors and does not necessarily PR:FUNDING_SOURCE represent the official views of the National Institutes of Health. The ReCHARGE PR:FUNDING_SOURCE ECHO Cohort is supported by the following ECHO Program Collaborators: ECHO PR:FUNDING_SOURCE Coordinating Center: Duke Clinical Research Institute, Durham, North Carolina: PR:FUNDING_SOURCE Smith PB, Newby KL, Benjamin DK; U2C OD023375; ECHO Data Analysis Center: Johns PR:FUNDING_SOURCE Hopkins University Bloomberg School of Public Health, Baltimore, Maryland: PR:FUNDING_SOURCE Jacobson LP; Research Triangle Institute, Durham, North Carolina: Catellier D; PR:FUNDING_SOURCE U24 OD023382; North Carolina Human Health Exposure Analysis Resource Hub: PR:FUNDING_SOURCE Research Triangle Institute: Fennell T, University of North Carolina at Chapel PR:FUNDING_SOURCE Hill: Sumner S, University of North Carolina at Charlotte: Du X; U2C ES030857; PR:FUNDING_SOURCE Human Health Exposure Analysis Resource Coordinating Center: Westat, Inc., PR:FUNDING_SOURCE Rockville, Maryland: O’Brien B; U24 ES026539 PR:DOI http://dx.doi.org/10.21228/M8Z12P #STUDY ST:STUDY_TITLE The ECHO Cohort Exposome: First Steps using HHEAR Analysis – An Opportunity ST:STUDY_TITLE for ALL ECHO Cohorts to Contribute Type A Samples – Untargeted Analysis ST:STUDY_TITLE (ReCHARGE Cohort) ST:STUDY_TYPE Case-Control Study ST:STUDY_SUMMARY The ReCHARGE study is a case control study of children with Autism Spectrum ST:STUDY_SUMMARY Disorder, Developmental Delay, and who are typically developing. They were ST:STUDY_SUMMARY initially recruited into the study between the ages and 2 and 5 years of age, ST:STUDY_SUMMARY and are being seen again during middle childhood and adolescence. This research ST:STUDY_SUMMARY was supported by the Environmental influences on Child Health Outcomes (ECHO) ST:STUDY_SUMMARY program, Office of The Director, National Institutes of Health. The content is ST:STUDY_SUMMARY solely the responsibility of the authors and does not necessarily represent the ST:STUDY_SUMMARY official views of the National Institutes of Health. ReCHARGE is an ECHO cohort ST:STUDY_SUMMARY which is supported by the following ECHO Program Collaborators: ECHO ST:STUDY_SUMMARY Coordinating Center: Duke Clinical Research Institute, Durham, North Carolina: ST:STUDY_SUMMARY Smith PB, Newby KL, Benjamin DK; U2C OD023375 ECHO Data Analysis Center: Johns ST:STUDY_SUMMARY Hopkins University Bloomberg School of Public Health, Baltimore, Maryland: ST:STUDY_SUMMARY Jacobson LP; Research Triangle Institute, Durham, North Carolina: Catellier D; ST:STUDY_SUMMARY U24 OD023382 North Carolina Human Health Exposure Analysis Resource Hub: ST:STUDY_SUMMARY Research Triangle Institute: Fennell T, University of North Carolina at Chapel ST:STUDY_SUMMARY Hill: Sumner S, University of North Carolina at Charlotte: Du X; U2C ES030857 ST:STUDY_SUMMARY Human Health Exposure Analysis Resource Coordinating Center: Westat, Inc., ST:STUDY_SUMMARY Rockville, Maryland: O’Brien B; U24 ES026539 ST:INSTITUTE University of California, Davis ST:DEPARTMENT School of Medicine, Public Health Sciences ST:LAST_NAME Deborah ST:FIRST_NAME Bennett ST:ADDRESS Public Health Sciences Medical Sciences 1-C Davis, CA 95616 ST:EMAIL dhbennett@ucdavis.edu ST:PHONE (530) 754-8282 ST:SUBMIT_DATE 2023-03-01 #SUBJECT SU:SUBJECT_TYPE Human SU:SUBJECT_SPECIES Homo sapiens SU:TAXONOMY_ID 9606 #SUBJECT_SAMPLE_FACTORS: SUBJECT(optional)[tab]SAMPLE[tab]FACTORS(NAME:VALUE pairs separated by |)[tab]Additional sample data SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_B_1 Sample Type:Blank | Batch:1 Analysis Order=12; RAW_FILE_NAME=ReCHARGE_B_1 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_B_2 Sample Type:Blank | Batch:1 Analysis Order=26; RAW_FILE_NAME=ReCHARGE_B_2 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_B_3 Sample Type:Blank | Batch:1 Analysis Order=39; RAW_FILE_NAME=ReCHARGE_B_3 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_B_4 Sample Type:Blank | Batch:1 Analysis Order=53; RAW_FILE_NAME=ReCHARGE_B_4 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_B_5 Sample Type:Blank | Batch:1 Analysis Order=67; RAW_FILE_NAME=ReCHARGE_B_5 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_B_6 Sample Type:Blank | Batch:1 Analysis Order=81; RAW_FILE_NAME=ReCHARGE_B_6 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_B_7 Sample Type:Blank | Batch:1 Analysis Order=94; RAW_FILE_NAME=ReCHARGE_B_7 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_B_8 Sample Type:Blank | Batch:1 Analysis Order=108; RAW_FILE_NAME=ReCHARGE_B_8 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_B_10 Sample Type:Blank | Batch:2 Analysis Order=137; RAW_FILE_NAME=ReCHARGE_B_10 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_B_11 Sample Type:Blank | Batch:2 Analysis Order=150; RAW_FILE_NAME=ReCHARGE_B_11 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_B_12 Sample Type:Blank | Batch:2 Analysis Order=164; RAW_FILE_NAME=ReCHARGE_B_12 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_B_13 Sample Type:Blank | Batch:2 Analysis Order=178; RAW_FILE_NAME=ReCHARGE_B_13 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_B_14 Sample Type:Blank | Batch:2 Analysis Order=192; RAW_FILE_NAME=ReCHARGE_B_14 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_B_15 Sample Type:Blank | Batch:2 Analysis Order=205; RAW_FILE_NAME=ReCHARGE_B_15 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_B_16 Sample Type:Blank | Batch:2 Analysis Order=219; RAW_FILE_NAME=ReCHARGE_B_16 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_B_9 Sample Type:Blank | Batch:2 Analysis Order=123; RAW_FILE_NAME=ReCHARGE_B_9 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_B_18 Sample Type:Blank | Batch:3 Analysis Order=247; RAW_FILE_NAME=ReCHARGE_B_18 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_B_19 Sample Type:Blank | Batch:3 Analysis Order=260; RAW_FILE_NAME=ReCHARGE_B_19 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_B_20 Sample Type:Blank | Batch:3 Analysis Order=274; RAW_FILE_NAME=ReCHARGE_B_20 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_B_21 Sample Type:Blank | Batch:3 Analysis Order=288; RAW_FILE_NAME=ReCHARGE_B_21 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_B_22 Sample Type:Blank | Batch:3 Analysis Order=295; RAW_FILE_NAME=ReCHARGE_B_22 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_CHEAR_U_1 Sample Type:CHEAR Urine Pool | Batch:1 Analysis Order=14; RAW_FILE_NAME=ReCHARGE_CHEAR_U_1 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_CHEAR_U_2 Sample Type:CHEAR Urine Pool | Batch:1 Analysis Order=41; RAW_FILE_NAME=ReCHARGE_CHEAR_U_2 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_CHEAR_U_3 Sample Type:CHEAR Urine Pool | Batch:1 Analysis Order=69; RAW_FILE_NAME=ReCHARGE_CHEAR_U_3 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_CHEAR_U_4 Sample Type:CHEAR Urine Pool | Batch:1 Analysis Order=96; RAW_FILE_NAME=ReCHARGE_CHEAR_U_4 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_CHEAR_U_5 Sample Type:CHEAR Urine Pool | Batch:2 Analysis Order=125; RAW_FILE_NAME=ReCHARGE_CHEAR_U_5 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_CHEAR_U_6 Sample Type:CHEAR Urine Pool | Batch:2 Analysis Order=152; RAW_FILE_NAME=ReCHARGE_CHEAR_U_6 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_CHEAR_U_7 Sample Type:CHEAR Urine Pool | Batch:2 Analysis Order=180; RAW_FILE_NAME=ReCHARGE_CHEAR_U_7 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_CHEAR_U_8 Sample Type:CHEAR Urine Pool | Batch:2 Analysis Order=207; RAW_FILE_NAME=ReCHARGE_CHEAR_U_8 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_CHEAR_U_10 Sample Type:CHEAR Urine Pool | Batch:3 Analysis Order=262; RAW_FILE_NAME=ReCHARGE_CHEAR_U_10 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_CHEAR_U_11 Sample Type:CHEAR Urine Pool | Batch:3 Analysis Order=290; RAW_FILE_NAME=ReCHARGE_CHEAR_U_11 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_CHEAR_U_9 Sample Type:CHEAR Urine Pool | Batch:3 Analysis Order=235; RAW_FILE_NAME=ReCHARGE_CHEAR_U_9 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_HHEAR_U1_1 Sample Type:HHEAR Urine Pool 1 (HHEAR_U1_20) | Batch:1 Analysis Order=13; RAW_FILE_NAME=ReCHARGE_HHEAR_U1_1 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_HHEAR_U1_2 Sample Type:HHEAR Urine Pool 1 (HHEAR_U1_20) | Batch:1 Analysis Order=40; RAW_FILE_NAME=ReCHARGE_HHEAR_U1_2 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_HHEAR_U1_3 Sample Type:HHEAR Urine Pool 1 (HHEAR_U1_20) | Batch:1 Analysis Order=68; RAW_FILE_NAME=ReCHARGE_HHEAR_U1_3 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_HHEAR_U1_4 Sample Type:HHEAR Urine Pool 1 (HHEAR_U1_20) | Batch:1 Analysis Order=95; RAW_FILE_NAME=ReCHARGE_HHEAR_U1_4 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_HHEAR_U1_5 Sample Type:HHEAR Urine Pool 1 (HHEAR_U1_20) | Batch:2 Analysis Order=124; RAW_FILE_NAME=ReCHARGE_HHEAR_U1_5 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_HHEAR_U1_6 Sample Type:HHEAR Urine Pool 1 (HHEAR_U1_20) | Batch:2 Analysis Order=151; RAW_FILE_NAME=ReCHARGE_HHEAR_U1_6 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_HHEAR_U1_7 Sample Type:HHEAR Urine Pool 1 (HHEAR_U1_20) | Batch:2 Analysis Order=179; RAW_FILE_NAME=ReCHARGE_HHEAR_U1_7 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_HHEAR_U1_8 Sample Type:HHEAR Urine Pool 1 (HHEAR_U1_20) | Batch:2 Analysis Order=206; RAW_FILE_NAME=ReCHARGE_HHEAR_U1_8 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_HHEAR_U1_10 Sample Type:HHEAR Urine Pool 1 (HHEAR_U1_20) | Batch:3 Analysis Order=261; RAW_FILE_NAME=ReCHARGE_HHEAR_U1_10 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_HHEAR_U1_11 Sample Type:HHEAR Urine Pool 1 (HHEAR_U1_20) | Batch:3 Analysis Order=289; RAW_FILE_NAME=ReCHARGE_HHEAR_U1_11 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_HHEAR_U1_9 Sample Type:HHEAR Urine Pool 1 (HHEAR_U1_20) | Batch:3 Analysis Order=234; RAW_FILE_NAME=ReCHARGE_HHEAR_U1_9 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_HHEAR_U2_1 Sample Type:HHEAR Urine Pool 2 (HHEAR_U2_50) | Batch:1 Analysis Order=27; RAW_FILE_NAME=ReCHARGE_HHEAR_U2_1 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_HHEAR_U2_2 Sample Type:HHEAR Urine Pool 2 (HHEAR_U2_50) | Batch:1 Analysis Order=54; RAW_FILE_NAME=ReCHARGE_HHEAR_U2_2 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_HHEAR_U2_3 Sample Type:HHEAR Urine Pool 2 (HHEAR_U2_50) | Batch:1 Analysis Order=82; RAW_FILE_NAME=ReCHARGE_HHEAR_U2_3 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_HHEAR_U2_4 Sample Type:HHEAR Urine Pool 2 (HHEAR_U2_50) | Batch:1 Analysis Order=109; RAW_FILE_NAME=ReCHARGE_HHEAR_U2_4 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_HHEAR_U2_5 Sample Type:HHEAR Urine Pool 2 (HHEAR_U2_50) | Batch:2 Analysis Order=138; RAW_FILE_NAME=ReCHARGE_HHEAR_U2_5 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_HHEAR_U2_6 Sample Type:HHEAR Urine Pool 2 (HHEAR_U2_50) | Batch:2 Analysis Order=165; RAW_FILE_NAME=ReCHARGE_HHEAR_U2_6 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_HHEAR_U2_7 Sample Type:HHEAR Urine Pool 2 (HHEAR_U2_50) | Batch:2 Analysis Order=193; RAW_FILE_NAME=ReCHARGE_HHEAR_U2_7 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_HHEAR_U2_8 Sample Type:HHEAR Urine Pool 2 (HHEAR_U2_50) | Batch:2 Analysis Order=220; RAW_FILE_NAME=ReCHARGE_HHEAR_U2_8 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_HHEAR_U2_10 Sample Type:HHEAR Urine Pool 2 (HHEAR_U2_50) | Batch:3 Analysis Order=275; RAW_FILE_NAME=ReCHARGE_HHEAR_U2_10 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_HHEAR_U2_11 Sample Type:HHEAR Urine Pool 2 (HHEAR_U2_50) | Batch:3 Analysis Order=296; RAW_FILE_NAME=ReCHARGE_HHEAR_U2_11 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_HHEAR_U2_9 Sample Type:HHEAR Urine Pool 2 (HHEAR_U2_50) | Batch:3 Analysis Order=248; RAW_FILE_NAME=ReCHARGE_HHEAR_U2_9 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_NIST_3672_1 Sample Type:NIST Urine Pool 3672 | Batch:1 Analysis Order=1; RAW_FILE_NAME=ReCHARGE_NIST_3672_1 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_NIST_3672_2 Sample Type:NIST Urine Pool 3672 | Batch:1 Analysis Order=56; RAW_FILE_NAME=ReCHARGE_NIST_3672_2 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_NIST_3672_3 Sample Type:NIST Urine Pool 3672 | Batch:1 Analysis Order=111; RAW_FILE_NAME=ReCHARGE_NIST_3672_3 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_NIST_3672_4 Sample Type:NIST Urine Pool 3672 | Batch:2 Analysis Order=112; RAW_FILE_NAME=ReCHARGE_NIST_3672_4 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_NIST_3672_5 Sample Type:NIST Urine Pool 3672 | Batch:2 Analysis Order=167; RAW_FILE_NAME=ReCHARGE_NIST_3672_5 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_NIST_3672_6 Sample Type:NIST Urine Pool 3672 | Batch:2 Analysis Order=222; RAW_FILE_NAME=ReCHARGE_NIST_3672_6 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_NIST_3672_7 Sample Type:NIST Urine Pool 3672 | Batch:3 Analysis Order=223; RAW_FILE_NAME=ReCHARGE_NIST_3672_7 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_NIST_3672_8 Sample Type:NIST Urine Pool 3672 | Batch:3 Analysis Order=277; RAW_FILE_NAME=ReCHARGE_NIST_3672_8 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_SP_1 Sample Type:Study Pool | Batch:1 Analysis Order=15; RAW_FILE_NAME=ReCHARGE_SP_1 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_SP_2 Sample Type:Study Pool | Batch:1 Analysis Order=28; RAW_FILE_NAME=ReCHARGE_SP_2 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_SP_3 Sample Type:Study Pool | Batch:1 Analysis Order=42; RAW_FILE_NAME=ReCHARGE_SP_3 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_SP_4 Sample Type:Study Pool | Batch:1 Analysis Order=55; RAW_FILE_NAME=ReCHARGE_SP_4 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_SP_5 Sample Type:Study Pool | Batch:1 Analysis Order=70; RAW_FILE_NAME=ReCHARGE_SP_5 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_SP_6 Sample Type:Study Pool | Batch:1 Analysis Order=83; RAW_FILE_NAME=ReCHARGE_SP_6 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_SP_7 Sample Type:Study Pool | Batch:1 Analysis Order=97; RAW_FILE_NAME=ReCHARGE_SP_7 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_SP_8 Sample Type:Study Pool | Batch:1 Analysis Order=110; RAW_FILE_NAME=ReCHARGE_SP_8 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_SP_10 Sample Type:Study Pool | Batch:2 Analysis Order=139; RAW_FILE_NAME=ReCHARGE_SP_10 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_SP_11 Sample Type:Study Pool | Batch:2 Analysis Order=153; RAW_FILE_NAME=ReCHARGE_SP_11 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_SP_12 Sample Type:Study Pool | Batch:2 Analysis Order=166; RAW_FILE_NAME=ReCHARGE_SP_12 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_SP_13 Sample Type:Study Pool | Batch:2 Analysis Order=181; RAW_FILE_NAME=ReCHARGE_SP_13 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_SP_14 Sample Type:Study Pool | Batch:2 Analysis Order=194; RAW_FILE_NAME=ReCHARGE_SP_14 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_SP_15 Sample Type:Study Pool | Batch:2 Analysis Order=208; RAW_FILE_NAME=ReCHARGE_SP_15 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_SP_16 Sample Type:Study Pool | Batch:2 Analysis Order=221; RAW_FILE_NAME=ReCHARGE_SP_16 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_SP_9 Sample Type:Study Pool | Batch:2 Analysis Order=126; RAW_FILE_NAME=ReCHARGE_SP_9 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_SP_17 Sample Type:Study Pool | Batch:3 Analysis Order=236; RAW_FILE_NAME=ReCHARGE_SP_17 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_SP_18 Sample Type:Study Pool | Batch:3 Analysis Order=249; RAW_FILE_NAME=ReCHARGE_SP_18 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_SP_19 Sample Type:Study Pool | Batch:3 Analysis Order=263; RAW_FILE_NAME=ReCHARGE_SP_19 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_SP_20 Sample Type:Study Pool | Batch:3 Analysis Order=276; RAW_FILE_NAME=ReCHARGE_SP_20 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_SP_21 Sample Type:Study Pool | Batch:3 Analysis Order=291; RAW_FILE_NAME=ReCHARGE_SP_21 SUBJECT_SAMPLE_FACTORS N/A ReCHARGE_SP_22 Sample Type:Study Pool | Batch:3 Analysis Order=297; RAW_FILE_NAME=ReCHARGE_SP_22 SUBJECT_SAMPLE_FACTORS EM-378T5-U-00-11601 ReCHARGE_S_1 Sample Type:Study Sample | Batch:1 Analysis Order=2; RAW_FILE_NAME=ReCHARGE_S_1 SUBJECT_SAMPLE_FACTORS EM-37RQ6-U-00-11601 ReCHARGE_S_10 Sample Type:Study Sample | Batch:1 Analysis Order=11; RAW_FILE_NAME=ReCHARGE_S_10 SUBJECT_SAMPLE_FACTORS EM-372M7-U-00-11601 ReCHARGE_S_11 Sample Type:Study Sample | Batch:1 Analysis Order=16; RAW_FILE_NAME=ReCHARGE_S_11 SUBJECT_SAMPLE_FACTORS EM-36C39-U-00-11601 ReCHARGE_S_12 Sample Type:Study Sample | Batch:1 Analysis Order=17; RAW_FILE_NAME=ReCHARGE_S_12 SUBJECT_SAMPLE_FACTORS EM-37911-U-00-11601 ReCHARGE_S_13 Sample Type:Study Sample | Batch:1 Analysis Order=18; RAW_FILE_NAME=ReCHARGE_S_13 SUBJECT_SAMPLE_FACTORS EM-37BB5-U-00-11601 ReCHARGE_S_14 Sample Type:Study Sample | Batch:1 Analysis Order=19; RAW_FILE_NAME=ReCHARGE_S_14 SUBJECT_SAMPLE_FACTORS EM-379P3-U-00-11601 ReCHARGE_S_15 Sample Type:Study Sample | Batch:1 Analysis Order=20; RAW_FILE_NAME=ReCHARGE_S_15 SUBJECT_SAMPLE_FACTORS EM-376L5-U-00-11601 ReCHARGE_S_16 Sample Type:Study Sample | Batch:1 Analysis Order=21; RAW_FILE_NAME=ReCHARGE_S_16 SUBJECT_SAMPLE_FACTORS EM-37NW7-U-00-11601 ReCHARGE_S_17 Sample Type:Study Sample | Batch:1 Analysis Order=22; RAW_FILE_NAME=ReCHARGE_S_17 SUBJECT_SAMPLE_FACTORS EM-37KM2-U-00-11601 ReCHARGE_S_18 Sample Type:Study Sample | Batch:1 Analysis Order=23; RAW_FILE_NAME=ReCHARGE_S_18 SUBJECT_SAMPLE_FACTORS EM-373B0-U-00-11601 ReCHARGE_S_19 Sample Type:Study Sample | Batch:1 Analysis Order=24; RAW_FILE_NAME=ReCHARGE_S_19 SUBJECT_SAMPLE_FACTORS EM-37473-U-00-11601 ReCHARGE_S_2 Sample Type:Study Sample | Batch:1 Analysis Order=3; RAW_FILE_NAME=ReCHARGE_S_2 SUBJECT_SAMPLE_FACTORS EM-37BS7-U-00-11601 ReCHARGE_S_20 Sample Type:Study Sample | Batch:1 Analysis Order=25; RAW_FILE_NAME=ReCHARGE_S_20 SUBJECT_SAMPLE_FACTORS EM-36W47-U-00-11601 ReCHARGE_S_21 Sample Type:Study Sample | Batch:1 Analysis Order=29; RAW_FILE_NAME=ReCHARGE_S_21 SUBJECT_SAMPLE_FACTORS EM-37KA8-U-00-11601 ReCHARGE_S_22 Sample Type:Study Sample | Batch:1 Analysis Order=30; RAW_FILE_NAME=ReCHARGE_S_22 SUBJECT_SAMPLE_FACTORS EM-37T30-U-00-11601 ReCHARGE_S_23 Sample Type:Study Sample | Batch:1 Analysis Order=31; RAW_FILE_NAME=ReCHARGE_S_23 SUBJECT_SAMPLE_FACTORS EM-36RS3-U-00-11601 ReCHARGE_S_24 Sample Type:Study Sample | Batch:1 Analysis Order=32; RAW_FILE_NAME=ReCHARGE_S_24 SUBJECT_SAMPLE_FACTORS EM-36N87-U-00-11601 ReCHARGE_S_25 Sample Type:Study Sample | Batch:1 Analysis Order=33; RAW_FILE_NAME=ReCHARGE_S_25 SUBJECT_SAMPLE_FACTORS EM-36H91-U-00-11601 ReCHARGE_S_26 Sample Type:Study Sample | Batch:1 Analysis Order=34; RAW_FILE_NAME=ReCHARGE_S_26 SUBJECT_SAMPLE_FACTORS EM-37A96-U-00-11601 ReCHARGE_S_27 Sample Type:Study Sample | Batch:1 Analysis Order=35; RAW_FILE_NAME=ReCHARGE_S_27 SUBJECT_SAMPLE_FACTORS EM-37Y01-U-00-11601 ReCHARGE_S_28 Sample Type:Study Sample | Batch:1 Analysis Order=36; RAW_FILE_NAME=ReCHARGE_S_28 SUBJECT_SAMPLE_FACTORS EM-36TB9-U-00-11601 ReCHARGE_S_29 Sample Type:Study Sample | Batch:1 Analysis Order=37; RAW_FILE_NAME=ReCHARGE_S_29 SUBJECT_SAMPLE_FACTORS EM-37861-U-00-11601 ReCHARGE_S_3 Sample Type:Study Sample | Batch:1 Analysis Order=4; RAW_FILE_NAME=ReCHARGE_S_3 SUBJECT_SAMPLE_FACTORS EM-37FS3-U-00-11601 ReCHARGE_S_30 Sample Type:Study Sample | Batch:1 Analysis Order=38; RAW_FILE_NAME=ReCHARGE_S_30 SUBJECT_SAMPLE_FACTORS EM-376F8-U-00-11601 ReCHARGE_S_31 Sample Type:Study Sample | Batch:1 Analysis Order=43; RAW_FILE_NAME=ReCHARGE_S_31 SUBJECT_SAMPLE_FACTORS EM-36UY7-U-00-11601 ReCHARGE_S_32 Sample Type:Study Sample | Batch:1 Analysis Order=44; RAW_FILE_NAME=ReCHARGE_S_32 SUBJECT_SAMPLE_FACTORS EM-37XK3-U-00-11601 ReCHARGE_S_33 Sample Type:Study Sample | Batch:1 Analysis Order=45; RAW_FILE_NAME=ReCHARGE_S_33 SUBJECT_SAMPLE_FACTORS EM-36SC8-U-00-11601 ReCHARGE_S_34 Sample Type:Study Sample | Batch:1 Analysis Order=46; RAW_FILE_NAME=ReCHARGE_S_34 SUBJECT_SAMPLE_FACTORS EM-370G2-U-00-11601 ReCHARGE_S_35 Sample Type:Study Sample | Batch:1 Analysis Order=47; RAW_FILE_NAME=ReCHARGE_S_35 SUBJECT_SAMPLE_FACTORS EM-37QD5-U-00-11601 ReCHARGE_S_36 Sample Type:Study Sample | Batch:1 Analysis Order=48; RAW_FILE_NAME=ReCHARGE_S_36 SUBJECT_SAMPLE_FACTORS EM-36RB1-U-00-11601 ReCHARGE_S_37 Sample Type:Study Sample | Batch:1 Analysis Order=49; RAW_FILE_NAME=ReCHARGE_S_37 SUBJECT_SAMPLE_FACTORS EM-37TF8-U-00-11601 ReCHARGE_S_38 Sample Type:Study Sample | Batch:1 Analysis Order=50; RAW_FILE_NAME=ReCHARGE_S_38 SUBJECT_SAMPLE_FACTORS EM-36VK7-U-00-11601 ReCHARGE_S_39 Sample Type:Study Sample | Batch:1 Analysis Order=51; RAW_FILE_NAME=ReCHARGE_S_39 SUBJECT_SAMPLE_FACTORS EM-36RM7-U-00-11601 ReCHARGE_S_4 Sample Type:Study Sample | Batch:1 Analysis Order=5; RAW_FILE_NAME=ReCHARGE_S_4 SUBJECT_SAMPLE_FACTORS EM-36G43-U-00-11601 ReCHARGE_S_40 Sample Type:Study Sample | Batch:1 Analysis Order=52; RAW_FILE_NAME=ReCHARGE_S_40 SUBJECT_SAMPLE_FACTORS EM-37PG0-U-00-11601 ReCHARGE_S_41 Sample Type:Study Sample | Batch:1 Analysis Order=57; RAW_FILE_NAME=ReCHARGE_S_41 SUBJECT_SAMPLE_FACTORS EM-36SX1-U-00-11601 ReCHARGE_S_42 Sample Type:Study Sample | Batch:1 Analysis Order=58; RAW_FILE_NAME=ReCHARGE_S_42 SUBJECT_SAMPLE_FACTORS EM-36J40-U-00-11601 ReCHARGE_S_43 Sample Type:Study Sample | Batch:1 Analysis Order=59; RAW_FILE_NAME=ReCHARGE_S_43 SUBJECT_SAMPLE_FACTORS EM-36MX7-U-00-11601 ReCHARGE_S_44 Sample Type:Study Sample | Batch:1 Analysis Order=60; RAW_FILE_NAME=ReCHARGE_S_44 SUBJECT_SAMPLE_FACTORS EM-37U39-U-00-11601 ReCHARGE_S_45 Sample Type:Study Sample | Batch:1 Analysis Order=61; RAW_FILE_NAME=ReCHARGE_S_45 SUBJECT_SAMPLE_FACTORS EM-36Q01-U-00-11601 ReCHARGE_S_46 Sample Type:Study Sample | Batch:1 Analysis Order=62; RAW_FILE_NAME=ReCHARGE_S_46 SUBJECT_SAMPLE_FACTORS EM-37SU6-U-00-11601 ReCHARGE_S_47 Sample Type:Study Sample | Batch:1 Analysis Order=63; RAW_FILE_NAME=ReCHARGE_S_47 SUBJECT_SAMPLE_FACTORS EM-37838-U-00-11601 ReCHARGE_S_48 Sample Type:Study Sample | Batch:1 Analysis Order=64; RAW_FILE_NAME=ReCHARGE_S_48 SUBJECT_SAMPLE_FACTORS EM-37MM0-U-00-11601 ReCHARGE_S_49 Sample Type:Study Sample | Batch:1 Analysis Order=65; RAW_FILE_NAME=ReCHARGE_S_49 SUBJECT_SAMPLE_FACTORS EM-37SL6-U-00-11601 ReCHARGE_S_5 Sample Type:Study Sample | Batch:1 Analysis Order=6; RAW_FILE_NAME=ReCHARGE_S_5 SUBJECT_SAMPLE_FACTORS EM-36NA7-U-00-11601 ReCHARGE_S_50 Sample Type:Study Sample | Batch:1 Analysis Order=66; RAW_FILE_NAME=ReCHARGE_S_50 SUBJECT_SAMPLE_FACTORS EM-377A8-U-00-11601 ReCHARGE_S_51 Sample Type:Study Sample | Batch:1 Analysis Order=71; RAW_FILE_NAME=ReCHARGE_S_51 SUBJECT_SAMPLE_FACTORS EM-37G58-U-00-11601 ReCHARGE_S_52 Sample Type:Study Sample | Batch:1 Analysis Order=72; RAW_FILE_NAME=ReCHARGE_S_52 SUBJECT_SAMPLE_FACTORS EM-36WU4-U-00-11601 ReCHARGE_S_53 Sample Type:Study Sample | Batch:1 Analysis Order=73; RAW_FILE_NAME=ReCHARGE_S_53 SUBJECT_SAMPLE_FACTORS EM-36PA5-U-00-11601 ReCHARGE_S_54 Sample Type:Study Sample | Batch:1 Analysis Order=74; RAW_FILE_NAME=ReCHARGE_S_54 SUBJECT_SAMPLE_FACTORS EM-36X04-U-00-11601 ReCHARGE_S_55 Sample Type:Study Sample | Batch:1 Analysis Order=75; RAW_FILE_NAME=ReCHARGE_S_55 SUBJECT_SAMPLE_FACTORS EM-37YN5-U-00-11601 ReCHARGE_S_56 Sample Type:Study Sample | Batch:1 Analysis Order=76; RAW_FILE_NAME=ReCHARGE_S_56 SUBJECT_SAMPLE_FACTORS EM-36HH8-U-00-11601 ReCHARGE_S_57 Sample Type:Study Sample | Batch:1 Analysis Order=77; RAW_FILE_NAME=ReCHARGE_S_57 SUBJECT_SAMPLE_FACTORS EM-36XA7-U-00-11601 ReCHARGE_S_58 Sample Type:Study Sample | Batch:1 Analysis Order=78; RAW_FILE_NAME=ReCHARGE_S_58 SUBJECT_SAMPLE_FACTORS EM-37LS7-U-00-11601 ReCHARGE_S_59 Sample Type:Study Sample | Batch:1 Analysis Order=79; RAW_FILE_NAME=ReCHARGE_S_59 SUBJECT_SAMPLE_FACTORS EM-36Q35-U-00-11601 ReCHARGE_S_6 Sample Type:Study Sample | Batch:1 Analysis Order=7; RAW_FILE_NAME=ReCHARGE_S_6 SUBJECT_SAMPLE_FACTORS EM-36KQ5-U-00-11601 ReCHARGE_S_60 Sample Type:Study Sample | Batch:1 Analysis Order=80; RAW_FILE_NAME=ReCHARGE_S_60 SUBJECT_SAMPLE_FACTORS EM-37AT6-U-00-11601 ReCHARGE_S_61 Sample Type:Study Sample | Batch:1 Analysis Order=84; RAW_FILE_NAME=ReCHARGE_S_61 SUBJECT_SAMPLE_FACTORS EM-36JN2-U-00-11601 ReCHARGE_S_62 Sample Type:Study Sample | Batch:1 Analysis Order=85; RAW_FILE_NAME=ReCHARGE_S_62 SUBJECT_SAMPLE_FACTORS EM-36VG6-U-00-11601 ReCHARGE_S_63 Sample Type:Study Sample | Batch:1 Analysis Order=86; RAW_FILE_NAME=ReCHARGE_S_63 SUBJECT_SAMPLE_FACTORS EM-36CB6-U-00-11601 ReCHARGE_S_64 Sample Type:Study Sample | Batch:1 Analysis Order=87; RAW_FILE_NAME=ReCHARGE_S_64 SUBJECT_SAMPLE_FACTORS EM-37EC0-U-00-11601 ReCHARGE_S_65 Sample Type:Study Sample | Batch:1 Analysis Order=88; RAW_FILE_NAME=ReCHARGE_S_65 SUBJECT_SAMPLE_FACTORS EM-36V89-U-00-11601 ReCHARGE_S_66 Sample Type:Study Sample | Batch:1 Analysis Order=89; RAW_FILE_NAME=ReCHARGE_S_66 SUBJECT_SAMPLE_FACTORS EM-37GU8-U-00-11601 ReCHARGE_S_67 Sample Type:Study Sample | Batch:1 Analysis Order=90; RAW_FILE_NAME=ReCHARGE_S_67 SUBJECT_SAMPLE_FACTORS EM-36MW0-U-00-11601 ReCHARGE_S_68 Sample Type:Study Sample | Batch:1 Analysis Order=91; RAW_FILE_NAME=ReCHARGE_S_68 SUBJECT_SAMPLE_FACTORS EM-36JQ6-U-00-11601 ReCHARGE_S_69 Sample Type:Study Sample | Batch:1 Analysis Order=92; RAW_FILE_NAME=ReCHARGE_S_69 SUBJECT_SAMPLE_FACTORS EM-36WP5-U-00-11601 ReCHARGE_S_7 Sample Type:Study Sample | Batch:1 Analysis Order=8; RAW_FILE_NAME=ReCHARGE_S_7 SUBJECT_SAMPLE_FACTORS EM-37168-U-00-11601 ReCHARGE_S_70 Sample Type:Study Sample | Batch:1 Analysis Order=93; RAW_FILE_NAME=ReCHARGE_S_70 SUBJECT_SAMPLE_FACTORS EM-37RJ1-U-00-11601 ReCHARGE_S_71 Sample Type:Study Sample | Batch:1 Analysis Order=98; RAW_FILE_NAME=ReCHARGE_S_71 SUBJECT_SAMPLE_FACTORS EM-37G17-U-00-11601 ReCHARGE_S_72 Sample Type:Study Sample | Batch:1 Analysis Order=99; RAW_FILE_NAME=ReCHARGE_S_72 SUBJECT_SAMPLE_FACTORS EM-36SG9-U-00-11601 ReCHARGE_S_73 Sample Type:Study Sample | Batch:1 Analysis Order=100; RAW_FILE_NAME=ReCHARGE_S_73 SUBJECT_SAMPLE_FACTORS EM-37YD7-U-00-11601 ReCHARGE_S_74 Sample Type:Study Sample | Batch:1 Analysis Order=101; RAW_FILE_NAME=ReCHARGE_S_74 SUBJECT_SAMPLE_FACTORS EM-36DV1-U-00-11601 ReCHARGE_S_75 Sample Type:Study Sample | Batch:1 Analysis Order=102; RAW_FILE_NAME=ReCHARGE_S_75 SUBJECT_SAMPLE_FACTORS EM-37B61-U-00-11601 ReCHARGE_S_76 Sample Type:Study Sample | Batch:1 Analysis Order=103; RAW_FILE_NAME=ReCHARGE_S_76 SUBJECT_SAMPLE_FACTORS EM-36CN9-U-00-11601 ReCHARGE_S_77 Sample Type:Study Sample | Batch:1 Analysis Order=104; RAW_FILE_NAME=ReCHARGE_S_77 SUBJECT_SAMPLE_FACTORS EM-37M37-U-00-11601 ReCHARGE_S_78 Sample Type:Study Sample | Batch:1 Analysis Order=105; RAW_FILE_NAME=ReCHARGE_S_78 SUBJECT_SAMPLE_FACTORS EM-37234-U-00-11601 ReCHARGE_S_79 Sample Type:Study Sample | Batch:1 Analysis Order=106; RAW_FILE_NAME=ReCHARGE_S_79 SUBJECT_SAMPLE_FACTORS EM-37B20-U-00-11601 ReCHARGE_S_8 Sample Type:Study Sample | Batch:1 Analysis Order=9; RAW_FILE_NAME=ReCHARGE_S_8 SUBJECT_SAMPLE_FACTORS EM-36EU2-U-00-11601 ReCHARGE_S_80 Sample Type:Study Sample | Batch:1 Analysis Order=107; RAW_FILE_NAME=ReCHARGE_S_80 SUBJECT_SAMPLE_FACTORS EM-37M03-U-00-11601 ReCHARGE_S_9 Sample Type:Study Sample | Batch:1 Analysis Order=10; RAW_FILE_NAME=ReCHARGE_S_9 SUBJECT_SAMPLE_FACTORS EM-36XG4-U-00-11601 ReCHARGE_S_100 Sample Type:Study Sample | Batch:2 Analysis Order=136; RAW_FILE_NAME=ReCHARGE_S_100 SUBJECT_SAMPLE_FACTORS EM-37TK7-U-00-11601 ReCHARGE_S_101 Sample Type:Study Sample | Batch:2 Analysis Order=140; RAW_FILE_NAME=ReCHARGE_S_101 SUBJECT_SAMPLE_FACTORS EM-36W13-U-00-11601 ReCHARGE_S_102 Sample Type:Study Sample | Batch:2 Analysis Order=141; RAW_FILE_NAME=ReCHARGE_S_102 SUBJECT_SAMPLE_FACTORS EM-37DE6-U-00-11601 ReCHARGE_S_103 Sample Type:Study Sample | Batch:2 Analysis Order=142; RAW_FILE_NAME=ReCHARGE_S_103 SUBJECT_SAMPLE_FACTORS EM-37CH1-U-00-11601 ReCHARGE_S_104 Sample Type:Study Sample | Batch:2 Analysis Order=143; RAW_FILE_NAME=ReCHARGE_S_104 SUBJECT_SAMPLE_FACTORS EM-37TL5-U-00-11601 ReCHARGE_S_105 Sample Type:Study Sample | Batch:2 Analysis Order=144; RAW_FILE_NAME=ReCHARGE_S_105 SUBJECT_SAMPLE_FACTORS EM-37HS1-U-00-11601 ReCHARGE_S_106 Sample Type:Study Sample | Batch:2 Analysis Order=145; RAW_FILE_NAME=ReCHARGE_S_106 SUBJECT_SAMPLE_FACTORS EM-372F2-U-00-11601 ReCHARGE_S_107 Sample Type:Study Sample | Batch:2 Analysis Order=146; RAW_FILE_NAME=ReCHARGE_S_107 SUBJECT_SAMPLE_FACTORS EM-36TW3-U-00-11601 ReCHARGE_S_108 Sample Type:Study Sample | Batch:2 Analysis Order=147; RAW_FILE_NAME=ReCHARGE_S_108 SUBJECT_SAMPLE_FACTORS EM-37MH1-U-00-11601 ReCHARGE_S_109 Sample Type:Study Sample | Batch:2 Analysis Order=148; RAW_FILE_NAME=ReCHARGE_S_109 SUBJECT_SAMPLE_FACTORS EM-37EH9-U-00-11601 ReCHARGE_S_110 Sample Type:Study Sample | Batch:2 Analysis Order=149; RAW_FILE_NAME=ReCHARGE_S_110 SUBJECT_SAMPLE_FACTORS EM-36P93-U-00-11601 ReCHARGE_S_111 Sample Type:Study Sample | Batch:2 Analysis Order=154; RAW_FILE_NAME=ReCHARGE_S_111 SUBJECT_SAMPLE_FACTORS EM-374Y8-U-00-11601 ReCHARGE_S_112 Sample Type:Study Sample | Batch:2 Analysis Order=155; RAW_FILE_NAME=ReCHARGE_S_112 SUBJECT_SAMPLE_FACTORS EM-36H75-U-00-11601 ReCHARGE_S_113 Sample Type:Study Sample | Batch:2 Analysis Order=156; RAW_FILE_NAME=ReCHARGE_S_113 SUBJECT_SAMPLE_FACTORS EM-379B4-U-00-11601 ReCHARGE_S_114 Sample Type:Study Sample | Batch:2 Analysis Order=157; RAW_FILE_NAME=ReCHARGE_S_114 SUBJECT_SAMPLE_FACTORS EM-36JE2-U-00-11601 ReCHARGE_S_115 Sample Type:Study Sample | Batch:2 Analysis Order=158; RAW_FILE_NAME=ReCHARGE_S_115 SUBJECT_SAMPLE_FACTORS EM-37CX5-U-00-11601 ReCHARGE_S_116 Sample Type:Study Sample | Batch:2 Analysis Order=159; RAW_FILE_NAME=ReCHARGE_S_116 SUBJECT_SAMPLE_FACTORS EM-36WD1-U-00-11601 ReCHARGE_S_117 Sample Type:Study Sample | Batch:2 Analysis Order=160; RAW_FILE_NAME=ReCHARGE_S_117 SUBJECT_SAMPLE_FACTORS EM-36KG7-U-00-11601 ReCHARGE_S_118 Sample Type:Study Sample | Batch:2 Analysis Order=161; RAW_FILE_NAME=ReCHARGE_S_118 SUBJECT_SAMPLE_FACTORS EM-37EF3-U-00-11601 ReCHARGE_S_119 Sample Type:Study Sample | Batch:2 Analysis Order=162; RAW_FILE_NAME=ReCHARGE_S_119 SUBJECT_SAMPLE_FACTORS EM-37GH7-U-00-11601 ReCHARGE_S_120 Sample Type:Study Sample | Batch:2 Analysis Order=163; RAW_FILE_NAME=ReCHARGE_S_120 SUBJECT_SAMPLE_FACTORS EM-36D38-U-00-11601 ReCHARGE_S_121 Sample Type:Study Sample | Batch:2 Analysis Order=168; RAW_FILE_NAME=ReCHARGE_S_121 SUBJECT_SAMPLE_FACTORS EM-36PV9-U-00-11601 ReCHARGE_S_122 Sample Type:Study Sample | Batch:2 Analysis Order=169; RAW_FILE_NAME=ReCHARGE_S_122 SUBJECT_SAMPLE_FACTORS EM-36KD3-U-00-11601 ReCHARGE_S_123 Sample Type:Study Sample | Batch:2 Analysis Order=170; RAW_FILE_NAME=ReCHARGE_S_123 SUBJECT_SAMPLE_FACTORS EM-37Y76-U-00-11601 ReCHARGE_S_124 Sample Type:Study Sample | Batch:2 Analysis Order=171; RAW_FILE_NAME=ReCHARGE_S_124 SUBJECT_SAMPLE_FACTORS EM-37VP4-U-00-11601 ReCHARGE_S_125 Sample Type:Study Sample | Batch:2 Analysis Order=172; RAW_FILE_NAME=ReCHARGE_S_125 SUBJECT_SAMPLE_FACTORS EM-370J5-U-00-11601 ReCHARGE_S_126 Sample Type:Study Sample | Batch:2 Analysis Order=173; RAW_FILE_NAME=ReCHARGE_S_126 SUBJECT_SAMPLE_FACTORS EM-37KY5-U-00-11601 ReCHARGE_S_127 Sample Type:Study Sample | Batch:2 Analysis Order=174; RAW_FILE_NAME=ReCHARGE_S_127 SUBJECT_SAMPLE_FACTORS EM-37Y43-U-00-11601 ReCHARGE_S_128 Sample Type:Study Sample | Batch:2 Analysis Order=175; RAW_FILE_NAME=ReCHARGE_S_128 SUBJECT_SAMPLE_FACTORS EM-371R7-U-00-11601 ReCHARGE_S_129 Sample Type:Study Sample | Batch:2 Analysis Order=176; RAW_FILE_NAME=ReCHARGE_S_129 SUBJECT_SAMPLE_FACTORS EM-37XS5-U-00-11601 ReCHARGE_S_130 Sample Type:Study Sample | Batch:2 Analysis Order=177; RAW_FILE_NAME=ReCHARGE_S_130 SUBJECT_SAMPLE_FACTORS EM-37CK4-U-00-11601 ReCHARGE_S_131 Sample Type:Study Sample | Batch:2 Analysis Order=182; RAW_FILE_NAME=ReCHARGE_S_131 SUBJECT_SAMPLE_FACTORS EM-36C96-U-00-11601 ReCHARGE_S_132 Sample Type:Study Sample | Batch:2 Analysis Order=183; RAW_FILE_NAME=ReCHARGE_S_132 SUBJECT_SAMPLE_FACTORS EM-37AX7-U-00-11601 ReCHARGE_S_133 Sample Type:Study Sample | Batch:2 Analysis Order=184; RAW_FILE_NAME=ReCHARGE_S_133 SUBJECT_SAMPLE_FACTORS EM-37317-U-00-11601 ReCHARGE_S_134 Sample Type:Study Sample | Batch:2 Analysis Order=185; RAW_FILE_NAME=ReCHARGE_S_134 SUBJECT_SAMPLE_FACTORS EM-37HQ6-U-00-11601 ReCHARGE_S_135 Sample Type:Study Sample | Batch:2 Analysis Order=186; RAW_FILE_NAME=ReCHARGE_S_135 SUBJECT_SAMPLE_FACTORS EM-36HC9-U-00-11601 ReCHARGE_S_136 Sample Type:Study Sample | Batch:2 Analysis Order=187; RAW_FILE_NAME=ReCHARGE_S_136 SUBJECT_SAMPLE_FACTORS EM-37242-U-00-11601 ReCHARGE_S_137 Sample Type:Study Sample | Batch:2 Analysis Order=188; RAW_FILE_NAME=ReCHARGE_S_137 SUBJECT_SAMPLE_FACTORS EM-36S74-U-00-11601 ReCHARGE_S_138 Sample Type:Study Sample | Batch:2 Analysis Order=189; RAW_FILE_NAME=ReCHARGE_S_138 SUBJECT_SAMPLE_FACTORS EM-37M45-U-00-11601 ReCHARGE_S_139 Sample Type:Study Sample | Batch:2 Analysis Order=190; RAW_FILE_NAME=ReCHARGE_S_139 SUBJECT_SAMPLE_FACTORS EM-37YC0-U-00-11601 ReCHARGE_S_140 Sample Type:Study Sample | Batch:2 Analysis Order=191; RAW_FILE_NAME=ReCHARGE_S_140 SUBJECT_SAMPLE_FACTORS EM-37RA1-U-00-11601 ReCHARGE_S_141 Sample Type:Study Sample | Batch:2 Analysis Order=195; RAW_FILE_NAME=ReCHARGE_S_141 SUBJECT_SAMPLE_FACTORS EM-36D20-U-00-11601 ReCHARGE_S_142 Sample Type:Study Sample | Batch:2 Analysis Order=196; RAW_FILE_NAME=ReCHARGE_S_142 SUBJECT_SAMPLE_FACTORS EM-37EG1-U-00-11601 ReCHARGE_S_143 Sample Type:Study Sample | Batch:2 Analysis Order=197; RAW_FILE_NAME=ReCHARGE_S_143 SUBJECT_SAMPLE_FACTORS EM-37BK5-U-00-11601 ReCHARGE_S_144 Sample Type:Study Sample | Batch:2 Analysis Order=198; RAW_FILE_NAME=ReCHARGE_S_144 SUBJECT_SAMPLE_FACTORS EM-36U07-U-00-11601 ReCHARGE_S_145 Sample Type:Study Sample | Batch:2 Analysis Order=199; RAW_FILE_NAME=ReCHARGE_S_145 SUBJECT_SAMPLE_FACTORS EM-37549-U-00-11601 ReCHARGE_S_146 Sample Type:Study Sample | Batch:2 Analysis Order=200; RAW_FILE_NAME=ReCHARGE_S_146 SUBJECT_SAMPLE_FACTORS EM-37LR0-U-00-11601 ReCHARGE_S_147 Sample Type:Study Sample | Batch:2 Analysis Order=201; RAW_FILE_NAME=ReCHARGE_S_147 SUBJECT_SAMPLE_FACTORS EM-37WN7-U-00-11601 ReCHARGE_S_148 Sample Type:Study Sample | Batch:2 Analysis Order=202; RAW_FILE_NAME=ReCHARGE_S_148 SUBJECT_SAMPLE_FACTORS EM-37RU7-U-00-11601 ReCHARGE_S_149 Sample Type:Study Sample | Batch:2 Analysis Order=203; RAW_FILE_NAME=ReCHARGE_S_149 SUBJECT_SAMPLE_FACTORS EM-37CU2-U-00-11601 ReCHARGE_S_150 Sample Type:Study Sample | Batch:2 Analysis Order=204; RAW_FILE_NAME=ReCHARGE_S_150 SUBJECT_SAMPLE_FACTORS EM-37MF5-U-00-11601 ReCHARGE_S_151 Sample Type:Study Sample | Batch:2 Analysis Order=209; RAW_FILE_NAME=ReCHARGE_S_151 SUBJECT_SAMPLE_FACTORS EM-36FE6-U-00-11601 ReCHARGE_S_152 Sample Type:Study Sample | Batch:2 Analysis Order=210; RAW_FILE_NAME=ReCHARGE_S_152 SUBJECT_SAMPLE_FACTORS EM-36RA3-U-00-11601 ReCHARGE_S_153 Sample Type:Study Sample | Batch:2 Analysis Order=211; RAW_FILE_NAME=ReCHARGE_S_153 SUBJECT_SAMPLE_FACTORS EM-374K9-U-00-11601 ReCHARGE_S_154 Sample Type:Study Sample | Batch:2 Analysis Order=212; RAW_FILE_NAME=ReCHARGE_S_154 SUBJECT_SAMPLE_FACTORS EM-37572-U-00-11601 ReCHARGE_S_155 Sample Type:Study Sample | Batch:2 Analysis Order=213; RAW_FILE_NAME=ReCHARGE_S_155 SUBJECT_SAMPLE_FACTORS EM-37TY6-U-00-11601 ReCHARGE_S_156 Sample Type:Study Sample | Batch:2 Analysis Order=214; RAW_FILE_NAME=ReCHARGE_S_156 SUBJECT_SAMPLE_FACTORS EM-36KK8-U-00-11601 ReCHARGE_S_157 Sample Type:Study Sample | Batch:2 Analysis Order=215; RAW_FILE_NAME=ReCHARGE_S_157 SUBJECT_SAMPLE_FACTORS EM-37K39-U-00-11601 ReCHARGE_S_158 Sample Type:Study Sample | Batch:2 Analysis Order=216; RAW_FILE_NAME=ReCHARGE_S_158 SUBJECT_SAMPLE_FACTORS EM-36YG3-U-00-11601 ReCHARGE_S_159 Sample Type:Study Sample | Batch:2 Analysis Order=217; RAW_FILE_NAME=ReCHARGE_S_159 SUBJECT_SAMPLE_FACTORS EM-36L89-U-00-11601 ReCHARGE_S_160 Sample Type:Study Sample | Batch:2 Analysis Order=218; RAW_FILE_NAME=ReCHARGE_S_160 SUBJECT_SAMPLE_FACTORS EM-36JS1-U-00-11601 ReCHARGE_S_81 Sample Type:Study Sample | Batch:2 Analysis Order=113; RAW_FILE_NAME=ReCHARGE_S_81 SUBJECT_SAMPLE_FACTORS EM-36J57-U-00-11601 ReCHARGE_S_82 Sample Type:Study Sample | Batch:2 Analysis Order=114; RAW_FILE_NAME=ReCHARGE_S_82 SUBJECT_SAMPLE_FACTORS EM-37AH3-U-00-11601 ReCHARGE_S_83 Sample Type:Study Sample | Batch:2 Analysis Order=115; RAW_FILE_NAME=ReCHARGE_S_83 SUBJECT_SAMPLE_FACTORS EM-37NR8-U-00-11601 ReCHARGE_S_84 Sample Type:Study Sample | Batch:2 Analysis Order=116; RAW_FILE_NAME=ReCHARGE_S_84 SUBJECT_SAMPLE_FACTORS EM-36RT1-U-00-11601 ReCHARGE_S_85 Sample Type:Study Sample | Batch:2 Analysis Order=117; RAW_FILE_NAME=ReCHARGE_S_85 SUBJECT_SAMPLE_FACTORS EM-36VR2-U-00-11601 ReCHARGE_S_86 Sample Type:Study Sample | Batch:2 Analysis Order=118; RAW_FILE_NAME=ReCHARGE_S_86 SUBJECT_SAMPLE_FACTORS EM-371W6-U-00-11601 ReCHARGE_S_87 Sample Type:Study Sample | Batch:2 Analysis Order=119; RAW_FILE_NAME=ReCHARGE_S_87 SUBJECT_SAMPLE_FACTORS EM-37HF0-U-00-11601 ReCHARGE_S_88 Sample Type:Study Sample | Batch:2 Analysis Order=120; RAW_FILE_NAME=ReCHARGE_S_88 SUBJECT_SAMPLE_FACTORS EM-375H5-U-00-11601 ReCHARGE_S_89 Sample Type:Study Sample | Batch:2 Analysis Order=121; RAW_FILE_NAME=ReCHARGE_S_89 SUBJECT_SAMPLE_FACTORS EM-37G33-U-00-11601 ReCHARGE_S_90 Sample Type:Study Sample | Batch:2 Analysis Order=122; RAW_FILE_NAME=ReCHARGE_S_90 SUBJECT_SAMPLE_FACTORS EM-37A05-U-00-11601 ReCHARGE_S_91 Sample Type:Study Sample | Batch:2 Analysis Order=127; RAW_FILE_NAME=ReCHARGE_S_91 SUBJECT_SAMPLE_FACTORS EM-374V5-U-00-11601 ReCHARGE_S_92 Sample Type:Study Sample | Batch:2 Analysis Order=128; RAW_FILE_NAME=ReCHARGE_S_92 SUBJECT_SAMPLE_FACTORS EM-36WG5-U-00-11601 ReCHARGE_S_93 Sample Type:Study Sample | Batch:2 Analysis Order=129; RAW_FILE_NAME=ReCHARGE_S_93 SUBJECT_SAMPLE_FACTORS EM-372W5-U-00-11601 ReCHARGE_S_94 Sample Type:Study Sample | Batch:2 Analysis Order=130; RAW_FILE_NAME=ReCHARGE_S_94 SUBJECT_SAMPLE_FACTORS EM-36QE5-U-00-11601 ReCHARGE_S_95 Sample Type:Study Sample | Batch:2 Analysis Order=131; RAW_FILE_NAME=ReCHARGE_S_95 SUBJECT_SAMPLE_FACTORS EM-36GH9-U-00-11601 ReCHARGE_S_96 Sample Type:Study Sample | Batch:2 Analysis Order=132; RAW_FILE_NAME=ReCHARGE_S_96 SUBJECT_SAMPLE_FACTORS EM-36CM2-U-00-11601 ReCHARGE_S_97 Sample Type:Study Sample | Batch:2 Analysis Order=133; RAW_FILE_NAME=ReCHARGE_S_97 SUBJECT_SAMPLE_FACTORS EM-37FL9-U-00-11601 ReCHARGE_S_98 Sample Type:Study Sample | Batch:2 Analysis Order=134; RAW_FILE_NAME=ReCHARGE_S_98 SUBJECT_SAMPLE_FACTORS EM-36NT5-U-00-11601 ReCHARGE_S_99 Sample Type:Study Sample | Batch:2 Analysis Order=135; RAW_FILE_NAME=ReCHARGE_S_99 SUBJECT_SAMPLE_FACTORS EM-37SF9-U-00-11601 ReCHARGE_S_161 Sample Type:Study Sample | Batch:3 Analysis Order=224; RAW_FILE_NAME=ReCHARGE_S_161 SUBJECT_SAMPLE_FACTORS EM-37MA6-U-00-11601 ReCHARGE_S_162 Sample Type:Study Sample | Batch:3 Analysis Order=225; RAW_FILE_NAME=ReCHARGE_S_162 SUBJECT_SAMPLE_FACTORS EM-37LQ2-U-00-11601 ReCHARGE_S_163 Sample Type:Study Sample | Batch:3 Analysis Order=226; RAW_FILE_NAME=ReCHARGE_S_163 SUBJECT_SAMPLE_FACTORS EM-36K56-U-00-11601 ReCHARGE_S_164 Sample Type:Study Sample | Batch:3 Analysis Order=227; RAW_FILE_NAME=ReCHARGE_S_164 SUBJECT_SAMPLE_FACTORS EM-37K62-U-00-11601 ReCHARGE_S_165 Sample Type:Study Sample | Batch:3 Analysis Order=228; RAW_FILE_NAME=ReCHARGE_S_165 SUBJECT_SAMPLE_FACTORS EM-37FT1-U-00-11601 ReCHARGE_S_166 Sample Type:Study Sample | Batch:3 Analysis Order=229; RAW_FILE_NAME=ReCHARGE_S_166 SUBJECT_SAMPLE_FACTORS EM-37Q33-U-00-11601 ReCHARGE_S_167 Sample Type:Study Sample | Batch:3 Analysis Order=230; RAW_FILE_NAME=ReCHARGE_S_167 SUBJECT_SAMPLE_FACTORS EM-36Z51-U-00-11601 ReCHARGE_S_168 Sample Type:Study Sample | Batch:3 Analysis Order=231; RAW_FILE_NAME=ReCHARGE_S_168 SUBJECT_SAMPLE_FACTORS EM-374D4-U-00-11601 ReCHARGE_S_169 Sample Type:Study Sample | Batch:3 Analysis Order=232; RAW_FILE_NAME=ReCHARGE_S_169 SUBJECT_SAMPLE_FACTORS EM-36V63-U-00-11601 ReCHARGE_S_170 Sample Type:Study Sample | Batch:3 Analysis Order=233; RAW_FILE_NAME=ReCHARGE_S_170 SUBJECT_SAMPLE_FACTORS EM-36VP6-U-00-11601 ReCHARGE_S_171 Sample Type:Study Sample | Batch:3 Analysis Order=237; RAW_FILE_NAME=ReCHARGE_S_171 SUBJECT_SAMPLE_FACTORS EM-375T8-U-00-11601 ReCHARGE_S_172 Sample Type:Study Sample | Batch:3 Analysis Order=238; RAW_FILE_NAME=ReCHARGE_S_172 SUBJECT_SAMPLE_FACTORS EM-37QA2-U-00-11601 ReCHARGE_S_173 Sample Type:Study Sample | Batch:3 Analysis Order=239; RAW_FILE_NAME=ReCHARGE_S_173 SUBJECT_SAMPLE_FACTORS EM-36SK0-U-00-11601 ReCHARGE_S_174 Sample Type:Study Sample | Batch:3 Analysis Order=240; RAW_FILE_NAME=ReCHARGE_S_174 SUBJECT_SAMPLE_FACTORS EM-372R6-U-00-11601 ReCHARGE_S_175 Sample Type:Study Sample | Batch:3 Analysis Order=241; RAW_FILE_NAME=ReCHARGE_S_175 SUBJECT_SAMPLE_FACTORS EM-379V0-U-00-11601 ReCHARGE_S_176 Sample Type:Study Sample | Batch:3 Analysis Order=242; RAW_FILE_NAME=ReCHARGE_S_176 SUBJECT_SAMPLE_FACTORS EM-36N53-U-00-11601 ReCHARGE_S_177 Sample Type:Study Sample | Batch:3 Analysis Order=243; RAW_FILE_NAME=ReCHARGE_S_177 SUBJECT_SAMPLE_FACTORS EM-36RU9-U-00-11601 ReCHARGE_S_178 Sample Type:Study Sample | Batch:3 Analysis Order=244; RAW_FILE_NAME=ReCHARGE_S_178 SUBJECT_SAMPLE_FACTORS EM-37AN9-U-00-11601 ReCHARGE_S_179 Sample Type:Study Sample | Batch:3 Analysis Order=245; RAW_FILE_NAME=ReCHARGE_S_179 SUBJECT_SAMPLE_FACTORS EM-37WP3-U-00-11601 ReCHARGE_S_180 Sample Type:Study Sample | Batch:3 Analysis Order=246; RAW_FILE_NAME=ReCHARGE_S_180 SUBJECT_SAMPLE_FACTORS EM-37L38-U-00-11601 ReCHARGE_S_181 Sample Type:Study Sample | Batch:3 Analysis Order=250; RAW_FILE_NAME=ReCHARGE_S_181 SUBJECT_SAMPLE_FACTORS EM-36KA0-U-00-11601 ReCHARGE_S_182 Sample Type:Study Sample | Batch:3 Analysis Order=251; RAW_FILE_NAME=ReCHARGE_S_182 SUBJECT_SAMPLE_FACTORS EM-378N8-U-00-11601 ReCHARGE_S_183 Sample Type:Study Sample | Batch:3 Analysis Order=252; RAW_FILE_NAME=ReCHARGE_S_183 SUBJECT_SAMPLE_FACTORS EM-36YJ6-U-00-11601 ReCHARGE_S_184 Sample Type:Study Sample | Batch:3 Analysis Order=253; RAW_FILE_NAME=ReCHARGE_S_184 SUBJECT_SAMPLE_FACTORS EM-36QK2-U-00-11601 ReCHARGE_S_185 Sample Type:Study Sample | Batch:3 Analysis Order=254; RAW_FILE_NAME=ReCHARGE_S_185 SUBJECT_SAMPLE_FACTORS EM-37GT0-U-00-11601 ReCHARGE_S_186 Sample Type:Study Sample | Batch:3 Analysis Order=255; RAW_FILE_NAME=ReCHARGE_S_186 SUBJECT_SAMPLE_FACTORS EM-37CV0-U-00-11601 ReCHARGE_S_187 Sample Type:Study Sample | Batch:3 Analysis Order=256; RAW_FILE_NAME=ReCHARGE_S_187 SUBJECT_SAMPLE_FACTORS EM-36ET4-U-00-11601 ReCHARGE_S_188 Sample Type:Study Sample | Batch:3 Analysis Order=257; RAW_FILE_NAME=ReCHARGE_S_188 SUBJECT_SAMPLE_FACTORS EM-37RM5-U-00-11601 ReCHARGE_S_189 Sample Type:Study Sample | Batch:3 Analysis Order=258; RAW_FILE_NAME=ReCHARGE_S_189 SUBJECT_SAMPLE_FACTORS EM-36YT4-U-00-11601 ReCHARGE_S_190 Sample Type:Study Sample | Batch:3 Analysis Order=259; RAW_FILE_NAME=ReCHARGE_S_190 SUBJECT_SAMPLE_FACTORS EM-37U54-U-00-11601 ReCHARGE_S_191 Sample Type:Study Sample | Batch:3 Analysis Order=264; RAW_FILE_NAME=ReCHARGE_S_191 SUBJECT_SAMPLE_FACTORS EM-36FM9-U-00-11601 ReCHARGE_S_192 Sample Type:Study Sample | Batch:3 Analysis Order=265; RAW_FILE_NAME=ReCHARGE_S_192 SUBJECT_SAMPLE_FACTORS EM-36R59-U-00-11601 ReCHARGE_S_193 Sample Type:Study Sample | Batch:3 Analysis Order=266; RAW_FILE_NAME=ReCHARGE_S_193 SUBJECT_SAMPLE_FACTORS EM-36GP1-U-00-11601 ReCHARGE_S_194 Sample Type:Study Sample | Batch:3 Analysis Order=267; RAW_FILE_NAME=ReCHARGE_S_194 SUBJECT_SAMPLE_FACTORS EM-37HL7-U-00-11601 ReCHARGE_S_195 Sample Type:Study Sample | Batch:3 Analysis Order=268; RAW_FILE_NAME=ReCHARGE_S_195 SUBJECT_SAMPLE_FACTORS EM-37564-U-00-11601 ReCHARGE_S_196 Sample Type:Study Sample | Batch:3 Analysis Order=269; RAW_FILE_NAME=ReCHARGE_S_196 SUBJECT_SAMPLE_FACTORS EM-36R75-U-00-11601 ReCHARGE_S_197 Sample Type:Study Sample | Batch:3 Analysis Order=270; RAW_FILE_NAME=ReCHARGE_S_197 SUBJECT_SAMPLE_FACTORS EM-37LC3-U-00-11601 ReCHARGE_S_198 Sample Type:Study Sample | Batch:3 Analysis Order=271; RAW_FILE_NAME=ReCHARGE_S_198 SUBJECT_SAMPLE_FACTORS EM-37YJ4-U-00-11601 ReCHARGE_S_199 Sample Type:Study Sample | Batch:3 Analysis Order=272; RAW_FILE_NAME=ReCHARGE_S_199 SUBJECT_SAMPLE_FACTORS EM-37Q74-U-00-11601 ReCHARGE_S_200 Sample Type:Study Sample | Batch:3 Analysis Order=273; RAW_FILE_NAME=ReCHARGE_S_200 SUBJECT_SAMPLE_FACTORS EM-36ZH0-U-00-11601 ReCHARGE_S_201 Sample Type:Study Sample | Batch:3 Analysis Order=278; RAW_FILE_NAME=ReCHARGE_S_201 SUBJECT_SAMPLE_FACTORS EM-37LP4-U-00-11601 ReCHARGE_S_202 Sample Type:Study Sample | Batch:3 Analysis Order=279; RAW_FILE_NAME=ReCHARGE_S_202 SUBJECT_SAMPLE_FACTORS EM-36H67-U-00-11601 ReCHARGE_S_203 Sample Type:Study Sample | Batch:3 Analysis Order=280; RAW_FILE_NAME=ReCHARGE_S_203 SUBJECT_SAMPLE_FACTORS EM-371A4-U-00-11601 ReCHARGE_S_204 Sample Type:Study Sample | Batch:3 Analysis Order=281; RAW_FILE_NAME=ReCHARGE_S_204 SUBJECT_SAMPLE_FACTORS EM-37TH4-U-00-11601 ReCHARGE_S_205 Sample Type:Study Sample | Batch:3 Analysis Order=282; RAW_FILE_NAME=ReCHARGE_S_205 SUBJECT_SAMPLE_FACTORS EM-37598-U-00-11601 ReCHARGE_S_206 Sample Type:Study Sample | Batch:3 Analysis Order=283; RAW_FILE_NAME=ReCHARGE_S_206 SUBJECT_SAMPLE_FACTORS EM-37S49-U-00-11601 ReCHARGE_S_207 Sample Type:Study Sample | Batch:3 Analysis Order=284; RAW_FILE_NAME=ReCHARGE_S_207 SUBJECT_SAMPLE_FACTORS EM-371X3-U-00-11601 ReCHARGE_S_208 Sample Type:Study Sample | Batch:3 Analysis Order=285; RAW_FILE_NAME=ReCHARGE_S_208 SUBJECT_SAMPLE_FACTORS EM-375L6-U-00-11601 ReCHARGE_S_209 Sample Type:Study Sample | Batch:3 Analysis Order=286; RAW_FILE_NAME=ReCHARGE_S_209 SUBJECT_SAMPLE_FACTORS EM-374C7-U-00-11601 ReCHARGE_S_210 Sample Type:Study Sample | Batch:3 Analysis Order=287; RAW_FILE_NAME=ReCHARGE_S_210 SUBJECT_SAMPLE_FACTORS EM-36KX9-U-00-11601 ReCHARGE_S_211 Sample Type:Study Sample | Batch:3 Analysis Order=292; RAW_FILE_NAME=ReCHARGE_S_211 SUBJECT_SAMPLE_FACTORS EM-36F02-U-00-11601 ReCHARGE_S_212 Sample Type:Study Sample | Batch:3 Analysis Order=293; RAW_FILE_NAME=ReCHARGE_S_212 SUBJECT_SAMPLE_FACTORS EM-37QS2-U-00-11601 ReCHARGE_S_213 Sample Type:Study Sample | Batch:3 Analysis Order=294; RAW_FILE_NAME=ReCHARGE_S_213 #COLLECTION CO:COLLECTION_SUMMARY NA CO:SAMPLE_TYPE Urine CO:STORAGE_CONDITIONS -80℃ #TREATMENT TR:TREATMENT_SUMMARY NA #SAMPLEPREP SP:SAMPLEPREP_SUMMARY Study samples (2 mL aliquots) were shipped from the University of California, SP:SAMPLEPREP_SUMMARY Davis to the NC HHEAR Hub on dry ice. The NC HHEAR Hub thawed and transferred 50 SP:SAMPLEPREP_SUMMARY µL of the study samples to a new set of tubes and used them for the analysis. SP:SAMPLEPREP_SUMMARY An additional 10 µL was taken from the original study sample and transferred to SP:SAMPLEPREP_SUMMARY another tube to make the total study pool for this project, and then distributed SP:SAMPLEPREP_SUMMARY with 50 µL per aliquot, used as quality control study pools (QC study pools) SP:SAMPLEPREP_SUMMARY throughout the whole analysis. All sample aliquots (50 µL each) and QC study SP:SAMPLEPREP_SUMMARY pools (50 µL each) were stored at -80° C until the day of sample preparation. SP:SAMPLEPREP_SUMMARY HHEAR Urine Pool 1 (50 µL each), HHEAR Urine Pool 2 (50 µL each), CHEAR SP:SAMPLEPREP_SUMMARY reference urine (50 µL each) and NIST urine (SRM 3672) reference material (50 SP:SAMPLEPREP_SUMMARY µL each) were provided by the NC HHEAR Hub. LC-MS grade water (50 µL) was used SP:SAMPLEPREP_SUMMARY as blanks. All samples were thawed at 4°C overnight before the preparation. SP:SAMPLEPREP_SUMMARY Samples, including study samples, study pool samples, HHEAR reference urine, SP:SAMPLEPREP_SUMMARY CHEAR reference urine, NIST reference urine, and blanks were mixed with 400 µL SP:SAMPLEPREP_SUMMARY methanol containing 500 ng/mL tryptophan-d5 as internal standard and vortexed by SP:SAMPLEPREP_SUMMARY a multiple tube vortex mixer for 2 min at 5000 rpm at room temperature. All SP:SAMPLEPREP_SUMMARY samples were centrifuged at 16,000 rcf for 10 min at 4°C. The supernatant (350 SP:SAMPLEPREP_SUMMARY µL) was transferred into a pre-labeled 2.0 mL Lo-bind Eppendorf tube, dried by SP:SAMPLEPREP_SUMMARY a SpeedVac overnight, and stored at -80° C. For immediate analysis, 100 µL of SP:SAMPLEPREP_SUMMARY water-methanol solution (95:5, v/v) was used to reconstitute the dried extracts. SP:SAMPLEPREP_SUMMARY Samples were thoroughly mixed on a multiple tube vortex mixer for 10 min at 5000 SP:SAMPLEPREP_SUMMARY rpm at room temperature and then centrifuged at 4°C for 10 min at 16,000 rcf. SP:SAMPLEPREP_SUMMARY The supernatant was transferred to pre-labeled autosampler vials for data SP:SAMPLEPREP_SUMMARY acquisition by LC-MS. SP:PROCESSING_STORAGE_CONDITIONS 4℃ SP:EXTRACTION_METHOD Vortex with methanol containing 500ng/ml tryptophan-d5 as internal standard SP:EXTRACT_STORAGE -80℃ SP:SAMPLE_RESUSPENSION Water-Methanol (95:5, v/v) SP:SAMPLE_SPIKING Tryptophan-d5 stock solution at 500 ng/mL #CHROMATOGRAPHY CH:CHROMATOGRAPHY_SUMMARY Reverse phase CH:INSTRUMENT_NAME Thermo Vanquish CH:COLUMN_NAME Waters ACQUITY UPLC HSS T3 (100 x 2.1mm,1.8um) CH:COLUMN_PRESSURE 6000-10000 CH:COLUMN_TEMPERATURE 50 oC CH:FLOW_GRADIENT Time(min) Flow Rate %A %B Curve 1. 0 0.4 99.0 1.0 5 2. 1.00 0.4 99.0 1.0 5 3. CH:FLOW_GRADIENT 16.00 0.4 1.0 99.0 5 4. 19.00 0.4 1.0 99.0 5 5. 19.50 0.4 99.0 1.0 5 6. 22.00 CH:FLOW_GRADIENT 0.4 99.0 1.0 5 CH:FLOW_RATE 0.4 mL/min CH:INJECTION_TEMPERATURE 8oC CH:SOLVENT_A 100% water; 0.1% formic acid CH:SOLVENT_B 100% methanol; 0.1% formic acid CH:ANALYTICAL_TIME 22 min CH:CHROMATOGRAPHY_TYPE Reversed phase #ANALYSIS AN:LABORATORY_NAME Sumner Lab, UNC-CH AN:ANALYSIS_TYPE MS AN:ACQUISITION_DATE 11/30/22-12/05/22 AN:SOFTWARE_VERSION Xcalibur 4.1.31.9 AN:DETECTOR_TYPE Orbitrap AN:DATA_FORMAT Profile #MS MS:INSTRUMENT_NAME Thermo Q Exactive HF-X Orbitrap MS:INSTRUMENT_TYPE Orbitrap MS:MS_TYPE ESI MS:MS_COMMENTS Instrument: Thermo Q Exactive HFx Software: Xcalibur 4.1.31.9 for data MS:MS_COMMENTS acquisition; Progenesis QI 2.4 for data preprocessing MS:ION_MODE POSITIVE MS:CAPILLARY_TEMPERATURE 320 °C MS:CAPILLARY_VOLTAGE 3.5 KV MS:COLLISION_ENERGY 20-45, ramp MS:COLLISION_GAS N2 MS:DRY_GAS_FLOW 55 MS:DRY_GAS_TEMP 400°C MS:FRAGMENT_VOLTAGE ES+ MS:FRAGMENTATION_METHOD CID MS:ION_SPRAY_VOLTAGE 3.5kV MS:IONIZATION ES+ MS:MASS_ACCURACY 5 ppm MS:DATAFORMAT Profile MS:DESOLVATION_GAS_FLOW 55 MS:DESOLVATION_TEMPERATURE 400 oC MS:MS_RESULTS_FILE ST002501_AN004110_Results.txt UNITS:m/z Has m/z:Yes Has RT:Yes RT units:Minutes #END