

                                INSTRUMENT CONTROL PARAMETERS:    5975C Inert XL MSD with Triple A
                                ------------------------------------------------------------------

   D:\METHODS\ALPHA KETO ACIDS-full.M
      Thu Sep 25 12:29:36 2014

Control Information
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Sample Inlet      :  GC
Injection Source  :  CTC PAL ALS
Mass Spectrometer :  Enabled

============================================================================
                                CTCPAL METHOD
============================================================================
                    Injection Volume: 1.00 ul
                        Syringe Size: 10ul
                          Cycle File: GC-Inj

                                CYCLE DETAILS
                               ---------------
                     Air Volume (µl): 0
         Pre Clean with Solvent 1 (): 3
         Pre Clean with Solvent 2 (): 3
            Pre Clean with Sample (): 0
                Filling Speed (µl/s): 5
                  Filling Strokes (): 6
                           Inject to: GC Inj1
              Injection Speed (µl/s): 100
               Pre Inject Delay (ms): 500
              Post Inject Delay (ms): 500
        Post Clean with Solvent 1 (): 3
        Post Clean with Solvent 2 (): 3
Oven
Equilibration Time                           0 min
Oven Program                                 On
    70 °C for 2 min
    then 25 °C/min to 300 °C for 2 min
Run Time                                     13.2 min






Front SS Inlet He
Mode                                         Split
Heater                                       On    260 °C
Pressure                                     On    9.9557 psi
Total Flow                                   On    15.1 mL/min
Septum Purge Flow                            On    3 mL/min
Gas Saver                                    On    20 mL/min After 2 min
Split Ratio                                  10 :1
Split Flow                                   11 mL/min


Thermal Aux 2 {MSD Transfer Line}
Heater                                       On
Temperature Program                          On
    320 °C for 0 min
Run Time                                     13.2 min


Column #1
DB-5MS + DG Part number 122-55: 2786.52816
DB-5MS + DG Part number 122-55
500 °C: 30 m x 250 µm x 0.25 µm
In: Front SS Inlet He
Out: Vacuum

(Initial)                                    70 °C
Pressure                                     9.9557 psi
Flow                                         1.1 mL/min
Average Velocity                             38.592 cm/sec
Holdup Time                                  1.2956 min
Flow Program                                 On
    1.1 mL/min for 0 min
Run Time                                     13.2 min











Aux EPC 1 N2
Aux EPC 2 N2
Aux EPC 3 N2



Signals
 Test Plot                                   Save Off
                                             50 Hz
 Test Plot                                   Save Off
                                             50 Hz
 Test Plot                                   Save Off
                                             50 Hz
 Test Plot                                   Save Off
                                             50 Hz


                                MS ACQUISITION PARAMETERS


General Information
------- -----------

Tune File                : air.u
Acquistion Mode          : Scan


MS Information
-- -----------

Solvent Delay            : 5.20 min

EMV Mode                 : Gain Factor
Gain Factor              : 1.00
Resulting EM Voltage     : 1318

[Scan Parameters]

Low Mass                 : 50.0
High Mass                : 500.0
Threshold                : 150
Sample #                 : 2       A/D Samples    4

[MSZones]

MS Source                : 230 C   maximum 250 C
MS Quad                  : 150 C   maximum 200 C


                             END OF MS ACQUISITION PARAMETERS


                              TUNE PARAMETERS for SN: US80838766
                        -----------------------------

 Trace Ion Detection is OFF.

 EMISSION    :      34.610
 ENERGY      :      69.922
 REPELLER    :      20.071
 IONFOCUS    :      84.463
 ENTRANCE_LE :      32.000
 EMVOLTS     :    1352.941
                               Actual EMV  :    1305.88
                               GAIN FACTOR :       0.90
 AMUGAIN     :    2047.000
 AMUOFFSET   :     117.375
 FILAMENT    :       1.000
 DCPOLARITY  :       0.000
 ENTLENSOFFS :      15.561
 MASSGAIN    :    -455.000   
 MASSOFFSET  :     -38.000   

                           END OF TUNE PARAMETERS
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                                               END OF INSTRUMENT CONTROL PARAMETERS
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