                                           INSTRUMENT CONTROL PARAMETERS:    GC-MS
                                           ---------------------------------------

   C:\MSDCHEM\1\METHODS\WAXPLUS_100-200C_2_SIM.M
      Tue Nov 25 12:55:12 2014

Control Information
------- -----------

Sample Inlet      :  GC
Injection Source  :  GC ALS
Mass Spectrometer :  Enabled


 No Sample Prep method has been assigned to this method.

=============================================================================
                                6890 GC METHOD
=============================================================================

OVEN
   Initial temp:  100 'C (On)              Maximum temp:  320 'C
   Initial time:  0.00 min                 Equilibration time:  1.00 min
   Ramps:
      #  Rate  Final temp  Final time
      1 20.00      210        2.00
      2   0.0(Off)
   Post temp:  0 'C
   Post time:  0.00 min
   Run time:  7.50 min

FRONT INLET (SPLIT/SPLITLESS)           BACK INLET (COOL ON COLUMN)
   Mode:  Split                            Mode:  Oven track
   Initial temp:  200 'C (On)              Pressure:  0.00 psi (Off)
   Pressure:  10.75 psi (On)               Gas type:  Helium
   Split ratio:  50:1
   Split flow:  50.9 mL/min
   Total flow:  54.9 mL/min
   Gas saver:  On
   Saver flow:  15.0 mL/min
   Saver time:  0.75 min
   Gas type:  Helium

COLUMN 1                                COLUMN 2
   Capillary Column                        (not installed)
   Model Number:  Phenomen ZB-WAXplus
   Poly-WAX MS compatible
   Max temperature:  250 'C
   Nominal length:  30.0 m
   Nominal diameter:  250.00 um
   Nominal film thickness:  0.25 um
   Mode:  constant flow
   Initial flow:  1.0 mL/min
   Nominal init pressure:  10.76 psi
   Average velocity:  38 cm/sec
   Inlet:  Front Inlet
   Outlet:  MSD
   Outlet pressure:  vacuum

FRONT DETECTOR (NO DET)                 BACK DETECTOR (NO DET)

SIGNAL 1                                SIGNAL 2
   Data rate:  20 Hz                       Data rate:  20 Hz
   Type:  test plot                        Type:  test plot
   Save Data:  Off                         Save Data:  Off
   Zero:  0.0 (Off)                        Zero:  0.0 (Off)
   Range:  0                               Range:  0
   Fast Peaks:  Off                        Fast Peaks:  Off
   Attenuation:  0                         Attenuation:  0

COLUMN COMP 1                           COLUMN COMP 2
   (No Detectors Installed)                (No Detectors Installed)

THERMAL AUX 2
   Use:  MSD Transfer Line Heater
   Description:
   Initial temp:  210 'C (On)
   Initial time:  0.00 min
      #  Rate  Final temp  Final time
      1   0.0(Off)

                                        POST RUN
                                           Post Time: 0.00 min

TIME TABLE
   Time       Specifier                     Parameter & Setpoint


                               GC Injector


     Front Injector:
        Sample Washes                 0
        Sample Pumps                  3
        Injection Volume           1.00 microliters
        Syringe Size               10.0 microliters
        PreInj Solvent A Washes       1
        PreInj Solvent B Washes       1
        PostInj Solvent A Washes      1
        PostInj Solvent B Washes      1
        Viscosity Delay               0 seconds
        Plunger Speed              Fast
        PreInjection Dwell         0.00 minutes
        PostInjection Dwell        0.00 minutes


     Back Injector:
No parameters specified

 Column 1 Inventory Number : CE003
 Column 2 Inventory Number :  

                                MS ACQUISITION PARAMETERS


General Information
------- -----------

Tune File                : atune.u
Acquistion Mode          : SIM


MS Information
-- -----------

Solvent Delay            : 1.80 min

EMV Mode                 : Gain Factor
Gain Factor              : 1.00
Resulting EM Voltage     : 1541

[Sim Parameters]

GROUP 1
Group ID                 : 1
Resolution               : Low
Plot 1 Ion               : 60.00
Ions/Dwell In Group      (  Mass,  Dwell) (  Mass,  Dwell) (  Mass,  Dwell) 
                         ( 43.00,    100) ( 60.00,    100) ( 62.00,    100) 
                         ( 63.00,    100) ( 64.00,    100) ( 74.00,    100) 

[MSZones]

MS Source                : 230 C   maximum 250 C
MS Quad                  : 150 C   maximum 200 C


                             END OF MS ACQUISITION PARAMETERS


                              TUNE PARAMETERS for SN: US43130477
                        -----------------------------

 Trace Ion Detection is OFF.

 EMISSION    :      34.610
 ENERGY      :      69.922
 REPELLER    :      24.092
 IONFOCUS    :      90.157
 ENTRANCE_LE :      21.500
 EMVOLTS     :    1376.471
                               Actual EMV  :    1541.18
                               GAIN FACTOR :       1.03
 AMUGAIN     :    2551.000
 AMUOFFSET   :     126.000
 FILAMENT    :       2.000
 DCPOLARITY  :       0.000
 ENTLENSOFFS :      17.569
 MASSGAIN    :     547.000   
 MASSOFFSET  :     -11.000   

                           END OF TUNE PARAMETERS
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                                             END OF INSTRUMENT CONTROL PARAMETERS
                                             ------------------------------------
