

                                INSTRUMENT CONTROL PARAMETERS:    5975C Inert XL MSD with Triple A
                                ------------------------------------------------------------------

   D:\METHODS\LZ OF FIEHN 2.M
      Tue Sep 23 17:58:46 2014

Control Information
------- -----------

Sample Inlet      :  GC
Injection Source  :  CTC PAL ALS
Mass Spectrometer :  Enabled

============================================================================
                                CTCPAL METHOD
============================================================================
                    Injection Volume: 2.00 ul
                        Syringe Size: 10ul
                          Cycle File: GC-Inj

                                CYCLE DETAILS
                               ---------------
                     Air Volume (l): 0
         Pre Clean with Solvent 1 (): 2
         Pre Clean with Solvent 2 (): 2
            Pre Clean with Sample (): 0
                Filling Speed (l/s): 1
                  Filling Strokes (): 4
                           Inject to: GC Inj1
              Injection Speed (l/s): 100
               Pre Inject Delay (ms): 100
              Post Inject Delay (ms): 100
        Post Clean with Solvent 1 (): 2
        Post Clean with Solvent 2 (): 2
Oven
Equilibration Time                           0.5 min
Oven Program                                 On
    60 C for 1 min
    then 10 C/min to 320 C for 10 min
Run Time                                     37 min






Front SS Inlet He
Mode                                         Split
Heater                                       On    250 C
Pressure                                     On    8.118 psi
Total Flow                                   On    13.891 mL/min
Septum Purge Flow                            On    3 mL/min
Gas Saver                                    On    20 mL/min After 3 min
Split Ratio                                  10 :1
Split Flow                                   9.901 mL/min


Thermal Aux 2 {MSD Transfer Line}
Heater                                       On
Temperature Program                          On
    320 C for 0 min
Run Time                                     37 min


Column #1
DB-5MS + DG Part number 122-55: 2786.52816
DB-5MS + DG Part number 122-55
500 C: 30 m x 250 m x 0.25 m
In: Front SS Inlet He
Out: Vacuum

(Initial)                                    60 C
Pressure                                     8.118 psi
Flow                                         0.9901 mL/min
Average Velocity                             36.441 cm/sec
Holdup Time                                  1.3721 min
Flow Program                                 Off
    0.9901 mL/min for 52 min
Run Time                                     37 min











Aux EPC 1 N2
Aux EPC 2 N2
Aux EPC 3 N2



Signals
 Test Plot                                   Save Off
                                             50 Hz
 Test Plot                                   Save Off
                                             50 Hz
 Test Plot                                   Save Off
                                             50 Hz
 Test Plot                                   Save Off
                                             50 Hz


                                MS ACQUISITION PARAMETERS


General Information
------- -----------

Tune File                : atune.u
Acquistion Mode          : Scan


MS Information
-- -----------

Solvent Delay            : 5.90 min

EMV Mode                 : Relative
Relative Voltage         : 188
Resulting EM Voltage     : 1518

[Scan Parameters]

Low Mass                 : 50.0
High Mass                : 600.0
Threshold                : 100
Sample #                 : 2       A/D Samples    4
Plot 2 low mass          : 40.0
Plot 2 high mass         : 610.0

[MSZones]

MS Source                : 250 C   maximum 250 C
MS Quad                  : 150 C   maximum 200 C


                             END OF MS ACQUISITION PARAMETERS


                              TUNE PARAMETERS for SN: US80838766
                        -----------------------------

 Trace Ion Detection is OFF.

 EMISSION    :      34.610
 ENERGY      :      69.922
 REPELLER    :      14.710
 IONFOCUS    :      80.667
 ENTRANCE_LE :      19.000
 EMVOLTS     :    1329.412
                               Actual EMV  :    1517.65
                               GAIN FACTOR :       5.94
 AMUGAIN     :    2050.000
 AMUOFFSET   :     118.000
 FILAMENT    :       1.000
 DCPOLARITY  :       0.000
 ENTLENSOFFS :      18.071
 MASSGAIN    :    -460.000   
 MASSOFFSET  :     -37.000   

                           END OF TUNE PARAMETERS
                      ------------------------------------



                                               END OF INSTRUMENT CONTROL PARAMETERS
                                               ------------------------------------

