

                 INSTRUMENT CONTROL PARAMETERS:    Agilent 5975B
                 -----------------------------------------------

   D:\CN178-205_DR_WILLIS_MOUSE_HEART-2\HAPO.M
      Thu Jun 02 06:04:24 2016

Control Information
------- -----------

Sample Inlet      :  GC
Injection Source  :  GC ALS
Mass Spectrometer :  Enabled

=============================================================================
                                6890 GC METHOD
=============================================================================


OVEN
   Initial temp:  60 'C (On)               Maximum temp:  330 'C
   Initial time:  1.00 min                 Equilibration time:  0.50 min
   Ramps:
      #  Rate  Final temp  Final time
      1 10.00      325        3.50
      2   0.0(Off)
   Post temp:  325 'C
   Post time:  6.50 min
   Run time:  31.00 min


FRONT INLET (UNKNOWN)                   BACK INLET (SPLIT/SPLITLESS)
                                           Mode:  Split
                                           Initial temp:  0 'C (Off)
                                           Pressure:  9.38 psi (On)
                                           Split ratio:  25:1
                                           Split flow:  55.1 mL/min
                                           Total flow:  60.1 mL/min
                                           Gas saver:  On
                                           Saver flow:  150.0 mL/min
                                           Saver time:  33.00 min
                                           Gas type:  Helium


COLUMN 1                                COLUMN 2
   Capillary Column                        Capillary Column
   Model Number:  J&W 122-5512             Model Number:  J&W 122-5512
   DB-5ms                                  DB-5ms
   Max temperature:  325 'C                Max temperature:  325 'C
   Nominal length:  15.0 m                 Nominal length:  15.0 m
   Nominal diameter:  250.00 um            Nominal diameter:  250.00 um
   Nominal film thickness:  0.25 um        Nominal film thickness:  0.25 um
   Mode:  constant flow                    Mode:  constant flow
   Initial flow:  2.2 mL/min               Initial flow:  1.3 mL/min
   Nominal init pressure:  9.39 psi        Nominal init pressure:  3.65 psi
   Average velocity:  77 cm/sec            Average velocity:  59 cm/sec
   Inlet:  Back Inlet                      Inlet:  Aux 4 Pressure Controller
   Outlet:  (unspecified)                  Outlet:  MSD
   Outlet pressure:  vacuum                Outlet pressure:  vacuum


FRONT DETECTOR (NO DET)                 BACK DETECTOR (NO DET)


SIGNAL 1                                SIGNAL 2
   Data rate:  20 Hz                       Data rate:  20 Hz
   Type:  test plot                        Type:  test plot
   Save Data:  Off                         Save Data:  Off
   Zero:  0.0 (Off)                        Zero:  0.0 (Off)
   Range:  0                               Range:  0
   Fast Peaks:  Off                        Fast Peaks:  Off
   Attenuation:  0                         Attenuation:  0


COLUMN COMP 1                           COLUMN COMP 2
   (No Detectors Installed)                (No Detectors Installed)


THERMAL AUX 2                           AUX PRESSURE 3
   Use:  MSD Transfer Line Heater          Description:
   Description:                            Gas Type:  Helium
   Initial temp:  290 'C (On)              Initial pressure:  0.00 psi (Off)
   Initial time:  0.00 min
      #  Rate  Final temp  Final time
      1   0.0(Off)


AUX PRESSURE 4                          AUX PRESSURE 5
   Description:                            Description:
   Gas Type:  Helium                       Gas Type:  Helium
   Driving Column 2                        Initial pressure:  0.00 psi (Off)
   Initial pressure:  3.64 psi (On)


                                        POST RUN
                                           Post Time: 6.50 min
                                           Oven Temperature: 325 'C
                                           Column 1 Flow: 0.1 mL/min
                                           Column 2 Flow: 4.3 mL/min


TIME TABLE
   Time       Specifier                     Parameter & Setpoint




                               GC Injector


     Front Injector:
No parameters specified

     Back Injector:
        Sample Washes                 1
        Sample Pumps                  2
        Injection Volume           5.00 microliters
        Syringe Size               10.0 microliters
        PreInj Solvent A Washes       1
        PreInj Solvent B Washes       1
        PostInj Solvent A Washes      2
        PostInj Solvent B Washes      2
        Viscosity Delay               0 seconds
        Plunger Speed              Fast
        PreInjection Dwell         0.00 minutes
        PostInjection Dwell        0.00 minutes


 Column 1 Inventory Number :  
 Column 2 Inventory Number :  

                                MS ACQUISITION PARAMETERS


General Information
------- -----------

Tune File                : atune.u
Acquistion Mode          : Scan


MS Information
-- -----------

Solvent Delay            : 5.60 min

EMV Mode                 : Gain Factor
Gain Factor              : 0.80
Resulting EM Voltage     : 1576

[Scan Parameters]

Low Mass                 : 50.0
High Mass                : 600.0
Threshold                : 150
Sample #                 : 2       A/D Samples    4
Plot 2 low mass          : 50.0
Plot 2 high mass         : 550.0

[MSZones]

MS Source                : 270 C   maximum 300 C
MS Quad                  : 150 C   maximum 200 C


                             END OF MS ACQUISITION PARAMETERS


                              TUNE PARAMETERS for SN: US62743684
                        -----------------------------

 Trace Ion Detection is OFF.

 EMISSION    :      34.610
 ENERGY      :      69.922
 REPELLER    :      34.814
 IONFOCUS    :      90.157
 ENTRANCE_LE :      25.500
 EMVOLTS     :    1470.588
                               Actual EMV  :    1576.47
                               GAIN FACTOR :       0.82
 AMUGAIN     :    1305.000
 AMUOFFSET   :     115.688
 FILAMENT    :       2.000
 DCPOLARITY  :       1.000
 ENTLENSOFFS :      21.835
 MASSGAIN    :    -927.000   
 MASSOFFSET  :     -42.000   

                           END OF TUNE PARAMETERS
                      ------------------------------------



                      END OF INSTRUMENT CONTROL PARAMETERS
                      ------------------------------------

