                                                ٷֱȱ

  ·  : C:\MSDCHEM\1\DATA\HUANGWENJIE\20190916GF14B2019\
  ļ  : Nip-0h-1.D                                          
  ɼ      : 16 Sep 2019  20:37
      : lvqi
  Ʒ      : Nip-0h-1
        :  
  ALS Ʒƿ: 4   Ʒ˻: 1

  ֲ  : autoint1.e
      : ѧվ

      : C:\MSDCHEM\1\METHODS\20181120-Ŵ-DB35MS-FINAL.M
        :  

  źţTIC: Nip-0h-1.D\data.ms

  ʱ ʼ 嶥 ֹ                       %
   #     ɨ ɨ ɨ             % ֵ   
 ---  ----- ----- ---- ---- ---  -------   -------  ------  -------
  1   4.324    28   34   45 PV 2   24088    507743   0.05%   0.016%
  2   4.515    49   62   71 PV 2   30468    985310   0.10%   0.031%
  3   4.662    74   83   87 VV 4    9508    214281   0.02%   0.007%
  4   4.906   110  118  123 PV     35691    820917   0.09%   0.026%
  5   4.998   123  131  146 VV   1225545  26893686   2.83%   0.843%
 
  6   5.476   194  200  204 VV 2   12582    261058   0.03%   0.008%
  7   5.534   204  208  216 VV 2    7999    186152   0.02%   0.006%
  8   5.868   250  256  263 VV 8    6471    157144   0.02%   0.005%
  9   6.020   270  278  286 PV 8    4891    144849   0.02%   0.005%
 10   6.286   310  317  324 VV 6    5528    120179   0.01%   0.004%
 
 11   6.396   327  332  340 VV 3    8688    211368   0.02%   0.007%
 12   6.642   357  368  382 PV    107597   2587609   0.27%   0.081%
 13   7.183   433  446  453 PV    452099   9603647   1.01%   0.301%
 14   7.254   453  456  463 VV 5    7721    190136   0.02%   0.006%
 15   7.510   488  493  498 VV 5    5864    134955   0.01%   0.004%
 
 16   7.622   501  509  522 VV    260588   5671431   0.60%   0.178%
 17   7.764   522  529  536 VV     38020    779717   0.08%   0.024%
 18   7.883   536  546  556 VV     85562   1833338   0.19%   0.057%
 19   8.092   568  576  584 VV    299284   6411618   0.67%   0.201%
 20   8.172   584  588  601 VV 2   16951    559341   0.06%   0.018%
 
 21   8.313   601  608  627 VV    223064   4841380   0.51%   0.152%
 22   8.776   666  675  684 PV    266457   5517754   0.58%   0.173%
 23   8.974   695  703  710 VV    230708   4636040   0.49%   0.145%
 24   9.033   710  712  723 VV 9    7987    192186   0.02%   0.006%
 25   9.226   730  740  750 VV   4565213  89692190   9.42%   2.811%
 
 26   9.321   750  753  759 VV 3   58437   1439768   0.15%   0.045%
 27   9.416   759  767  781 VV   4086534  78143473   8.21%   2.449%
 28   9.533   781  784  791 VV 7   14445    486693   0.05%   0.015%
 29   9.633   791  798  802 VV     69415   1560661   0.16%   0.049%
 30   9.686   802  806  822 VV 6   29882   1239983   0.13%   0.039%
 
 31   9.915   832  839  847 VV 4   15709    600703   0.06%   0.019%
 32  10.050   850  858  863 VV   2072212  38534176   4.05%   1.208%
 33  10.101   863  865  874 VV    146532   2701010   0.28%   0.085%
 34  10.288   880  892  895 VV    231353   4911269   0.52%   0.154%
 35  10.331   895  899  902 VV    744354  13745700   1.44%   0.431%
 
 36  10.375   902  905  914 VV    432403   8225608   0.86%   0.258%
 37  10.477   914  920  924 VV 2   28632    657371   0.07%   0.021%
 38  10.533   924  928  932 VV     33011    698883   0.07%   0.022%
 39  10.579   932  934  940 VV 2   19407    432645   0.05%   0.014%
 40  10.864   968  975  982 VV 3    7228    208309   0.02%   0.007%
 
 41  10.943   982  987  993 VV 6    8815    283581   0.03%   0.009%
 42  11.010   993  996 1000 VV 3   11527    239211   0.03%   0.007%
 43  11.119  1000 1012 1021 VV    117175   2588643   0.27%   0.081%
 44  11.228  1021 1028 1037 VV     75150   1591646   0.17%   0.050%
 45  11.350  1041 1045 1048 VV 6   10164    208553   0.02%   0.007%
 
 46  11.398  1048 1052 1058 VV 7    8123    244645   0.03%   0.008%
 47  11.718  1091 1098 1106 VV 5   18967    497213   0.05%   0.016%
 48  11.817  1106 1112 1116 VV 4    7023    170503   0.02%   0.005%
 49  11.884  1116 1122 1141 VV     55982   1414717   0.15%   0.044%
 50  12.044  1141 1145 1154 VV 7    8098    210878   0.02%   0.007%
 
 51  12.178  1157 1164 1167 VV 7    5795    152398   0.02%   0.005%
 52  12.214  1167 1170 1174 VV 5    5464    106686   0.01%   0.003%
 53  12.275  1174 1178 1184 VV 6    7420    168448   0.02%   0.005%
 54  12.383  1187 1194 1195 VV 7    4829     99742   0.01%   0.003%
 55  12.408  1195 1197 1203 VV 5    6678    166934   0.02%   0.005%
 
 56  12.556  1208 1219 1226 VV 7   13068    596139   0.06%   0.019%
 57  12.721  1234 1243 1258 VV   5333427  91954359   9.66%   2.882%
 58  12.865  1258 1263 1269 VV 6   14991    475407   0.05%   0.015%
 59  12.960  1272 1277 1284 VV 4   16564    566286   0.06%   0.018%
 60  13.064  1284 1292 1299 VV 2  493683   9131671   0.96%   0.286%
 
 61  13.141  1299 1303 1308 VV 4   24860    617108   0.06%   0.019%
 62  13.228  1308 1315 1321 VV   2159112  36932721   3.88%   1.157%
 63  13.278  1321 1323 1339 VV 2  125311   2794463   0.29%   0.088%
 64  13.493  1339 1354 1363 VV 5  112210   5113371   0.54%   0.160%
 65  13.571  1363 1365 1369 VV     42188    913395   0.10%   0.029%
 
 66  13.635  1369 1374 1379 VV 5   38647   1099962   0.12%   0.034%
 67  13.747  1379 1390 1399 VV    148368   4645120   0.49%   0.146%
 68  13.847  1399 1405 1406 VV 6   37097    931632   0.10%   0.029%
 69  13.922  1406 1415 1433 VV   1113267  22282909   2.34%   0.698%
 70  14.098  1433 1441 1447 VV 4   33671   1112211   0.12%   0.035%
 
 71  14.177  1447 1452 1460 VV 2   47452   1263594   0.13%   0.040%
 72  14.267  1460 1465 1470 VV 2   40891    933828   0.10%   0.029%
 73  14.356  1470 1478 1488 VV    354597   7141575   0.75%   0.224%
 74  14.500  1488 1499 1508 VV 5   48209   2313850   0.24%   0.073%
 75  14.614  1508 1515 1525 VV   1318345  25048331   2.63%   0.785%
 
 76  14.734  1525 1532 1536 VV    533266  10619873   1.12%   0.333%
 77  14.796  1536 1541 1558 VV   3802013  64583718   6.79%   2.024%
 78  15.043  1573 1577 1578 VV 4   17829    314683   0.03%   0.010%
 79  15.090  1578 1584 1589 VV    164620   3281072   0.34%   0.103%
 80  15.159  1589 1593 1599 VV     56204   1244448   0.13%   0.039%
 
 81  15.275  1599 1610 1616 VV 4   65334   2192310   0.23%   0.069%
 82  15.353  1616 1621 1626 VV 2   63154   1408541   0.15%   0.044%
 83  15.435  1626 1633 1636 VV     35459    952452   0.10%   0.030%
 84  15.496  1636 1642 1649 VV 2  233714   4723345   0.50%   0.148%
 85  15.586  1649 1655 1660 VV    109167   2422620   0.25%   0.076%
 
 86  15.630  1660 1661 1666 VV 4   24301    456153   0.05%   0.014%
 87  15.818  1676 1688 1692 VV 3   42228   1434870   0.15%   0.045%
 88  15.864  1692 1695 1701 VV 4   23557    585857   0.06%   0.018%
 89  15.991  1701 1713 1719 VV 4  359517   9695645   1.02%   0.304%
 90  16.097  1719 1728 1735 VV 2 9035945 178902838  18.80%   5.607%
 
 91  16.181  1735 1741 1752 VV    575551  11957307   1.26%   0.375%
 92  16.294  1752 1757 1760 VV 2   54128   1491567   0.16%   0.047%
 93  16.359  1760 1766 1771 VV    385893   7465644   0.78%   0.234%
 94  16.428  1771 1776 1786 VV    402930  10639343   1.12%   0.333%
 95  16.528  1786 1790 1793 VV 4   62142   1525074   0.16%   0.048%
 
 96  16.575  1793 1797 1809 VV 2   85845   2452762   0.26%   0.077%
 97  16.723  1813 1819 1823 VV     70377   1551644   0.16%   0.049%
 98  16.824  1823 1833 1839 VV 4   63585   2438072   0.26%   0.076%
 99  17.004  1839 1859 1865 VV   11783217 218263628  22.93%   6.840%
100  17.077  1865 1869 1875 VV 3  216258   4948216   0.52%   0.155%
 
101  17.181  1875 1884 1891 VV   8058094 150484805  15.81%   4.716%
102  17.247  1891 1894 1900 VV    386003   8966227   0.94%   0.281%
103  17.351  1900 1909 1913 VV   18358178 348843316  36.65%  10.932%
104  17.405  1913 1917 1922 VV   7698861 134389081  14.12%   4.212%
105  17.466  1922 1925 1930 VV    483268   9234157   0.97%   0.289%
 
106  17.550  1930 1938 1942 VV 3 4289163  87852915   9.23%   2.753%
107  17.602  1942 1945 1952 VV   3706467  67157774   7.06%   2.105%
108  17.676  1952 1956 1961 VV 3   63084   1680959   0.18%   0.053%
109  17.797  1968 1973 1984 VV 8   42184   1863545   0.20%   0.058%
110  17.920  1984 1991 1999 VV 8   39884   1664094   0.17%   0.052%
 
111  18.012  1999 2004 2007 VV 4   37214    889710   0.09%   0.028%
112  18.088  2007 2015 2020 VV    538032  10162424   1.07%   0.318%
113  18.142  2020 2023 2040 VV 10   50367   2004589   0.21%   0.063%
114  18.320  2045 2048 2050 VV 3   16369    291967   0.03%   0.009%
115  18.382  2050 2057 2061 VV 3  106163   2504909   0.26%   0.079%
 
116  18.442  2061 2066 2078 VV 5   86681   2967024   0.31%   0.093%
117  18.592  2078 2087 2098 VV   3261286  56831464   5.97%   1.781%
118  18.675  2098 2099 2101 VV 2   18432    238971   0.03%   0.007%
119  18.732  2101 2108 2123 VV 3  103790   3045070   0.32%   0.095%
120  18.890  2123 2130 2139 VV    133646   3089967   0.32%   0.097%
 
121  18.965  2139 2141 2145 VV 4   12949    248059   0.03%   0.008%
122  19.093  2154 2160 2164 VV 3   55373   1248050   0.13%   0.039%
123  19.160  2164 2169 2177 VV 3   58170   1452594   0.15%   0.046%
124  19.250  2177 2182 2190 VV 3   39781   1021217   0.11%   0.032%
125  19.382  2190 2201 2213 VV   3311003  74327039   7.81%   2.329%
 
126  19.504  2213 2219 2228 VV    205332   4526594   0.48%   0.142%
127  19.601  2228 2233 2239 VV 3   33300    851657   0.09%   0.027%
128  19.743  2246 2253 2260 VV 4   29061    810390   0.09%   0.025%
129  19.835  2260 2266 2268 VV 5    6801    184724   0.02%   0.006%
130  19.899  2268 2276 2283 VV     82487   1928480   0.20%   0.060%
 
131  20.006  2283 2291 2304 VV 8   18719    795574   0.08%   0.025%
132  20.168  2310 2314 2324 VV 6   10702    314943   0.03%   0.010%
133  20.296  2324 2333 2338 VV 4   38960   1224397   0.13%   0.038%
134  20.351  2338 2341 2348 VV 5   25182    695430   0.07%   0.022%
135  20.518  2351 2365 2371 VV 8   15349    627115   0.07%   0.020%
 
136  20.617  2371 2379 2390 VV 2   68801   2079799   0.22%   0.065%
137  20.710  2390 2392 2401 VV 10    6790    240079   0.03%   0.008%
138  20.827  2401 2409 2419 VV 5   29621    868805   0.09%   0.027%
139  20.933  2419 2424 2433 VV 4   13784    375555   0.04%   0.012%
140  21.060  2433 2443 2457 VV     50124   1420091   0.15%   0.045%
 
141  21.191  2457 2462 2472 VV      6101    237659   0.02%   0.007%
142  21.399  2483 2491 2502 VV 7    8038    247744   0.03%   0.008%
143  21.566  2510 2515 2526 VV 9    4749    177041   0.02%   0.006%
144  21.706  2526 2536 2542 VV 7    9290    319935   0.03%   0.010%
145  21.964  2563 2573 2575 PV 6    6186    156192   0.02%   0.005%
 
146  22.004  2575 2579 2587 VV 9   12438    308161   0.03%   0.010%
147  22.088  2587 2591 2595 VV 6    4587    111184   0.01%   0.003%
148  22.295  2611 2620 2627 PV 6    6486    147995   0.02%   0.005%
149  22.387  2627 2634 2638 VV 9    4949    101366   0.01%   0.003%
150  22.449  2638 2643 2651 VV 6   28562    617219   0.06%   0.019%
 
151  22.517  2651 2652 2660 VV 5    4069     86999   0.01%   0.003%
152  22.693  2660 2678 2686 VV     99181   2414731   0.25%   0.076%
153  22.780  2686 2690 2693 VV 4   16051    296748   0.03%   0.009%
154  22.825  2693 2697 2700 VV 2   27616    507969   0.05%   0.016%
155  22.881  2700 2705 2715 VV 6   43577   1222446   0.13%   0.038%
 
156  22.998  2715 2722 2734 VV     86790   1605249   0.17%   0.050%
157  23.146  2734 2743 2748 VV 9    9137    297499   0.03%   0.009%
158  23.213  2748 2753 2756 VV 2   26797    450722   0.05%   0.014%
159  23.256  2756 2759 2761 VV 3   16697    266663   0.03%   0.008%
160  23.306  2761 2766 2768 VV 6   12705    271554   0.03%   0.009%
 
161  23.349  2768 2772 2777 VV 7   24944    652706   0.07%   0.020%
162  23.421  2777 2782 2786 VV    123892   2071901   0.22%   0.065%
163  23.469  2786 2789 2798 VV 2   65713   1178926   0.12%   0.037%
164  23.583  2798 2806 2812 VV 5   33782    782661   0.08%   0.025%
165  23.695  2819 2822 2827 VV 6    5307    110358   0.01%   0.003%
 
166  23.826  2831 2841 2849 VV 2  288022   8083834   0.85%   0.253%
167  23.909  2849 2853 2859 VV 6   23157    534731   0.06%   0.017%
168  23.977  2859 2863 2865 VV 5   11104    221625   0.02%   0.007%
169  24.018  2865 2868 2876 VV 5   25951    492544   0.05%   0.015%
170  24.112  2876 2882 2890 VV 2   41833    881382   0.09%   0.028%
 
171  24.191  2890 2893 2898 VV 3    9055    217366   0.02%   0.007%
172  24.247  2898 2901 2904 VV 3   11739    223962   0.02%   0.007%
173  24.315  2904 2911 2914 VV 4   18140    431619   0.05%   0.014%
174  24.348  2914 2916 2919 VV 3   10541    146161   0.02%   0.005%
175  24.395  2919 2923 2926 VV 3   21380    388402   0.04%   0.012%
 
176  24.458  2926 2932 2935 VV 4   29391    659739   0.07%   0.021%
177  24.505  2935 2938 2947 VV 5   20961    553243   0.06%   0.017%
178  24.620  2951 2955 2958 VV      8505    164505   0.02%   0.005%
179  24.721  2962 2969 2974 VV 8   14461    319068   0.03%   0.010%
180  24.817  2981 2983 2988 VV 6    4960    108299   0.01%   0.003%
 
181  24.882  2988 2993 2997 VV 3   20460    380202   0.04%   0.012%
182  24.966  2997 3005 3041 VV   33522317 951795441 100.00%  29.828%
183  25.229  3041 3043 3047 VV 5   94345   2535544   0.27%   0.079%
184  25.293  3047 3052 3054 VV 5  106020   2475181   0.26%   0.078%
185  25.323  3054 3056 3060 VV    117752   2555007   0.27%   0.080%
 
186  25.380  3060 3064 3076 VV    303947   7735562   0.81%   0.242%
187  25.555  3080 3090 3101 VV 4  118867   6540009   0.69%   0.205%
188  25.667  3101 3106 3112 VV    265065   5675581   0.60%   0.178%
189  25.726  3112 3114 3127 VV 7   73891   3343158   0.35%   0.105%
190  25.875  3127 3136 3140 VV     91656   2609204   0.27%   0.082%
 
191  25.920  3140 3142 3150 VV 9   36159   1177774   0.12%   0.037%
192  26.030  3153 3158 3160 VV 6   37616    917260   0.10%   0.029%
193  26.052  3160 3161 3168 VV 7   37878   1174763   0.12%   0.037%
194  26.147  3168 3175 3178 VV 4   90835   2504271   0.26%   0.078%
195  26.197  3178 3182 3187 VV 2  100437   2011848   0.21%   0.063%
 
196  26.279  3191 3194 3198 VV 5   26094    651412   0.07%   0.020%
197  26.319  3198 3200 3210 VV 10   23399    984387   0.10%   0.031%
198  26.425  3210 3215 3219 VV 8   20705    624112   0.07%   0.020%
199  26.478  3219 3222 3225 VV 5   21194    460418   0.05%   0.014%
200  26.521  3225 3229 3232 VV 5   38149    777262   0.08%   0.024%
 
201  26.548  3232 3232 3242 VV 8   27561    930428   0.10%   0.029%
202  26.647  3242 3247 3255 VV 10   23751   1076664   0.11%   0.034%
203  26.748  3255 3261 3263 VV     41503    873548   0.09%   0.027%
204  26.781  3263 3266 3271 VV 4   56336   1427973   0.15%   0.045%
205  26.851  3271 3276 3304 VV   3835098  68268654   7.17%   2.139%
 
206  27.056  3304 3306 3308 VV 3   33132    620335   0.07%   0.019%
207  27.088  3308 3310 3312 VV 3   33076    438735   0.05%   0.014%
208  27.112  3312 3314 3322 VV 9   31846   1160413   0.12%   0.036%
209  27.288  3335 3339 3350 VV 10   27899   1269962   0.13%   0.040%
210  27.489  3366 3368 3372 VV 5   18669    423497   0.04%   0.013%
 
211  27.545  3372 3376 3384 VV 2   30364   1006521   0.11%   0.032%
212  27.645  3384 3390 3400 VV 2   20451   1137259   0.12%   0.036%
213  27.807  3408 3414 3417 VV 8   19287    589718   0.06%   0.018%
214  27.871  3417 3423 3433 VV 8   23059   1247062   0.13%   0.039%
215  28.081  3450 3453 3458 VV 7   15799    466723   0.05%   0.015%
 
216  28.216  3468 3472 3475 VV 5   20291    433377   0.05%   0.014%
217  28.245  3475 3477 3482 VV 6   18136    520247   0.05%   0.016%
218  28.295  3482 3484 3489 VV 6   17092    445552   0.05%   0.014%
219  28.480  3502 3510 3513 VV 10   23719    763531   0.08%   0.024%
220  28.516  3513 3516 3518 VV 4   15505    308422   0.03%   0.010%
 
221  28.585  3518 3526 3535 VV 5   43843   1883882   0.20%   0.059%
222  28.660  3535 3536 3540 VV 4   19538    421825   0.04%   0.013%
223  28.717  3540 3545 3554 VV 4   18491    954111   0.10%   0.030%
224  29.067  3592 3595 3604 VV 10   15248    671315   0.07%   0.021%
225  29.148  3604 3607 3609 VV 4   13950    225891   0.02%   0.007%
 
226  29.176  3609 3611 3613 VV 2   13565    209972   0.02%   0.007%
227  29.230  3613 3618 3622 VV 8   14692    474067   0.05%   0.015%
228  29.432  3640 3647 3652 VV 8   12758    561275   0.06%   0.018%
229  29.725  3686 3690 3694 VV 7   10273    281012   0.03%   0.009%
230  30.082  3736 3741 3746 VV 9    9201    297433   0.03%   0.009%
 
231  30.171  3749 3754 3758 VV 8    7515    234114   0.02%   0.007%
232  30.696  3828 3829 3834 VV 5    6871    124611   0.01%   0.004%
233  31.141  3887 3893 3899 VV 5    4822    178147   0.02%   0.006%
234  31.323  3912 3920 3922 VV 9    5454    134078   0.01%   0.004%
235  31.806  3976 3989 3991 VV 9    4006    127253   0.01%   0.004%
 
236  31.947  4007 4010 4012 PV 4    2751     24598   0.00%   0.001%
237  32.138  4035 4037 4040 PV 4    3517     33761   0.00%   0.001%
 
 
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