                                                ٷֱȱ

  ·  : C:\MSDCHEM\1\DATA\HUANGWENJIE\20190916GF14B2019\
  ļ  : Nip-0h-5.D                                          
  ɼ      : 17 Sep 2019  19:08
      : lvqi
  Ʒ      : Nip-0h-5
        :  
  ALS Ʒƿ: 40   Ʒ˻: 1

  ֲ  : autoint1.e
      : ѧվ

      : C:\MSDCHEM\1\METHODS\20181120-Ŵ-DB35MS-FINAL.M
        :  

  źţTIC: Nip-0h-5.D\data.ms

  ʱ ʼ 嶥 ֹ                       %
   #     ɨ ɨ ɨ             % ֵ   
 ---  ----- ----- ---- ---- ---  -------   -------  ------  -------
  1   4.324    28   34   40 BV     29230    653240   0.07%   0.024%
  2   4.513    52   61   72 PV 2   29760    946456   0.11%   0.035%
  3   4.662    77   83   91 VV 2   10456    234116   0.03%   0.009%
  4   4.905   110  118  123 VV     40224    874054   0.10%   0.032%
  5   4.996   123  131  143 VV    878057  19204470   2.14%   0.706%
 
  6   5.472   194  199  203 VV 3   11128    237875   0.03%   0.009%
  7   5.531   203  208  219 VV 2    9642    265766   0.03%   0.010%
  8   5.856   250  255  259 PV 7    5367    103777   0.01%   0.004%
  9   6.290   312  317  324 VV 5    4420     93886   0.01%   0.003%
 10   6.391   324  332  340 VV 4    6384    182194   0.02%   0.007%
 
 11   6.640   358  367  377 VV 2  118958   2831703   0.32%   0.104%
 12   7.182   437  445  453 PV    363050   7528300   0.84%   0.277%
 13   7.257   453  456  466 VV 7    7730    218305   0.02%   0.008%
 14   7.435   479  482  486 VV 5    3746     69523   0.01%   0.003%
 15   7.507   486  492  500 VV 3    5290    167563   0.02%   0.006%
 
 16   7.620   500  509  517 VV    227859   5007889   0.56%   0.184%
 17   7.762   523  529  539 VV 2   36365    797701   0.09%   0.029%
 18   7.881   539  546  554 VV     77425   1631972   0.18%   0.060%
 19   8.091   562  576  583 VV    206802   4476629   0.50%   0.165%
 20   8.173   583  588  598 VV     26550    692311   0.08%   0.025%
 
 21   8.313   598  608  622 VV    163956   3537280   0.39%   0.130%
 22   8.775   666  675  683 PV    212263   4276148   0.48%   0.157%
 23   8.973   696  703  710 VV    167339   3471509   0.39%   0.128%
 24   9.033   710  712  721 VV 7    5495    118735   0.01%   0.004%
 25   9.224   728  739  749 VV   4286157  81662036   9.10%   3.004%
 
 26   9.320   749  753  759 VV     63887   1570398   0.17%   0.058%
 27   9.414   759  767  779 VV   2524609  47751645   5.32%   1.756%
 28   9.630   791  798  802 VV     56342   1259844   0.14%   0.046%
 29   9.687   802  806  818 VV 7   29676   1167858   0.13%   0.043%
 30   9.919   832  839  849 VV     29186    843021   0.09%   0.031%
 
 31  10.048   849  858  863 VV   1702725  31282006   3.48%   1.151%
 32  10.099   863  865  873 VV    138673   2572813   0.29%   0.095%
 33  10.286   881  892  894 VV    188476   4015040   0.45%   0.148%
 34  10.329   894  898  902 VV    784111  14360288   1.60%   0.528%
 35  10.374   902  905  913 VV    345985   6429499   0.72%   0.236%
 
 36  10.473   913  919  923 VV 4   25023    613256   0.07%   0.023%
 37  10.532   923  928  932 VV     34244    700588   0.08%   0.026%
 38  10.578   932  934  939 VV     16767    328413   0.04%   0.012%
 39  10.863   969  975  981 VV 6    5413    160440   0.02%   0.006%
 40  10.926   981  984  985 VV 3    4820     64188   0.01%   0.002%
 
 41  11.008   985  996 1004 VV 9    9986    409642   0.05%   0.015%
 42  11.118  1004 1012 1021 VV     88883   2031821   0.23%   0.075%
 43  11.226  1021 1027 1036 VV 2   59694   1269703   0.14%   0.047%
 44  11.347  1040 1045 1050 VV 5   10648    275266   0.03%   0.010%
 45  11.414  1050 1054 1059 VV 8    7723    221922   0.02%   0.008%
 
 46  11.714  1089 1098 1108 VV 8   15448    487913   0.05%   0.018%
 47  11.810  1108 1112 1116 VV 6    6217    132637   0.01%   0.005%
 48  11.881  1116 1122 1132 VV     30568    827950   0.09%   0.030%
 49  12.047  1141 1146 1150 VV 6    9655    216605   0.02%   0.008%
 50  12.181  1161 1165 1167 VV 2    5540    106597   0.01%   0.004%
 
 51  12.272  1173 1178 1186 VV 10    9131    259351   0.03%   0.010%
 52  12.408  1186 1198 1204 VV 4   16625    488664   0.05%   0.018%
 53  12.556  1208 1219 1226 VV 4   24404    791614   0.09%   0.029%
 54  12.719  1226 1242 1257 VV   4377706  74705756   8.32%   2.748%
 55  12.856  1257 1262 1268 VV 6   14863    502405   0.06%   0.018%
 
 56  12.948  1268 1275 1285 VV 8   15789    794755   0.09%   0.029%
 57  13.063  1285 1292 1298 VV 2  344410   6411268   0.71%   0.236%
 58  13.137  1298 1302 1308 VV 5   21379    590222   0.07%   0.022%
 59  13.227  1308 1315 1321 VV   1822214  30912395   3.44%   1.137%
 60  13.277  1321 1323 1334 VV 3  107996   2404255   0.27%   0.088%
 
 61  13.494  1341 1354 1370 VV 5  275613  13753774   1.53%   0.506%
 62  13.632  1370 1374 1379 VV 7   40526   1230748   0.14%   0.045%
 63  13.707  1379 1385 1386 VV 3   52786   1068895   0.12%   0.039%
 64  13.745  1386 1390 1402 VV    119816   3695020   0.41%   0.136%
 65  13.921  1402 1415 1423 VV    927884  18809929   2.10%   0.692%
 
 66  14.097  1435 1441 1446 VV 2   32645    971154   0.11%   0.036%
 67  14.175  1446 1452 1458 VV 3   39738   1079063   0.12%   0.040%
 68  14.265  1458 1465 1469 VV 3   31006    828698   0.09%   0.030%
 69  14.354  1469 1478 1487 VV    492341   9370571   1.04%   0.345%
 70  14.452  1487 1492 1494 VV 4   19403    487252   0.05%   0.018%
 
 71  14.497  1494 1498 1507 VV 2   40266   1403312   0.16%   0.052%
 72  14.613  1507 1515 1525 VV   1245184  23707344   2.64%   0.872%
 73  14.733  1525 1532 1536 VV    612094  12007689   1.34%   0.442%
 74  14.794  1536 1541 1553 VV   3090690  52157134   5.81%   1.919%
 75  14.943  1559 1562 1564 VV 4   13556    234392   0.03%   0.009%
 
 76  14.979  1564 1568 1573 VV 5   15837    516472   0.06%   0.019%
 77  15.089  1573 1583 1589 VV    138480   3039640   0.34%   0.112%
 78  15.157  1589 1593 1598 VV 2   42905    941901   0.10%   0.035%
 79  15.274  1598 1610 1615 VV 3   56835   1996417   0.22%   0.073%
 80  15.351  1615 1621 1626 VV     55160   1328253   0.15%   0.049%
 
 81  15.434  1626 1633 1636 VV     32444    884325   0.10%   0.033%
 82  15.495  1636 1642 1648 VV 2  172399   3546396   0.40%   0.130%
 83  15.584  1648 1655 1665 VV    188835   4051062   0.45%   0.149%
 84  15.816  1679 1688 1692 VV 5   28768    970623   0.11%   0.036%
 85  15.862  1692 1695 1701 VV 4   18849    479441   0.05%   0.018%
 
 86  15.998  1701 1714 1719 VV 6  152894   4397693   0.49%   0.162%
 87  16.092  1719 1728 1736 VV   6651417 113489861  12.64%   4.175%
 88  16.180  1736 1740 1750 VV 2  169470   4336269   0.48%   0.160%
 89  16.290  1750 1756 1760 VV 3   40685   1174486   0.13%   0.043%
 90  16.356  1760 1766 1771 VV    309013   5836303   0.65%   0.215%
 
 91  16.425  1771 1776 1786 VV    214212   6111884   0.68%   0.225%
 92  16.525  1786 1790 1794 VV 4   46031   1201473   0.13%   0.044%
 93  16.573  1794 1797 1807 VV 4   28333    916604   0.10%   0.034%
 94  16.722  1813 1818 1824 VV     46737   1025570   0.11%   0.038%
 95  16.822  1824 1833 1840 VV 4   46223   1513063   0.17%   0.056%
 
 96  17.002  1840 1859 1865 VV   10869957 198929036  22.16%   7.317%
 97  17.074  1865 1869 1875 VV 2  187409   4166687   0.46%   0.153%
 98  17.179  1875 1884 1890 VV   7387981 135355650  15.08%   4.979%
 99  17.245  1890 1894 1900 VV    357076   8254134   0.92%   0.304%
100  17.348  1900 1908 1913 VV   17699345 327743145  36.51%  12.055%
 
101  17.403  1913 1916 1922 VV   6827436 115277157  12.84%   4.240%
102  17.464  1922 1925 1930 VV    110483   2390284   0.27%   0.088%
103  17.550  1930 1938 1941 VV 3 2129272  45347063   5.05%   1.668%
104  17.599  1941 1945 1952 VV   3348374  60925273   6.79%   2.241%
105  17.674  1952 1955 1960 VV 3   49702   1391215   0.15%   0.051%
 
106  17.799  1968 1973 1983 VV 8   29104   1323218   0.15%   0.049%
107  17.921  1983 1991 1998 VV 9   33527   1245913   0.14%   0.046%
108  18.009  1998 2004 2006 VV 5   25721    638945   0.07%   0.024%
109  18.087  2006 2015 2020 VV    400948   7794064   0.87%   0.287%
110  18.139  2020 2022 2043 VV     41439   1881896   0.21%   0.069%
 
111  18.314  2043 2048 2050 VV 6   12762    328812   0.04%   0.012%
112  18.382  2050 2057 2060 VV 4   85815   1870731   0.21%   0.069%
113  18.430  2060 2064 2079 VV 6  122088   3951042   0.44%   0.145%
114  18.589  2079 2087 2097 VV    680113  12490373   1.39%   0.459%
115  18.675  2097 2099 2101 VV 3   13555    215853   0.02%   0.008%
 
116  18.731  2101 2107 2114 VV 3   73638   1845427   0.21%   0.068%
117  18.889  2123 2130 2137 VV     96971   2176832   0.24%   0.080%
118  18.955  2137 2140 2144 VV 5   12895    291348   0.03%   0.011%
119  19.090  2153 2159 2164 VV 2   45390   1010632   0.11%   0.037%
120  19.157  2164 2169 2177 VV 2   37875   1016371   0.11%   0.037%
 
121  19.249  2177 2182 2188 VV 7   10791    338712   0.04%   0.012%
122  19.380  2192 2201 2213 VV   2613337  61613740   6.86%   2.266%
123  19.503  2213 2219 2229 VV    159090   3619703   0.40%   0.133%
124  19.604  2229 2233 2244 VV 9   13707    496946   0.06%   0.018%
125  19.741  2247 2253 2262 VV 7   23322    689057   0.08%   0.025%
 
126  19.898  2262 2275 2283 VV     63311   1610298   0.18%   0.059%
127  20.003  2283 2291 2302 VV 4   46048   1414380   0.16%   0.052%
128  20.175  2308 2315 2322 VV 7    9634    318819   0.04%   0.012%
129  20.298  2322 2333 2336 VV 4   29962    881491   0.10%   0.032%
130  20.351  2336 2341 2352 VV 3   30603    959951   0.11%   0.035%
 
131  20.476  2352 2359 2368 VV 9    6328    297569   0.03%   0.011%
132  20.615  2368 2379 2388 VV 4   57545   1781362   0.20%   0.066%
133  20.724  2388 2394 2397 VV 7    6245    180220   0.02%   0.007%
134  20.826  2402 2409 2417 VV 9   17530    515203   0.06%   0.019%
135  20.934  2417 2425 2433 VV 5    8157    227988   0.03%   0.008%
 
136  21.059  2433 2443 2458 PV     68256   1904996   0.21%   0.070%
137  21.210  2458 2464 2470 VV 9    5899    212434   0.02%   0.008%
138  21.402  2486 2492 2500 VV 7    8411    198235   0.02%   0.007%
139  21.710  2528 2536 2545 VV 10    7148    258937   0.03%   0.010%
140  22.009  2574 2579 2584 VV 8   10087    233622   0.03%   0.009%
 
141  22.296  2613 2621 2625 PV 8    8503    178510   0.02%   0.007%
142  22.383  2630 2633 2638 VV 6    3967     75108   0.01%   0.003%
143  22.447  2638 2642 2650 VV 5   24141    489157   0.05%   0.018%
144  22.648  2666 2671 2673 VV 3    8986    167369   0.02%   0.006%
145  22.692  2673 2678 2686 VV 3   85758   1921291   0.21%   0.071%
 
146  22.779  2686 2690 2693 VV 5   13484    247518   0.03%   0.009%
147  22.825  2693 2697 2700 VV 4   22271    428382   0.05%   0.016%
148  22.883  2700 2705 2715 VV 9   34748   1018694   0.11%   0.037%
149  22.997  2715 2721 2728 VV 2   45428    875634   0.10%   0.032%
150  23.142  2738 2742 2747 VV 7    9178    226100   0.03%   0.008%
 
151  23.212  2747 2752 2756 VV 3   27567    505263   0.06%   0.019%
152  23.254  2756 2758 2762 VV 3   16827    318336   0.04%   0.012%
153  23.306  2762 2766 2767 VV 3   15786    258105   0.03%   0.009%
154  23.348  2767 2772 2777 VV 4   41651   1000657   0.11%   0.037%
155  23.420  2777 2782 2786 VV    130856   2245132   0.25%   0.083%
 
156  23.467  2786 2789 2797 VV 3   55980   1077736   0.12%   0.040%
157  23.584  2797 2806 2813 VV 6   33334    992799   0.11%   0.037%
158  23.700  2818 2823 2826 VV 7    6026    145425   0.02%   0.005%
159  23.824  2832 2840 2849 VV 2  239677   6581539   0.73%   0.242%
160  23.911  2849 2853 2859 VV 6   22655    545652   0.06%   0.020%
 
161  23.972  2859 2862 2864 VV 3   11032    198129   0.02%   0.007%
162  24.018  2864 2868 2874 VV 5   22241    483315   0.05%   0.018%
163  24.113  2874 2882 2887 VV 6   25113    592561   0.07%   0.022%
164  24.188  2887 2893 2895 VV 6    7902    205758   0.02%   0.008%
165  24.245  2898 2901 2905 VV 5   11271    245142   0.03%   0.009%
 
166  24.317  2905 2911 2914 VV 7   11975    346761   0.04%   0.013%
167  24.393  2919 2922 2925 VV 3   13372    239189   0.03%   0.009%
168  24.443  2925 2930 2934 VV 6   11754    312270   0.03%   0.011%
169  24.513  2934 2940 2945 VV 5   16689    399746   0.04%   0.015%
170  24.617  2948 2955 2959 VV 3   10951    286877   0.03%   0.011%
 
171  24.712  2964 2968 2973 VV 8   14830    350342   0.04%   0.013%
172  24.879  2988 2992 2997 VV 3   17510    355307   0.04%   0.013%
173  24.965  2997 3005 3041 VV   34835795 897665174 100.00%  33.019%
174  25.234  3041 3043 3049 VV 4   62187   1776739   0.20%   0.065%
175  25.322  3049 3056 3060 VV 2   65707   2472347   0.28%   0.091%
 
176  25.380  3060 3064 3071 VV    268629   5183366   0.58%   0.191%
177  25.440  3071 3073 3077 VV 4   40903   1040878   0.12%   0.038%
178  25.553  3077 3089 3101 VV 5   91058   5420052   0.60%   0.199%
179  25.666  3101 3105 3111 VV    195706   4250765   0.47%   0.156%
180  25.725  3111 3114 3118 VV 5   73760   1987698   0.22%   0.073%
 
181  25.770  3118 3121 3127 VV 6   54519   1511800   0.17%   0.056%
182  25.874  3127 3136 3140 VV 3   53165   1840450   0.21%   0.068%
183  25.928  3140 3143 3154 VV 3   33373   1664678   0.19%   0.061%
184  26.033  3154 3158 3167 VV 3   37359   1851646   0.21%   0.068%
185  26.146  3167 3175 3179 VV 3   92909   2547595   0.28%   0.094%
 
186  26.196  3179 3182 3190 VV     77910   1860744   0.21%   0.068%
187  26.274  3190 3193 3196 VV 5   24983    585637   0.07%   0.022%
188  26.320  3196 3200 3202 VV 5   22417    467380   0.05%   0.017%
189  26.428  3212 3215 3221 VV 8   20502    696164   0.08%   0.026%
190  26.482  3221 3223 3225 VV 3   19913    277829   0.03%   0.010%
 
191  26.517  3225 3228 3231 VV 4   32171    628277   0.07%   0.023%
192  26.549  3231 3233 3237 VV 5   26475    566373   0.06%   0.021%
193  26.644  3243 3246 3249 VV 5   22519    475791   0.05%   0.018%
194  26.679  3249 3251 3257 VV 7   19770    546488   0.06%   0.020%
195  26.746  3257 3261 3263 VV     35540    621489   0.07%   0.023%
 
196  26.782  3263 3266 3271 VV 4   57318   1381902   0.15%   0.051%
197  26.849  3271 3276 3288 VV   2982314  49372971   5.50%   1.816%
198  26.944  3288 3289 3296 VV 5   55335   1503778   0.17%   0.055%
199  27.059  3303 3306 3308 VV 4   28983    611326   0.07%   0.022%
200  27.117  3308 3314 3318 VV 8   29520   1096742   0.12%   0.040%
 
201  27.157  3318 3320 3331 VV 8   24921   1191823   0.13%   0.044%
202  27.285  3334 3338 3342 VV 7   27995    733176   0.08%   0.027%
203  27.494  3365 3369 3371 VV 5   18310    430696   0.05%   0.016%
204  27.541  3371 3375 3379 VV 4   25638    638190   0.07%   0.023%
205  27.583  3379 3381 3384 VV 4   18417    307840   0.03%   0.011%
 
206  27.618  3384 3386 3400 VV 4   18679   1147322   0.13%   0.042%
207  27.810  3411 3414 3418 VV 5   18220    454222   0.05%   0.017%
208  27.892  3418 3426 3431 VV 5   20689    897511   0.10%   0.033%
209  28.083  3445 3453 3456 VV 10   15718    626606   0.07%   0.023%
210  28.210  3468 3472 3475 VV 5   17795    415132   0.05%   0.015%
 
211  28.247  3475 3477 3480 VV 4   19651    400398   0.04%   0.015%
212  28.476  3506 3510 3518 VV 10   21301    778155   0.09%   0.029%
213  28.584  3518 3525 3541 VV 3   49853   2311067   0.26%   0.085%
214  28.703  3541 3543 3549 VV 7   18735    567441   0.06%   0.021%
215  28.758  3549 3550 3561 VV 10   17693    760736   0.08%   0.028%
 
216  28.848  3561 3564 3568 VV 6   16038    450215   0.05%   0.017%
217  29.005  3582 3586 3588 VV 5   12214    231249   0.03%   0.009%
218  29.077  3591 3596 3599 VV 6   15221    443308   0.05%   0.016%
219  29.234  3616 3619 3621 VV 4   14547    272134   0.03%   0.010%
220  29.275  3621 3625 3631 VV 8   15631    549386   0.06%   0.020%
 
221  29.409  3641 3644 3646 VV 3   12914    194168   0.02%   0.007%
222  29.436  3646 3648 3654 VV 7   14827    400527   0.04%   0.015%
223  29.550  3660 3664 3668 VV 7    9801    299827   0.03%   0.011%
224  30.507  3792 3802 3804 VV 10    4547    152726   0.02%   0.006%
225  30.646  3817 3822 3824 VV 6    4136     69525   0.01%   0.003%
 
226  31.155  3894 3895 3901 VV 6    2488     29916   0.00%   0.001%
227  31.515  3945 3947 3951 PV 5    2631     25455   0.00%   0.001%
228  31.974  4007 4013 4019 VV 9    6534    199478   0.02%   0.007%
229  32.311  4060 4062 4063 PV 2    2708     18481   0.00%   0.001%
 
 
                        ͣ 2718637551
