                                                ٷֱȱ

  ·  : C:\MSDCHEM\1\DATA\HUANGWENJIE\20190916GF14B2019\
  ļ  : Nip-24h-1.D                                         
  ɼ      : 16 Sep 2019  21:15
      : lvqi
  Ʒ      : Nip-24h-1
        :  
  ALS Ʒƿ: 5   Ʒ˻: 1

  ֲ  : autoint1.e
      : ѧվ

      : C:\MSDCHEM\1\METHODS\20181120-Ŵ-DB35MS-FINAL.M
        :  

  źţTIC: Nip-24h-1.D\data.ms

  ʱ ʼ 嶥 ֹ                       %
   #     ɨ ɨ ɨ             % ֵ   
 ---  ----- ----- ---- ---- ---  -------   -------  ------  -------
  1   4.322    25   34   46 PV     22678    545458   0.06%   0.018%
  2   4.517    53   62   70 VV 2   34795   1143143   0.12%   0.037%
  3   4.622    70   77   90 VV 7   16900    687532   0.07%   0.022%
  4   4.789    97  101  110 VV 5    4680    140269   0.01%   0.005%
  5   4.907   110  118  123 PV     34962    827379   0.09%   0.027%
 
  6   4.998   123  131  145 VV   1024171  22799908   2.44%   0.734%
  7   5.472   192  199  204 VV 2   12238    280929   0.03%   0.009%
  8   5.525   204  207  214 VV 2    7681    206829   0.02%   0.007%
  9   5.862   250  256  263 VV 6    7748    206226   0.02%   0.007%
 10   6.289   311  317  323 VV 2    7930    180193   0.02%   0.006%
 
 11   6.397   323  332  343 VV 2   11056    388454   0.04%   0.012%
 12   6.510   343  349  358 VV 8    6219    184134   0.02%   0.006%
 13   6.641   358  368  376 VV    114280   2769673   0.30%   0.089%
 14   7.184   436  446  453 PV    383781   8196853   0.88%   0.264%
 15   7.257   453  456  467 VV 8    8482    226003   0.02%   0.007%
 
 16   7.455   477  485  488 VV 6    4939    118213   0.01%   0.004%
 17   7.508   488  492  501 VV 6    6900    196973   0.02%   0.006%
 18   7.622   501  509  522 VV    258143   5649465   0.60%   0.182%
 19   7.765   522  529  540 VV     37567    829360   0.09%   0.027%
 20   7.883   540  546  555 VV     94527   2009778   0.21%   0.065%
 
 21   8.093   566  576  584 VV    369557   7784007   0.83%   0.250%
 22   8.169   584  587  598 VV 3   20013    588225   0.06%   0.019%
 23   8.314   602  608  620 VV    133240   2966245   0.32%   0.095%
 24   8.777   667  675  684 PV    141728   3040243   0.32%   0.098%
 25   8.868   684  688  696 VV 7    3298     78297   0.01%   0.003%
 
 26   8.974   696  703  709 VV    198168   3977398   0.42%   0.128%
 27   9.034   709  712  726 VV 4   12274    327053   0.03%   0.011%
 28   9.227   730  740  750 VV   5802862 114443498  12.23%   3.682%
 29   9.320   750  753  759 VV     60621   1580086   0.17%   0.051%
 30   9.417   759  767  781 VV   3528681  67917090   7.26%   2.185%
 
 31   9.536   781  784  788 VV 4   16013    418745   0.04%   0.013%
 32   9.633   792  798  803 VV    146928   3150970   0.34%   0.101%
 33   9.682   803  805  821 VV 6   31911   1267428   0.14%   0.041%
 34   9.814   821  824  831 VV 6   13244    438881   0.05%   0.014%
 35   9.914   831  839  846 VV 4   15620    664315   0.07%   0.021%
 
 36  10.051   850  858  864 VV   3334323  61193844   6.54%   1.969%
 37  10.100   864  865  875 VV    148840   2595280   0.28%   0.083%
 38  10.287   882  892  894 VV 2  168031   3886882   0.42%   0.125%
 39  10.331   894  899  902 VV    742254  13797685   1.47%   0.444%
 40  10.375   902  905  913 VV    402041   7473590   0.80%   0.240%
 
 41  10.475   913  919  924 VV 2   31780    779073   0.08%   0.025%
 42  10.534   924  928  931 VV     30692    627268   0.07%   0.020%
 43  10.580   931  934  946 VV     29326    793350   0.08%   0.026%
 44  10.866   968  976  981 VV 8    5285    189959   0.02%   0.006%
 45  10.946   981  987  993 VV 5    9586    331734   0.04%   0.011%
 
 46  11.011   993  996 1001 VV 3   10477    262544   0.03%   0.008%
 47  11.119  1001 1012 1022 VV     80525   1849093   0.20%   0.059%
 48  11.226  1022 1027 1037 VV     96710   1918713   0.20%   0.062%
 49  11.349  1040 1045 1049 VV 5   11005    255643   0.03%   0.008%
 50  11.400  1049 1052 1059 VV 3   11496    334040   0.04%   0.011%
 
 51  11.625  1078 1085 1091 VV 8    5004    155946   0.02%   0.005%
 52  11.712  1091 1097 1106 VV 4   22268    606116   0.06%   0.020%
 53  11.815  1106 1112 1117 VV 2    8889    213503   0.02%   0.007%
 54  11.886  1117 1122 1133 VV 2   32263    860994   0.09%   0.028%
 55  12.045  1140 1145 1157 VV 7   12161    337491   0.04%   0.011%
 
 56  12.218  1160 1170 1174 VV 8   15014    509101   0.05%   0.016%
 57  12.274  1174 1178 1184 VV 7   11502    265038   0.03%   0.009%
 58  12.403  1190 1197 1201 VV 8    8018    237740   0.03%   0.008%
 59  12.457  1201 1205 1208 VV 6    5576    112946   0.01%   0.004%
 60  12.519  1208 1213 1228 VV 9   16444    802101   0.09%   0.026%
 
 61  12.721  1228 1242 1257 VV   4826687  82862802   8.85%   2.666%
 62  12.832  1257 1258 1260 VV 3   10392    113444   0.01%   0.004%
 63  12.865  1260 1263 1268 VV 5   11101    312534   0.03%   0.010%
 64  12.960  1268 1277 1284 VV 5   19216    734350   0.08%   0.024%
 65  13.064  1284 1292 1299 VV    611334  11054468   1.18%   0.356%
 
 66  13.138  1299 1302 1308 VV 3   28322    722065   0.08%   0.023%
 67  13.229  1308 1316 1337 VV   4019700  72723437   7.77%   2.340%
 68  13.489  1343 1353 1369 VV 8   75145   4198473   0.45%   0.135%
 69  13.633  1369 1374 1379 VV 4   38093   1071407   0.11%   0.034%
 70  13.746  1379 1390 1399 VV 3   98290   3318337   0.35%   0.107%
 
 71  13.921  1399 1415 1423 VV    664106  14111080   1.51%   0.454%
 72  13.989  1423 1425 1430 VV 6   18684    462903   0.05%   0.015%
 73  14.096  1433 1440 1446 VV 2   39817   1213778   0.13%   0.039%
 74  14.175  1446 1452 1459 VV 2   43777   1139918   0.12%   0.037%
 75  14.267  1459 1465 1470 VV 2   40573   1067598   0.11%   0.034%
 
 76  14.356  1470 1478 1488 VV    205330   4649258   0.50%   0.150%
 77  14.457  1488 1492 1494 VV 4   28290    616354   0.07%   0.020%
 78  14.499  1494 1498 1507 VV 4   59129   1970750   0.21%   0.063%
 79  14.615  1507 1515 1526 VV   1379878  30726381   3.28%   0.989%
 80  14.734  1526 1532 1536 VV    472135   9556160   1.02%   0.307%
 
 81  14.796  1536 1541 1557 VV   4813394  83363760   8.91%   2.682%
 82  14.977  1557 1567 1572 VV 7   23549   1130759   0.12%   0.036%
 83  15.090  1572 1583 1589 VV    252502   5371388   0.57%   0.173%
 84  15.158  1589 1593 1598 VV     73397   1550482   0.17%   0.050%
 85  15.275  1598 1610 1616 VV 4   68642   2564830   0.27%   0.083%
 
 86  15.351  1616 1621 1628 VV     71593   1681038   0.18%   0.054%
 87  15.434  1628 1633 1636 VV 2   36541    896663   0.10%   0.029%
 88  15.498  1636 1642 1649 VV    305563   5844092   0.62%   0.188%
 89  15.585  1649 1655 1674 VV    107562   3181056   0.34%   0.102%
 90  15.818  1678 1688 1693 VV    104783   2506635   0.27%   0.081%
 
 91  15.866  1693 1695 1702 VV 4   25405    565743   0.06%   0.018%
 92  16.001  1702 1715 1720 VV 3  188852   4977006   0.53%   0.160%
 93  16.093  1720 1728 1737 VV   5382140  89712634   9.58%   2.886%
 94  16.184  1737 1741 1750 VV     77445   2121005   0.23%   0.068%
 95  16.295  1750 1757 1760 VV 3   60544   1719048   0.18%   0.055%
 
 96  16.358  1760 1766 1771 VV    670908  12427355   1.33%   0.400%
 97  16.427  1771 1776 1785 VV    323912   8903917   0.95%   0.286%
 98  16.524  1785 1790 1807 VV 2  106025   3394105   0.36%   0.109%
 99  16.658  1807 1809 1812 VV 4   15070    291740   0.03%   0.009%
100  16.721  1812 1818 1823 VV     55623   1233874   0.13%   0.040%
 
101  16.822  1823 1833 1841 VV 3   70321   2106797   0.23%   0.068%
102  17.004  1841 1859 1865 VV   14125503 264778412  28.29%   8.519%
103  17.081  1865 1870 1876 VV 2  412165   8775297   0.94%   0.282%
104  17.181  1876 1884 1891 VV   9624470 180143338  19.25%   5.796%
105  17.246  1891 1894 1900 VV    323442   7316799   0.78%   0.235%
 
106  17.350  1900 1909 1913 VV   19781645 374983847  40.06%  12.064%
107  17.404  1913 1917 1930 VV   6902409 120335066  12.86%   3.872%
108  17.551  1930 1938 1941 VV 3 1895513  38552067   4.12%   1.240%
109  17.601  1941 1945 1953 VV   3933559  72323984   7.73%   2.327%
110  17.676  1953 1956 1961 VV 3   59820   1564446   0.17%   0.050%
 
111  17.799  1968 1973 1984 VV 9   61554   2384001   0.25%   0.077%
112  17.919  1984 1991 1998 VV 6   48876   1760541   0.19%   0.057%
113  18.010  1998 2004 2008 VV 2   42168   1180921   0.13%   0.038%
114  18.088  2008 2015 2020 VV    516416   9478154   1.01%   0.305%
115  18.137  2020 2022 2043 VV     49486   2220991   0.24%   0.071%
 
116  18.383  2043 2057 2060 VV 6   61408   2034660   0.22%   0.065%
117  18.449  2060 2067 2080 VV 4  112331   3935915   0.42%   0.127%
118  18.590  2080 2087 2097 VV     97737   2391470   0.26%   0.077%
119  18.675  2097 2099 2101 VV 3   15503    263809   0.03%   0.008%
120  18.732  2101 2108 2113 VV 2  107917   2458790   0.26%   0.079%
 
121  18.799  2113 2117 2123 VV 3   17673    520154   0.06%   0.017%
122  18.889  2123 2130 2138 VV    154099   3489925   0.37%   0.112%
123  18.953  2138 2139 2147 VV 7   11864    351719   0.04%   0.011%
124  19.092  2154 2159 2164 VV     64442   1404476   0.15%   0.045%
125  19.159  2164 2169 2179 VV 2   58128   1422541   0.15%   0.046%
 
126  19.261  2179 2184 2188 VV 6    7611    211302   0.02%   0.007%
127  19.382  2191 2201 2213 VV   3457960  79042940   8.44%   2.543%
128  19.504  2213 2219 2228 VV    184830   4150740   0.44%   0.134%
129  19.604  2228 2233 2241 VV 2   38374    958051   0.10%   0.031%
130  19.745  2248 2253 2262 VV 5   28528    780878   0.08%   0.025%
 
131  19.842  2262 2267 2269 VV 6    5722    120043   0.01%   0.004%
132  19.898  2269 2275 2284 VV     69284   1616856   0.17%   0.052%
133  20.007  2284 2291 2302 VV     15161    704537   0.08%   0.023%
134  20.177  2308 2316 2322 VV 7   11714    348292   0.04%   0.011%
135  20.296  2322 2333 2338 VV 3   38126   1214014   0.13%   0.039%
 
136  20.351  2338 2341 2351 VV 8   23912    730665   0.08%   0.024%
137  20.495  2351 2361 2366 VV 10    8330    344408   0.04%   0.011%
138  20.617  2370 2379 2388 VV 3   77030   2197200   0.23%   0.071%
139  20.715  2388 2393 2398 VV 8    7382    236464   0.03%   0.008%
140  20.827  2403 2409 2419 VV 5   32569    912068   0.10%   0.029%
 
141  20.933  2419 2424 2432 VV 5    8657    239755   0.03%   0.008%
142  21.059  2432 2443 2456 VV     55290   1595081   0.17%   0.051%
143  21.216  2460 2465 2472 VV 9    6485    198229   0.02%   0.006%
144  21.404  2488 2492 2497 VV 7    6375    141364   0.02%   0.005%
145  21.590  2511 2519 2528 PV     19387    475214   0.05%   0.015%
 
146  21.710  2528 2536 2548 VV 5   14073    512534   0.05%   0.016%
147  21.942  2562 2570 2573 PV 6    6702    162243   0.02%   0.005%
148  22.004  2573 2578 2585 VV 5   18384    459225   0.05%   0.015%
149  22.093  2585 2591 2595 VV 9    5205    157473   0.02%   0.005%
150  22.296  2614 2621 2625 PV 5    8702    153980   0.02%   0.005%
 
151  22.390  2628 2634 2637 VV 6    4220    100274   0.01%   0.003%
152  22.450  2637 2643 2652 VV 4   48960   1023619   0.11%   0.033%
153  22.648  2665 2671 2673 VV 5   13450    231100   0.02%   0.007%
154  22.695  2673 2678 2686 VV    154597   3318135   0.35%   0.107%
155  22.781  2686 2690 2693 VV 4   24686    480716   0.05%   0.015%
 
156  22.825  2693 2697 2700 VV 3   35127    641139   0.07%   0.021%
157  22.883  2700 2705 2715 VV 6   51986   1509634   0.16%   0.049%
158  22.999  2715 2722 2738 VV    101946   2068711   0.22%   0.067%
159  23.145  2738 2743 2747 VV 6   14623    341140   0.04%   0.011%
160  23.213  2747 2753 2756 VV 2   33710    605626   0.06%   0.019%
 
161  23.255  2756 2758 2762 VV 2   26709    471134   0.05%   0.015%
162  23.305  2762 2766 2768 VV 4   18732    367723   0.04%   0.012%
163  23.348  2768 2772 2777 VV 7   33593    827905   0.09%   0.027%
164  23.421  2777 2782 2786 VV 2  191402   3199904   0.34%   0.103%
165  23.469  2786 2789 2798 VV     82748   1523954   0.16%   0.049%
 
166  23.582  2798 2806 2818 VV 3   45880   1225647   0.13%   0.039%
167  23.699  2818 2822 2828 VV 7    8856    203400   0.02%   0.007%
168  23.845  2831 2843 2849 VV 2  223399   5623858   0.60%   0.181%
169  23.911  2849 2853 2858 VV 6   26152    586705   0.06%   0.019%
170  23.972  2858 2862 2865 VV 6   14253    285404   0.03%   0.009%
 
171  24.019  2865 2868 2875 VV 5   26333    560632   0.06%   0.018%
172  24.111  2875 2882 2888 VV 6   19156    566351   0.06%   0.018%
173  24.191  2888 2893 2895 VV 3   11777    206762   0.02%   0.007%
174  24.214  2895 2897 2899 VV 3   10318    146774   0.02%   0.005%
175  24.244  2899 2901 2905 VV 3   13415    246620   0.03%   0.008%
 
176  24.314  2905 2911 2914 VV 7   11323    356385   0.04%   0.011%
177  24.350  2914 2916 2919 VV 3   10054    186536   0.02%   0.006%
178  24.395  2919 2923 2925 VV 2   22978    393721   0.04%   0.013%
179  24.449  2925 2930 2935 VV 5   32672    946130   0.10%   0.030%
180  24.512  2935 2939 2945 VV 7   23681    551897   0.06%   0.018%
 
181  24.618  2951 2955 2960 VV 3   11872    261944   0.03%   0.008%
182  24.720  2963 2969 2974 VV 8   16875    381730   0.04%   0.012%
183  24.882  2987 2993 2997 VV 4   27597    548290   0.06%   0.018%
184  24.966  2997 3005 3040 VV   33504837 935990639 100.00%  30.113%
185  25.229  3040 3043 3048 VV 7  101726   3117324   0.33%   0.100%
 
186  25.323  3048 3056 3061 VV    436806  10000617   1.07%   0.322%
187  25.380  3061 3064 3079 VV    248071   7465597   0.80%   0.240%
188  25.554  3079 3089 3097 VV 4  177243   7285468   0.78%   0.234%
189  25.668  3101 3106 3111 VV 2  196571   4814833   0.51%   0.155%
190  25.731  3111 3115 3128 VV 3   89591   4260024   0.46%   0.137%
 
191  25.878  3128 3136 3140 VV 5   57300   2076013   0.22%   0.067%
192  25.928  3140 3143 3152 VV 10   40059   1591421   0.17%   0.051%
193  26.043  3152 3160 3167 VV 7   54054   2518472   0.27%   0.081%
194  26.147  3167 3175 3177 VV 3  110210   2731003   0.29%   0.088%
195  26.190  3177 3181 3190 VV 2  166110   4468306   0.48%   0.144%
 
196  26.321  3196 3200 3203 VV 6   30777    769852   0.08%   0.025%
197  26.426  3212 3215 3219 VV 6   24575    638820   0.07%   0.021%
198  26.478  3219 3222 3225 VV 5   23302    515827   0.06%   0.017%
199  26.520  3225 3228 3231 VV 4   38347    703168   0.08%   0.023%
200  26.550  3231 3233 3237 VV 4   31412    731654   0.08%   0.024%
 
201  26.644  3241 3246 3250 VV 8   27719    822930   0.09%   0.026%
202  26.681  3250 3252 3257 VV 6   25187    574346   0.06%   0.018%
203  26.747  3257 3261 3263 VV     44412    784710   0.08%   0.025%
204  26.781  3263 3266 3271 VV 4   69832   1862341   0.20%   0.060%
205  26.850  3271 3276 3288 VV   1170113  21806840   2.33%   0.702%
 
206  26.948  3288 3290 3298 VV 7   54715   1558174   0.17%   0.050%
207  27.118  3308 3315 3318 VV 8   33183   1249692   0.13%   0.040%
208  27.160  3318 3320 3328 VV 9   28489    965773   0.10%   0.031%
209  27.227  3328 3330 3335 VV 6   21369    541293   0.06%   0.017%
210  27.286  3335 3339 3343 VV 7   34559    818531   0.09%   0.026%
 
211  27.330  3343 3345 3349 VV 5   21193    458159   0.05%   0.015%
212  27.493  3365 3368 3372 VV 6   24765    560537   0.06%   0.018%
213  27.546  3372 3376 3380 VV 3   25804    683177   0.07%   0.022%
214  27.591  3380 3383 3384 VV 3   19170    322704   0.03%   0.010%
215  27.615  3384 3386 3388 VV 3   21191    369257   0.04%   0.012%
 
216  27.649  3388 3391 3396 VV 7   22558    599214   0.06%   0.019%
217  27.810  3410 3414 3417 VV 5   23231    579556   0.06%   0.019%
218  27.894  3417 3426 3435 VV 10   36999   1717806   0.18%   0.055%
219  27.979  3435 3438 3445 VV 8   19756    697141   0.07%   0.022%
220  28.080  3445 3453 3459 VV 8   21735    944898   0.10%   0.030%
 
221  28.152  3459 3463 3465 VV 5   16719    417162   0.04%   0.013%
222  28.214  3465 3472 3476 VV 10   25308    885988   0.09%   0.029%
223  28.255  3476 3478 3480 VV 3   21426    309552   0.03%   0.010%
224  28.296  3480 3484 3490 VV 9   19959    714576   0.08%   0.023%
225  28.478  3501 3510 3514 VV 9   29351   1027770   0.11%   0.033%
 
226  28.515  3514 3515 3518 VV 3   19588    331432   0.04%   0.011%
227  28.587  3518 3526 3535 VV 4   54680   2143918   0.23%   0.069%
228  28.664  3535 3537 3548 VV 4   23178   1170667   0.13%   0.038%
229  28.756  3548 3550 3554 VV 5   20879    438849   0.05%   0.014%
230  28.805  3554 3557 3560 VV 5   20325    471393   0.05%   0.015%
 
231  28.849  3560 3564 3568 VV 7   21927    611174   0.07%   0.020%
232  29.027  3587 3589 3591 VV 3   15489    253678   0.03%   0.008%
233  29.076  3591 3596 3600 VV 8   16852    563860   0.06%   0.018%
234  29.131  3600 3604 3610 VV 9   15217    565350   0.06%   0.018%
235  29.238  3615 3620 3623 VV 7   15183    472176   0.05%   0.015%
 
236  29.353  3631 3636 3641 VV 9   16242    565879   0.06%   0.018%
237  29.434  3641 3648 3666 VV 3   40443   1771345   0.19%   0.057%
238  30.029  3730 3733 3737 VV 6    8789    206099   0.02%   0.007%
239  30.079  3737 3741 3751 VV 6    9079    375285   0.04%   0.012%
240  30.675  3822 3826 3840 VV 6    6721    343802   0.04%   0.011%
 
241  30.966  3863 3868 3871 VV 6    5262    136536   0.01%   0.004%
242  31.328  3918 3920 3927 VV 8    5077     88796   0.01%   0.003%
243  31.421  3932 3934 3938 VV 5    4349     47093   0.01%   0.002%
244  31.817  3986 3991 3993 VV 6    4639     86889   0.01%   0.003%
245  31.979  4005 4014 4020 VV 6    3775    119987   0.01%   0.004%
 
 
 
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