                                                ٷֱȱ

  ·  : C:\MSDCHEM\1\DATA\HUANGWENJIE\20190916GF14B2019\
  ļ  : Nip-24h-5.D                                         
  ɼ      : 17 Sep 2019  19:46
      : lvqi
  Ʒ      : Nip-24h-5
        :  
  ALS Ʒƿ: 41   Ʒ˻: 1

  ֲ  : autoint1.e
      : ѧվ

      : C:\MSDCHEM\1\METHODS\20181120-Ŵ-DB35MS-FINAL.M
        :  

  źţTIC: Nip-24h-5.D\data.ms

  ʱ ʼ 嶥 ֹ                       %
   #     ɨ ɨ ɨ             % ֵ   
 ---  ----- ----- ---- ---- ---  -------   -------  ------  -------
  1   4.217    14   19   25 PV 10    4299    101283   0.02%   0.003%
  2   4.324    28   34   46 VV 3   22239    533928   0.09%   0.017%
  3   4.515    46   62   70 VV 2   37426   1213824   0.20%   0.038%
  4   4.627    70   78   89 VV 7   14492    591249   0.10%   0.019%
  5   4.754    89   96  109 PV 7    3993    207912   0.03%   0.007%
 
  6   4.906   109  118  123 VV     39748    899958   0.15%   0.028%
  7   4.997   123  131  152 VV   1009142  22141317   3.61%   0.700%
  8   5.472   194  199  204 VV     13491    302790   0.05%   0.010%
  9   5.524   204  207  214 VV      8969    212428   0.03%   0.007%
 10   6.026   271  279  287 PV      3868    133850   0.02%   0.004%
 
 11   6.289   311  317  322 VV 3    7182    168505   0.03%   0.005%
 12   6.398   322  333  343 VV 3   11199    359806   0.06%   0.011%
 13   6.511   343  349  359 VV 10    5162    147714   0.02%   0.005%
 14   6.640   359  367  380 VV    128110   3011672   0.49%   0.095%
 15   7.183   435  446  453 PV    389845   8170528   1.33%   0.258%
 
 16   7.256   453  456  474 VV 8    9015    307160   0.05%   0.010%
 17   7.438   477  482  486 VV 7    4101     92497   0.02%   0.003%
 18   7.512   486  493  501 VV 5    6604    210856   0.03%   0.007%
 19   7.621   501  509  519 VV    267988   5827585   0.95%   0.184%
 20   7.763   519  529  539 VV     35438    774647   0.13%   0.024%
 
 21   7.882   539  546  553 VV     81960   1675892   0.27%   0.053%
 22   8.091   568  576  583 VV    306954   6376502   1.04%   0.201%
 23   8.173   583  588  596 VV 2   28267    719954   0.12%   0.023%
 24   8.313   596  608  623 VV    131363   2889430   0.47%   0.091%
 25   8.776   664  675  684 VV    144471   3004818   0.49%   0.095%
 
 26   8.973   695  703  709 VV    185380   3777213   0.62%   0.119%
 27   9.033   709  712  720 VV 4   11744    293069   0.05%   0.009%
 28   9.225   724  739  749 VV   6220896 117853959  19.19%   3.724%
 29   9.320   749  753  759 VV     68879   1747958   0.28%   0.055%
 30   9.415   759  767  780 VV   3130214  59207203   9.64%   1.871%
 
 31   9.531   780  784  788 VV 4   14528    388724   0.06%   0.012%
 32   9.632   788  798  803 VV    140521   3091404   0.50%   0.098%
 33   9.683   803  805  820 VV 5   33010   1186483   0.19%   0.037%
 34   9.819   820  825  830 VV 8   11692    397703   0.06%   0.013%
 35   9.921   830  840  846 VV 2   35632   1037422   0.17%   0.033%
 
 36  10.050   849  858  864 VV   3485369  63375028  10.32%   2.002%
 37  10.099   864  865  881 VV    143128   2739364   0.45%   0.087%
 38  10.286   881  892  894 VV 2  165240   3775693   0.61%   0.119%
 39  10.329   894  898  902 VV    777134  14097825   2.30%   0.445%
 40  10.374   902  905  913 VV    389671   7414668   1.21%   0.234%
 
 41  10.474   913  919  924 VV 3   32212    820446   0.13%   0.026%
 42  10.534   924  928  931 VV 2   36297    705216   0.11%   0.022%
 43  10.578   931  934  945 VV     26106    698043   0.11%   0.022%
 44  10.874   966  977  981 VV 9    5807    226865   0.04%   0.007%
 45  10.938   981  986  992 VV 6    7757    274511   0.04%   0.009%
 
 46  11.005   992  996 1001 VV 4   12223    297665   0.05%   0.009%
 47  11.117  1001 1012 1021 VV     76985   1913705   0.31%   0.060%
 48  11.225  1021 1027 1040 VV     90920   1927722   0.31%   0.061%
 49  11.351  1040 1045 1048 VV 5   12218    262435   0.04%   0.008%
 50  11.397  1048 1052 1070 VV 7   11404    543156   0.09%   0.017%
 
 51  11.625  1077 1085 1087 VV 9    5812    138166   0.02%   0.004%
 52  11.714  1092 1098 1107 VV 6   22843    629230   0.10%   0.020%
 53  11.817  1107 1112 1116 VV 2    9052    215526   0.04%   0.007%
 54  11.884  1116 1122 1129 VV     21448    597500   0.10%   0.019%
 55  12.044  1141 1145 1154 VV 6   13403    331199   0.05%   0.010%
 
 56  12.187  1154 1166 1167 VV 8   11905    293495   0.05%   0.009%
 57  12.214  1167 1170 1174 VV 4   14758    313586   0.05%   0.010%
 58  12.274  1174 1178 1184 VV 7   13132    304733   0.05%   0.010%
 59  12.406  1184 1197 1202 VV 5   15279    510085   0.08%   0.016%
 60  12.555  1208 1219 1227 VV 3   26560   1054173   0.17%   0.033%
 
 61  12.719  1227 1242 1249 VV   4742338  80902129  13.18%   2.556%
 62  12.775  1249 1250 1259 VV 2   40290    888137   0.14%   0.028%
 63  12.860  1259 1263 1270 VV 6   13976    507306   0.08%   0.016%
 64  12.955  1270 1276 1285 VV 5   17568    750014   0.12%   0.024%
 65  13.063  1285 1292 1298 VV 2  594189  10668234   1.74%   0.337%
 
 66  13.138  1298 1303 1308 VV 6   27536    727589   0.12%   0.023%
 67  13.228  1308 1315 1340 VV   4119159  75054955  12.22%   2.371%
 68  13.495  1340 1354 1369 VV 5  185207   9576497   1.56%   0.303%
 69  13.632  1369 1374 1378 VV 3   43803   1189246   0.19%   0.038%
 70  13.745  1378 1390 1398 VV 3   98653   3748529   0.61%   0.118%
 
 71  13.920  1398 1415 1424 VV    548431  12098352   1.97%   0.382%
 72  13.994  1424 1426 1433 VV 7   20603    597313   0.10%   0.019%
 73  14.098  1433 1441 1446 VV 3   41406   1203467   0.20%   0.038%
 74  14.173  1446 1451 1457 VV 3   40435   1032199   0.17%   0.033%
 75  14.267  1457 1465 1469 VV 3   38575   1115606   0.18%   0.035%
 
 76  14.354  1469 1478 1488 VV    306540   6585384   1.07%   0.208%
 77  14.456  1488 1492 1494 VV 3   26193    499620   0.08%   0.016%
 78  14.498  1494 1498 1506 VV 2   54132   1758181   0.29%   0.056%
 79  14.614  1506 1515 1525 VV   1292582  28571186   4.65%   0.903%
 80  14.733  1525 1532 1536 VV    699883  13424987   2.19%   0.424%
 
 81  14.796  1536 1541 1558 VV   4816496  82444881  13.43%   2.605%
 82  14.982  1558 1568 1573 VV 10   23270   1060284   0.17%   0.034%
 83  15.089  1573 1583 1589 VV    265052   5635853   0.92%   0.178%
 84  15.158  1589 1593 1598 VV 2   67701   1401398   0.23%   0.044%
 85  15.274  1598 1610 1615 VV 4   66924   2738095   0.45%   0.087%
 
 86  15.352  1615 1621 1628 VV 2   88128   1984720   0.32%   0.063%
 87  15.435  1628 1633 1636 VV 2   37374    939033   0.15%   0.030%
 88  15.497  1636 1642 1649 VV    280866   5491249   0.89%   0.174%
 89  15.584  1649 1655 1674 VV    228746   5307025   0.86%   0.168%
 90  15.817  1674 1688 1693 VV     94786   2448506   0.40%   0.077%
 
 91  15.867  1693 1695 1701 VV 3   23180    536578   0.09%   0.017%
 92  16.000  1701 1715 1720 VV 3  175122   4466494   0.73%   0.141%
 93  16.090  1720 1727 1737 VV   4689231  77874745  12.68%   2.461%
 94  16.183  1737 1741 1750 VV 2   76674   2302720   0.38%   0.073%
 95  16.296  1750 1757 1760 VV 4   53328   1517825   0.25%   0.048%
 
 96  16.357  1760 1766 1771 VV    729551  13073187   2.13%   0.413%
 97  16.425  1771 1776 1784 VV    213536   6101268   0.99%   0.193%
 98  16.521  1784 1789 1799 VV 2   94478   2759096   0.45%   0.087%
 99  16.655  1806 1809 1812 VV 4   13435    299221   0.05%   0.009%
100  16.722  1812 1818 1824 VV     48947   1158122   0.19%   0.037%
 
101  16.822  1824 1833 1841 VV 4   62669   1885844   0.31%   0.060%
102  17.004  1841 1859 1865 VV   14600171 274114388  44.65%   8.661%
103  17.081  1865 1870 1876 VV 3  426708   9167069   1.49%   0.290%
104  17.180  1876 1884 1891 VV   9994440 187138658  30.48%   5.913%
105  17.246  1891 1894 1900 VV    339403   7646207   1.25%   0.242%
 
106  17.350  1900 1909 1913 VV   20901474 391390081  63.75%  12.366%
107  17.404  1913 1917 1929 VV   7526856 128991768  21.01%   4.076%
108  17.550  1929 1937 1941 VV 2 2003281  40768465   6.64%   1.288%
109  17.600  1941 1945 1952 VV   4046197  74685227  12.16%   2.360%
110  17.677  1952 1956 1960 VV 2   55206   1500624   0.24%   0.047%
 
111  17.726  1960 1963 1968 VV 5   33967    882206   0.14%   0.028%
112  17.800  1968 1973 1984 VV 6   54651   2123959   0.35%   0.067%
113  17.919  1984 1991 1999 VV 10   45436   1704985   0.28%   0.054%
114  18.010  1999 2004 2008 VV 3   39755   1129175   0.18%   0.036%
115  18.087  2008 2015 2020 VV    503763   9264778   1.51%   0.293%
 
116  18.138  2020 2022 2033 VV 10   48530   1719554   0.28%   0.054%
117  18.227  2033 2035 2043 VV 8   18901    582504   0.09%   0.018%
118  18.317  2043 2048 2050 VV 6   14952    347640   0.06%   0.011%
119  18.384  2050 2058 2059 VV 6   59408   1459762   0.24%   0.046%
120  18.442  2059 2066 2081 VV 6  122626   4820406   0.79%   0.152%
 
121  18.589  2081 2087 2096 VV     89352   2195530   0.36%   0.069%
122  18.678  2096 2100 2102 VV 3   15340    323395   0.05%   0.010%
123  18.731  2102 2108 2113 VV 2   96114   2169781   0.35%   0.069%
124  18.796  2113 2117 2123 VV 5   18134    525657   0.09%   0.017%
125  18.889  2123 2130 2138 VV    139931   3158025   0.51%   0.100%
 
126  18.956  2138 2140 2147 VV 7   13553    355830   0.06%   0.011%
127  19.091  2153 2159 2164 VV     57318   1314689   0.21%   0.042%
128  19.158  2164 2169 2177 VV 3   44186   1164387   0.19%   0.037%
129  19.381  2191 2201 2213 VV   3534565  81957374  13.35%   2.590%
130  19.503  2213 2219 2227 VV    196573   4264826   0.69%   0.135%
 
131  19.602  2227 2233 2240 VV 4   18435    605864   0.10%   0.019%
132  19.743  2247 2253 2262 VV 4   27038    778675   0.13%   0.025%
133  19.898  2269 2275 2283 VV     68947   1580044   0.26%   0.050%
134  20.004  2283 2291 2303 VV 8   26547   1109123   0.18%   0.035%
135  20.167  2308 2314 2321 VV 10   10496    347773   0.06%   0.011%
 
136  20.296  2325 2333 2337 VV 4   37330   1182625   0.19%   0.037%
137  20.349  2337 2340 2350 VV 3   38610   1099262   0.18%   0.035%
138  20.479  2350 2359 2366 VV 9    9560    360906   0.06%   0.011%
139  20.616  2370 2379 2392 VV 4   69264   2178654   0.35%   0.069%
140  20.717  2392 2393 2396 VV 3    7092    105102   0.02%   0.003%
 
141  20.826  2403 2409 2419 VV 8   19796    623216   0.10%   0.020%
142  20.935  2419 2425 2433 VV 7    6923    200208   0.03%   0.006%
143  21.058  2433 2442 2458 VV     81043   2236778   0.36%   0.071%
144  21.205  2458 2463 2476 VV      8363    323663   0.05%   0.010%
145  21.400  2485 2492 2498 VV 8    6384    167390   0.03%   0.005%
 
146  21.590  2509 2519 2528 PV 3   16400    491068   0.08%   0.016%
147  21.706  2528 2536 2546 VV 5   13636    463357   0.08%   0.015%
148  21.936  2562 2569 2573 VV 7    5623    134751   0.02%   0.004%
149  22.006  2573 2579 2585 VV 5   19253    443534   0.07%   0.014%
150  22.087  2585 2590 2595 PV 8    5134    130356   0.02%   0.004%
 
151  22.295  2610 2620 2629 VV 8    9013    203270   0.03%   0.006%
152  22.386  2629 2633 2637 VV 5    4117     76808   0.01%   0.002%
153  22.448  2637 2642 2653 PV 4   48510    983677   0.16%   0.031%
154  22.589  2659 2663 2665 VV 5    3843     53076   0.01%   0.002%
155  22.646  2665 2671 2673 VV 6   12544    235935   0.04%   0.007%
 
156  22.693  2673 2678 2686 VV    145277   3047682   0.50%   0.096%
157  22.780  2686 2690 2693 VV 4   22364    403658   0.07%   0.013%
158  22.821  2693 2696 2699 VV 2   27323    514582   0.08%   0.016%
159  22.881  2699 2705 2715 VV 8   47053   1419326   0.23%   0.045%
160  22.997  2715 2721 2728 VV 2   77563   1444256   0.24%   0.046%
 
161  23.069  2728 2732 2735 VV 5    7769    182082   0.03%   0.006%
162  23.143  2738 2742 2748 VV 9   15105    369268   0.06%   0.012%
163  23.212  2748 2752 2756 VV 3   32715    588164   0.10%   0.019%
164  23.254  2756 2758 2762 VV 3   26308    498753   0.08%   0.016%
165  23.302  2762 2765 2767 VV 3   24923    431327   0.07%   0.014%
 
166  23.349  2767 2772 2777 VV 3   54045   1299963   0.21%   0.041%
167  23.420  2777 2782 2786 VV    194017   3244820   0.53%   0.103%
168  23.466  2786 2789 2797 VV     79369   1566456   0.26%   0.049%
169  23.581  2797 2806 2812 VV 4   49382   1375640   0.22%   0.043%
170  23.690  2816 2821 2826 VV 8    9296    282293   0.05%   0.009%
 
171  23.842  2831 2843 2849 VV 2  218911   5814938   0.95%   0.184%
172  23.907  2849 2852 2858 VV 6   26122    617607   0.10%   0.020%
173  23.974  2858 2862 2864 VV 5   18018    330158   0.05%   0.010%
174  24.016  2864 2868 2875 VV 4   27351    633194   0.10%   0.020%
175  24.112  2875 2882 2889 VV 9   19557    554174   0.09%   0.018%
 
176  24.189  2889 2893 2895 VV 2   10720    204827   0.03%   0.006%
177  24.245  2895 2901 2904 VV 4   15516    390638   0.06%   0.012%
178  24.314  2904 2911 2913 VV 7   13145    379587   0.06%   0.012%
179  24.350  2913 2916 2919 VV 5   10866    198235   0.03%   0.006%
180  24.393  2919 2922 2925 VV 3   22058    350545   0.06%   0.011%
 
181  24.436  2925 2929 2934 VV 7   24215    598971   0.10%   0.019%
182  24.514  2934 2940 2944 VV 6   22625    477908   0.08%   0.015%
183  24.618  2948 2955 2958 VV 3   14511    344422   0.06%   0.011%
184  24.712  2963 2968 2972 VV 5   17556    408575   0.07%   0.013%
185  24.752  2972 2974 2981 VV 7    8291    241133   0.04%   0.008%
 
186  24.823  2981 2984 2988 VV 6    7584    181663   0.03%   0.006%
187  24.882  2988 2993 2997 VV 3   28982    555960   0.09%   0.018%
188  24.965  2997 3005 3007 VV   34807930 613984873 100.00%  19.399%
189  24.986  3007 3008 3039 VV   31815483 339160740  55.24%  10.716%
190  25.224  3039 3042 3050 VV 5   78525   3243112   0.53%   0.102%
 
191  25.323  3050 3056 3061 VV    513553   9176803   1.49%   0.290%
192  25.380  3061 3064 3078 VV    234553   6408115   1.04%   0.202%
193  25.552  3078 3089 3101 VV 4  169537   7484161   1.22%   0.236%
194  25.667  3101 3106 3111 VV 2  186773   4474858   0.73%   0.141%
195  25.724  3111 3114 3119 VV 4  104878   2922632   0.48%   0.092%
 
196  25.772  3119 3121 3128 VV 3   71022   1856165   0.30%   0.059%
197  25.876  3131 3136 3140 VV 5   58022   1699594   0.28%   0.054%
198  25.924  3140 3143 3153 VV 10   43930   1775911   0.29%   0.056%
199  26.043  3153 3160 3166 VV 5   60326   2505243   0.41%   0.079%
200  26.147  3166 3175 3178 VV 4  117372   3316089   0.54%   0.105%
 
201  26.195  3178 3182 3190 VV 2  136116   3435602   0.56%   0.109%
202  26.274  3190 3193 3196 VV 4   30761    623826   0.10%   0.020%
203  26.320  3196 3200 3212 VV 10   32055   1624465   0.26%   0.051%
204  26.428  3212 3215 3219 VV 6   27977    639787   0.10%   0.020%
205  26.478  3219 3222 3225 VV 5   25039    605575   0.10%   0.019%
 
206  26.519  3225 3228 3230 VV 3   40013    714313   0.12%   0.023%
207  26.551  3230 3233 3241 VV 7   36008   1181819   0.19%   0.037%
208  26.649  3241 3247 3256 VV 7   29007   1499256   0.24%   0.047%
209  26.746  3256 3261 3263 VV     44664    816526   0.13%   0.026%
210  26.780  3263 3266 3271 VV 5   73075   1925109   0.31%   0.061%
 
211  26.849  3271 3276 3288 VV   1002270  18292368   2.98%   0.578%
212  26.948  3288 3290 3301 VV 8   48858   1916652   0.31%   0.061%
213  27.055  3301 3305 3308 VV 5   29158    777511   0.13%   0.025%
214  27.091  3308 3311 3312 VV 3   31521    439787   0.07%   0.014%
215  27.120  3312 3315 3318 VV 3   32980    791682   0.13%   0.025%
 
216  27.158  3318 3320 3335 VV 3   31069   1619204   0.26%   0.051%
217  27.285  3335 3338 3341 VV 5   38919    739678   0.12%   0.023%
218  27.336  3341 3346 3349 VV 7   23732    718832   0.12%   0.023%
219  27.374  3349 3351 3354 VV 4   21598    378666   0.06%   0.012%
220  27.493  3362 3368 3371 VV 7   23674    756002   0.12%   0.024%
 
221  27.543  3371 3376 3380 VV 7   23411    699741   0.11%   0.022%
222  27.585  3380 3382 3384 VV 3   19969    324454   0.05%   0.010%
223  27.640  3384 3390 3395 VV 9   23140    909619   0.15%   0.029%
224  27.750  3403 3405 3407 VV 3   17434    246616   0.04%   0.008%
225  27.807  3407 3414 3417 VV 9   22853    723917   0.12%   0.023%
 
226  27.893  3417 3426 3430 VV 9   36577   1318973   0.21%   0.042%
227  27.937  3430 3432 3435 VV 3   20628    364604   0.06%   0.012%
228  27.973  3435 3438 3444 VV 8   18289    559017   0.09%   0.018%
229  28.072  3444 3452 3462 VV 8   18454   1070400   0.17%   0.034%
230  28.212  3462 3472 3475 VV 5   26657    948811   0.15%   0.030%
 
231  28.252  3475 3478 3481 VV 5   22371    467846   0.08%   0.015%
232  28.295  3481 3484 3494 VV 5   22369    877657   0.14%   0.028%
233  28.393  3494 3498 3506 VV 5   15410    714983   0.12%   0.023%
234  28.479  3506 3510 3514 VV 4   35116    807382   0.13%   0.026%
235  28.520  3514 3516 3519 VV 4   18306    330293   0.05%   0.010%
 
236  28.586  3519 3526 3533 VV 3   58598   2110154   0.34%   0.067%
237  28.651  3533 3535 3537 VV 3   23180    294232   0.05%   0.009%
238  28.675  3537 3538 3541 VV 3   22438    346606   0.06%   0.011%
239  28.704  3541 3543 3548 VV 6   22118    646999   0.11%   0.020%
240  28.852  3560 3564 3569 VV 5   23666    704238   0.11%   0.022%
 
241  28.903  3569 3571 3583 VV 5   18343    855915   0.14%   0.027%
242  29.073  3583 3596 3598 VV 5   14910    765268   0.12%   0.024%
243  29.097  3598 3599 3604 VV 5   14087    348026   0.06%   0.011%
244  29.237  3613 3619 3622 VV 8   17705    540854   0.09%   0.017%
245  29.270  3622 3624 3628 VV 5   16134    377012   0.06%   0.012%
 
246  29.310  3628 3630 3631 VV 2   14904    176441   0.03%   0.006%
247  29.353  3631 3636 3641 VV 6   21427    662549   0.11%   0.021%
248  29.433  3641 3648 3658 VV 2   49831   1617351   0.26%   0.051%
249  30.077  3731 3740 3743 VV 8    8637    277624   0.05%   0.009%
250  30.491  3794 3800 3804 VV 9    4951    103120   0.02%   0.003%
 
251  30.698  3828 3830 3835 VV 5    3937     64111   0.01%   0.002%
252  31.015  3872 3875 3881 VV 8    3272     59998   0.01%   0.002%
253  31.820  3985 3991 3998 VV 8    7190    211157   0.03%   0.007%
254  31.966  4005 4012 4020 PV 8    5001    175040   0.03%   0.006%
 
 
                        ͣ 3164981180
