                                                ٷֱȱ

  ·  : C:\MSDCHEM\1\DATA\HUANGWENJIE\20190916GF14B2019\
  ļ  : QC-20190916-d1.D                                    
  ɼ      : 17 Sep 2019  12:53
      : lvqi
  Ʒ      : QC-20190916-d1
        :  
  ALS Ʒƿ: 30   Ʒ˻: 1

  ֲ  : autoint1.e
      : ѧվ

      : C:\MSDCHEM\1\METHODS\20181120-Ŵ-DB35MS-FINAL.M
        :  

  źţTIC: QC-20190916-d1.D\data.ms

  ʱ ʼ 嶥 ֹ                       %
   #     ɨ ɨ ɨ             % ֵ   
 ---  ----- ----- ---- ---- ---  -------   -------  ------  -------
  1   4.325    26   34   43 PV 2   27926    660122   0.08%   0.022%
  2   4.512    49   61   71 PV 2   28425    951590   0.11%   0.032%
  3   4.639    71   80   81 VV 6    8869    227486   0.03%   0.008%
  4   4.663    81   83   88 VV 4   10405    194465   0.02%   0.007%
  5   4.906   108  118  123 PV     44245    994129   0.12%   0.033%
 
  6   4.997   123  131  144 VV   1114650  24158570   2.90%   0.813%
  7   5.474   189  200  203 PV     18590    383482   0.05%   0.013%
  8   5.525   203  207  216 VV     10763    256495   0.03%   0.009%
  9   5.854   252  254  260 VV 7    4512     74373   0.01%   0.003%
 10   6.015   274  277  279 VV 3    4093     54896   0.01%   0.002%
 
 11   6.036   279  280  286 VV 5    4643     66231   0.01%   0.002%
 12   6.281   313  316  322 VV 3    4464    108461   0.01%   0.004%
 13   6.390   322  332  340 VV 3    8552    279335   0.03%   0.009%
 14   6.514   343  349  352 PV 6    3401     73347   0.01%   0.002%
 15   6.639   359  367  379 VV    141880   3353854   0.40%   0.113%
 
 16   7.182   435  445  453 VV    368361   7746360   0.93%   0.261%
 17   7.247   453  455  466 VV 6    7201    215317   0.03%   0.007%
 18   7.441   478  483  486 VV 6    3991     87626   0.01%   0.003%
 19   7.509   486  492  501 VV 6    6003    178610   0.02%   0.006%
 20   7.621   501  509  518 VV    422541   8992707   1.08%   0.303%
 
 21   7.763   522  529  536 VV     37040    783840   0.09%   0.026%
 22   7.882   536  546  557 VV    200498   4226296   0.51%   0.142%
 23   8.091   568  576  584 VV    418558   8585889   1.03%   0.289%
 24   8.171   584  588  600 VV     27165    784338   0.09%   0.026%
 25   8.314   600  608  620 VV    148974   3216533   0.39%   0.108%
 
 26   8.776   666  675  683 VV    167445   3377669   0.40%   0.114%
 27   8.973   694  703  710 PV    212713   4360886   0.52%   0.147%
 28   9.034   710  712  720 VV 6    9022    189898   0.02%   0.006%
 29   9.226   730  740  750 BV   6348472 120847564  14.49%   4.068%
 30   9.320   750  753  759 VV     56798   1414651   0.17%   0.048%
 
 31   9.415   759  767  779 VV   3205887  60439652   7.25%   2.035%
 32   9.539   779  785  791 VV 8   11772    423824   0.05%   0.014%
 33   9.632   791  798  803 VV    106542   2225521   0.27%   0.075%
 34   9.684   803  806  821 VV 6   29819   1138601   0.14%   0.038%
 35   9.921   832  840  847 VV 2   40207   1069315   0.13%   0.036%
 
 36  10.049   847  858  863 VV   2116685  38884960   4.66%   1.309%
 37  10.099   863  865  876 VV    140839   2605323   0.31%   0.088%
 38  10.287   882  892  894 VV    189720   4061448   0.49%   0.137%
 39  10.330   894  898  902 VV    793915  14438768   1.73%   0.486%
 40  10.374   902  905  913 VV    373156   7014776   0.84%   0.236%
 
 41  10.475   913  919  924 VV     41478    871838   0.10%   0.029%
 42  10.532   924  928  932 VV     30979    604862   0.07%   0.020%
 43  10.580   932  934  947 VV     16735    432912   0.05%   0.015%
 44  10.863   971  975  981 VV 6    5048    118270   0.01%   0.004%
 45  10.956   981  989  991 VV 5    6154    181532   0.02%   0.006%
 
 46  11.006   991  996 1003 VV 7    9528    279408   0.03%   0.009%
 47  11.117  1003 1012 1021 VV     73187   1686476   0.20%   0.057%
 48  11.225  1021 1027 1040 VV     69660   1470032   0.18%   0.049%
 49  11.348  1040 1045 1049 VV 4   10324    242629   0.03%   0.008%
 50  11.426  1049 1056 1060 VV 4   10742    334482   0.04%   0.011%
 
 51  11.717  1092 1098 1105 VV 5   18015    430621   0.05%   0.014%
 52  11.815  1105 1112 1117 PV 3    8588    169827   0.02%   0.006%
 53  11.884  1117 1122 1133 VV 3   15537    449750   0.05%   0.015%
 54  12.045  1138 1145 1153 VV 5   11869    281977   0.03%   0.009%
 55  12.192  1159 1166 1168 VV 5    5808    128882   0.02%   0.004%
 
 56  12.218  1168 1170 1174 VV 5    6942    114343   0.01%   0.004%
 57  12.275  1174 1178 1184 VV 4   12502    263147   0.03%   0.009%
 58  12.408  1189 1198 1202 VV 4   12109    325172   0.04%   0.011%
 59  12.555  1207 1219 1229 VV 5   30474    957174   0.11%   0.032%
 60  12.720  1229 1242 1257 VV   4799033  81562789   9.78%   2.746%
 
 61  12.862  1257 1263 1269 VV 8   11291    399939   0.05%   0.013%
 62  12.957  1269 1277 1284 VV 9   14595    647080   0.08%   0.022%
 63  13.064  1284 1292 1299 VV   1018533  18056637   2.16%   0.608%
 64  13.137  1299 1303 1308 VV 4   19999    564207   0.07%   0.019%
 65  13.227  1308 1315 1321 VV   2266287  38638587   4.63%   1.301%
 
 66  13.273  1321 1322 1335 VV 2  149272   3125279   0.37%   0.105%
 67  13.489  1335 1353 1369 VV 6  211278  10449954   1.25%   0.352%
 68  13.631  1369 1374 1379 VV 6   32996    975079   0.12%   0.033%
 69  13.745  1379 1390 1399 VV 3   94762   3492855   0.42%   0.118%
 70  13.823  1399 1401 1402 VV 2   19231    234599   0.03%   0.008%
 
 71  13.921  1402 1415 1423 VV    381875   8367800   1.00%   0.282%
 72  14.095  1435 1440 1447 VV 5   28302    847127   0.10%   0.029%
 73  14.173  1447 1452 1459 VV 3   37697    949565   0.11%   0.032%
 74  14.264  1459 1465 1470 VV 4   24922    684642   0.08%   0.023%
 75  14.355  1470 1478 1488 VV    291957   6052268   0.73%   0.204%
 
 76  14.456  1488 1492 1494 VV 4   21076    436875   0.05%   0.015%
 77  14.499  1494 1499 1507 VV 3   50415   1668143   0.20%   0.056%
 78  14.613  1507 1515 1525 VV   1235059  24618553   2.95%   0.829%
 79  14.734  1525 1532 1536 VV    789404  15165205   1.82%   0.511%
 80  14.795  1536 1541 1558 VV   2999626  52113295   6.25%   1.754%
 
 81  14.977  1558 1567 1574 VV     18203    945298   0.11%   0.032%
 82  15.089  1574 1583 1589 VV    144634   3165410   0.38%   0.107%
 83  15.158  1589 1593 1598 VV 2   43108    944785   0.11%   0.032%
 84  15.276  1598 1610 1616 VV 5   70433   2432661   0.29%   0.082%
 85  15.351  1616 1621 1628 VV 2   66449   1518294   0.18%   0.051%
 
 86  15.435  1628 1633 1637 VV     39131    904614   0.11%   0.030%
 87  15.498  1637 1642 1648 VV    167772   3380956   0.41%   0.114%
 88  15.584  1648 1655 1667 VV    298671   5935704   0.71%   0.200%
 89  15.817  1679 1688 1692 VV     47785   1259715   0.15%   0.042%
 90  15.863  1692 1695 1702 VV 5   26330    597503   0.07%   0.020%
 
 91  16.001  1702 1715 1720 VV 2  156987   4102077   0.49%   0.138%
 92  16.092  1720 1728 1738 VV   5616614  92203804  11.05%   3.104%
 93  16.185  1738 1741 1751 VV 3   49645   1694604   0.20%   0.057%
 94  16.296  1751 1757 1760 VV 5   39572   1090982   0.13%   0.037%
 95  16.358  1760 1766 1771 VV    962663  17267167   2.07%   0.581%
 
 96  16.425  1771 1776 1785 VV    201352   5696281   0.68%   0.192%
 97  16.524  1785 1790 1806 VV 4   76420   2521226   0.30%   0.085%
 98  16.723  1812 1818 1825 VV 2   41615   1006063   0.12%   0.034%
 99  16.822  1825 1833 1840 VV 4   57390   1611182   0.19%   0.054%
100  17.004  1840 1859 1865 VV   13894329 257406664  30.86%   8.665%
 
101  17.078  1865 1870 1875 VV 2  298963   6334874   0.76%   0.213%
102  17.181  1875 1884 1891 VV   9637348 178119521  21.36%   5.996%
103  17.248  1891 1894 1900 VV    376128   8595832   1.03%   0.289%
104  17.351  1900 1909 1913 VV   21621787 422294451  50.63%  14.216%
105  17.405  1913 1917 1928 VV   6988503 121171399  14.53%   4.079%
 
106  17.555  1928 1938 1941 VV 3 1809199  37789727   4.53%   1.272%
107  17.601  1941 1945 1952 VV   4513924  82128311   9.85%   2.765%
108  17.674  1952 1955 1961 VV 3   55327   1515468   0.18%   0.051%
109  17.801  1968 1974 1984 VV 10   38240   1638719   0.20%   0.055%
110  17.921  1984 1991 1999 VV 7   37727   1380783   0.17%   0.046%
 
111  18.013  1999 2004 2007 VV 3   33249    841140   0.10%   0.028%
112  18.088  2007 2015 2020 VV    386226   7471809   0.90%   0.252%
113  18.140  2020 2022 2040 VV     39818   1866946   0.22%   0.063%
114  18.316  2045 2048 2050 VV 4   14138    266484   0.03%   0.009%
115  18.385  2050 2058 2060 VV 6   58247   1435975   0.17%   0.048%
 
116  18.436  2060 2065 2079 VV 6  122574   4494226   0.54%   0.151%
117  18.591  2081 2087 2096 VV     42245   1229431   0.15%   0.041%
118  18.675  2096 2099 2102 VV 4   14400    245885   0.03%   0.008%
119  18.732  2102 2108 2114 VV 2   81352   1920765   0.23%   0.065%
120  18.799  2114 2117 2123 VV 7   15139    420931   0.05%   0.014%
 
121  18.889  2123 2130 2138 VV    112500   2637753   0.32%   0.089%
122  18.957  2138 2140 2148 VV 6   12553    330375   0.04%   0.011%
123  19.093  2153 2160 2164 VV 2   57039   1288117   0.15%   0.043%
124  19.158  2164 2169 2181 VV     41077   1143858   0.14%   0.039%
125  19.382  2191 2201 2213 VV   3433616  80044830   9.60%   2.695%
 
126  19.505  2213 2219 2227 VV    161959   3559604   0.43%   0.120%
127  19.602  2227 2233 2239 VV 4   14321    509122   0.06%   0.017%
128  19.743  2248 2253 2260 VV 5   26030    707796   0.08%   0.024%
129  19.899  2268 2276 2282 VV     50865   1205160   0.14%   0.041%
130  20.005  2282 2291 2303 VV 7   34853   1211592   0.15%   0.041%
 
131  20.173  2307 2315 2322 VV 7   11989    360829   0.04%   0.012%
132  20.295  2322 2333 2337 VV 5   32982   1036886   0.12%   0.035%
133  20.348  2337 2340 2351 VV 3   37348   1049101   0.13%   0.035%
134  20.469  2351 2358 2359 VV 4    6557    126023   0.02%   0.004%
135  20.492  2359 2361 2368 VV 8    6816    151813   0.02%   0.005%
 
136  20.617  2368 2379 2389 VV 6   52618   1685376   0.20%   0.057%
137  20.704  2389 2391 2402 VV 10    6617    246058   0.03%   0.008%
138  20.827  2402 2409 2417 VV 9   19959    538582   0.06%   0.018%
139  20.935  2417 2425 2434 VV 7    8068    241971   0.03%   0.008%
140  21.060  2434 2443 2456 PV     77750   2092006   0.25%   0.070%
 
141  21.166  2456 2458 2461 VV 4    4790     89066   0.01%   0.003%
142  21.202  2461 2463 2470 VV 8    5996    139080   0.02%   0.005%
143  21.399  2488 2492 2498 VV 6    7427    145962   0.02%   0.005%
144  21.584  2510 2518 2525 PV 8    7096    214081   0.03%   0.007%
145  21.699  2529 2535 2545 VV 8    8748    291846   0.03%   0.010%
 
146  21.936  2563 2569 2571 PV 6    5481     72775   0.01%   0.002%
147  22.011  2571 2580 2586 VV 9   13912    377577   0.05%   0.013%
148  22.296  2615 2621 2630 PV 10    8725    185611   0.02%   0.006%
149  22.390  2630 2634 2638 VV 4    3330     53198   0.01%   0.002%
150  22.450  2638 2643 2653 PV 6   30713    650179   0.08%   0.022%
 
151  22.650  2660 2672 2673 VV 8    9854    225550   0.03%   0.008%
152  22.694  2673 2678 2686 VV    122820   2578241   0.31%   0.087%
153  22.781  2686 2690 2693 VV 6   14687    324361   0.04%   0.011%
154  22.825  2693 2697 2699 VV 2   26517    464484   0.06%   0.016%
155  22.877  2699 2704 2716 VV 5   57598   2001309   0.24%   0.067%
 
156  22.998  2716 2722 2731 VV     87118   1619046   0.19%   0.055%
157  23.146  2737 2743 2748 VV 7   14502    375697   0.05%   0.013%
158  23.213  2748 2752 2756 VV 6   21886    420021   0.05%   0.014%
159  23.257  2756 2759 2762 VV 4   17501    349602   0.04%   0.012%
160  23.352  2762 2772 2778 VV 7   51869   1636581   0.20%   0.055%
 
161  23.420  2778 2782 2786 VV    121714   2097765   0.25%   0.071%
162  23.468  2786 2789 2797 VV 3   66505   1231973   0.15%   0.041%
163  23.583  2797 2806 2814 VV 8   38071   1246450   0.15%   0.042%
164  23.693  2818 2822 2829 VV 10    8995    254599   0.03%   0.009%
165  23.826  2829 2841 2849 VV 2  263004   7234005   0.87%   0.244%
 
166  23.911  2849 2853 2859 VV 8   27505    696737   0.08%   0.023%
167  23.976  2859 2862 2865 VV 5   14430    313526   0.04%   0.011%
168  24.019  2865 2868 2876 VV 5   23279    511027   0.06%   0.017%
169  24.115  2876 2882 2888 VV 10   15169    422042   0.05%   0.014%
170  24.189  2888 2893 2898 VV 7   10916    292706   0.04%   0.010%
 
171  24.245  2898 2901 2904 VV 4   11498    220452   0.03%   0.007%
172  24.288  2904 2907 2914 VV 8   10800    377303   0.05%   0.013%
173  24.348  2914 2916 2919 VV 4   10808    209133   0.03%   0.007%
174  24.394  2919 2923 2926 VV 4   18209    319477   0.04%   0.011%
175  24.444  2926 2930 2934 VV 6   16885    418476   0.05%   0.014%
 
176  24.511  2934 2939 2946 VV 4   21229    537791   0.06%   0.018%
177  24.616  2946 2954 2959 VV 3   16105    445699   0.05%   0.015%
178  24.712  2963 2968 2973 VV 6   16854    448428   0.05%   0.015%
179  24.877  2987 2992 2997 VV 6   23929    493640   0.06%   0.017%
180  24.966  2997 3005 3039 VV   34580178 834053169 100.00%  28.077%
 
181  25.232  3039 3043 3050 VV 9   64148   2612391   0.31%   0.088%
182  25.322  3050 3056 3060 VV    342807   6174492   0.74%   0.208%
183  25.380  3060 3064 3071 VV    201826   4347598   0.52%   0.146%
184  25.447  3071 3074 3076 VV 4   46739    781326   0.09%   0.026%
185  25.466  3076 3077 3079 VV 2   42118    511004   0.06%   0.017%
 
186  25.551  3079 3089 3101 VV 4  163535   6838429   0.82%   0.230%
187  25.667  3101 3106 3111 VV    326703   6592269   0.79%   0.222%
188  25.724  3111 3114 3119 VV 5   95359   2635997   0.32%   0.089%
189  25.771  3119 3121 3132 VV 5   67295   2334986   0.28%   0.079%
190  25.875  3132 3136 3140 VV 5   46616   1247893   0.15%   0.042%
 
191  25.926  3140 3143 3153 VV 5   35918   1732318   0.21%   0.058%
192  26.041  3153 3159 3162 VV 4   48067   1344425   0.16%   0.045%
193  26.064  3162 3163 3168 VV 5   42202   1024761   0.12%   0.034%
194  26.146  3168 3175 3177 VV 2  112128   2719524   0.33%   0.092%
195  26.194  3177 3182 3191 VV 2  123140   3600356   0.43%   0.121%
 
196  26.276  3191 3193 3197 VV 4   31045    683509   0.08%   0.023%
197  26.429  3209 3215 3220 VV 10   27265    909682   0.11%   0.031%
198  26.476  3220 3222 3225 VV 4   25434    532146   0.06%   0.018%
199  26.517  3225 3228 3231 VV 2   59888   1101499   0.13%   0.037%
200  26.549  3231 3233 3237 VV 5   34613    721251   0.09%   0.024%
 
201  26.646  3242 3247 3250 VV 5   29331    911653   0.11%   0.031%
202  26.685  3250 3252 3257 VV 6   26687    617062   0.07%   0.021%
203  26.747  3257 3261 3263 VV     50981    939976   0.11%   0.032%
204  26.785  3263 3267 3271 VV 6   74852   1898573   0.23%   0.064%
205  26.849  3271 3276 3288 VV   1710799  29896457   3.58%   1.006%
 
206  26.948  3288 3290 3297 VV 7   58280   1663659   0.20%   0.056%
207  27.059  3302 3306 3309 VV 4   33746    870338   0.10%   0.029%
208  27.095  3309 3311 3313 VV 3   34215    570410   0.07%   0.019%
209  27.116  3313 3314 3318 VV 4   35055    712267   0.09%   0.024%
210  27.159  3318 3320 3322 VV 3   29896    456671   0.05%   0.015%
 
211  27.186  3322 3324 3329 VV 6   31323    777407   0.09%   0.026%
212  27.285  3333 3339 3343 VV 8   40226   1125644   0.13%   0.038%
213  27.490  3366 3368 3372 VV 5   25956    613639   0.07%   0.021%
214  27.545  3372 3376 3383 VV     63386   1533719   0.18%   0.052%
215  27.644  3383 3390 3402 VV     26547   1759955   0.21%   0.059%
 
216  27.746  3402 3405 3410 VV 7   21332    591411   0.07%   0.020%
217  27.809  3410 3414 3419 VV 8   26284    778450   0.09%   0.026%
218  27.894  3419 3426 3430 VV 9   33365   1196376   0.14%   0.040%
219  27.931  3430 3432 3436 VV 5   20948    500312   0.06%   0.017%
220  28.079  3450 3453 3462 VV 10   21506    953507   0.11%   0.032%
 
221  28.217  3469 3473 3475 VV 5   25629    532546   0.06%   0.018%
222  28.245  3475 3477 3480 VV 4   24612    483954   0.06%   0.016%
223  28.298  3480 3484 3491 VV 10   26283   1022354   0.12%   0.034%
224  28.385  3491 3497 3500 VV 8   20352    614228   0.07%   0.021%
225  28.478  3506 3510 3515 VV 4   39762    924311   0.11%   0.031%
 
226  28.522  3515 3516 3518 VV 2   20585    276018   0.03%   0.009%
227  28.587  3518 3526 3531 VV 4   47624   1815977   0.22%   0.061%
228  28.636  3531 3533 3535 VV 3   24644    390403   0.05%   0.013%
229  28.682  3535 3540 3542 VV 6   25305    603929   0.07%   0.020%
230  28.712  3542 3544 3547 VV 4   24927    527367   0.06%   0.018%
 
231  28.747  3547 3549 3553 VV 5   23807    550336   0.07%   0.019%
232  28.802  3553 3557 3567 VV 5   23489   1130430   0.14%   0.038%
233  29.075  3592 3596 3603 VV 9   18048    802446   0.10%   0.027%
234  29.145  3603 3606 3615 VV 9   16587    760497   0.09%   0.026%
235  29.235  3615 3619 3621 VV 5   18689    386795   0.05%   0.013%
 
236  29.258  3621 3622 3626 VV 4   18558    366259   0.04%   0.012%
237  29.434  3639 3648 3660 VV 4   29356   1492711   0.18%   0.050%
238  29.565  3660 3667 3670 VV 9   15337    524324   0.06%   0.018%
239  29.600  3670 3672 3679 VV 8   16332    528093   0.06%   0.018%
240  30.077  3737 3740 3747 VV 9   12588    389572   0.05%   0.013%
 
241  30.257  3762 3766 3768 VV 5    7742    165000   0.02%   0.006%
242  30.635  3819 3821 3822 VV 2    7841     87565   0.01%   0.003%
243  31.333  3915 3921 3925 VV 9    6054    186864   0.02%   0.006%
244  31.812  3986 3990 3993 VV 6    5157    120202   0.01%   0.004%
245  31.981  4006 4014 4022 VV 6    8305    329702   0.04%   0.011%
 
246  32.096  4026 4031 4034 VV 6    4137     82297   0.01%   0.003%
247  32.182  4037 4043 4045 PV 7    2916     54477   0.01%   0.002%
 
 
                        ͣ 2970556196
