                                                ٷֱȱ

  ·  : C:\MSDCHEM\1\DATA\HUANGWENJIE\20190916GF14B2019\
  ļ  : QC-20190916-e1.D                                    
  ɼ      : 17 Sep 2019  18:31
      : lvqi
  Ʒ      : QC-20190916-e1
        :  
  ALS Ʒƿ: 39   Ʒ˻: 1

  ֲ  : autoint1.e
      : ѧվ

      : C:\MSDCHEM\1\METHODS\20181120-Ŵ-DB35MS-FINAL.M
        :  

  źţTIC: QC-20190916-e1.D\data.ms

  ʱ ʼ 嶥 ֹ                       %
   #     ɨ ɨ ɨ             % ֵ   
 ---  ----- ----- ---- ---- ---  -------   -------  ------  -------
  1   4.221    14   19   25 PV 9    4118     86619   0.01%   0.003%
  2   4.326    28   34   48 PV 3   19436    457718   0.06%   0.015%
  3   4.520    53   62   71 VV 2   28555    899940   0.11%   0.030%
  4   4.659    71   82   89 VV 4   10519    404628   0.05%   0.013%
  5   4.906   109  118  123 VV     42502    974780   0.12%   0.032%
 
  6   4.997   123  131  145 VV   1133435  24493278   2.95%   0.811%
  7   5.474   192  200  204 PV 2   19042    410547   0.05%   0.014%
  8   5.529   204  208  224 VV 4    9556    289645   0.03%   0.010%
  9   6.033   271  280  286 VV 8    4604    144969   0.02%   0.005%
 10   6.289   313  317  321 VV 3    4985    107573   0.01%   0.004%
 
 11   6.397   325  332  344 VV 3    7864    252438   0.03%   0.008%
 12   6.640   357  367  377 VV 2  132833   3193273   0.38%   0.106%
 13   7.183   437  446  455 PV    371915   7880914   0.95%   0.261%
 14   7.261   455  457  464 VV 6    7544    164263   0.02%   0.005%
 15   7.442   477  483  488 VV 7    5419    128699   0.02%   0.004%
 
 16   7.507   488  492  500 VV 5    6408    169645   0.02%   0.006%
 17   7.621   500  509  518 VV    424095   9132298   1.10%   0.302%
 18   7.763   522  529  539 VV     37969    814739   0.10%   0.027%
 19   7.883   539  546  555 VV    199251   4177349   0.50%   0.138%
 20   8.091   569  576  584 VV    412638   8510142   1.02%   0.282%
 
 21   8.173   584  588  597 VV 2   31047    820817   0.10%   0.027%
 22   8.313   597  608  622 VV    144258   3348517   0.40%   0.111%
 23   8.776   667  675  683 VV    164738   3370168   0.41%   0.112%
 24   8.973   696  703  710 VV    217866   4428622   0.53%   0.147%
 25   9.033   710  712  719 VV 7    9153    216402   0.03%   0.007%
 
 26   9.226   730  740  750 VV   6572800 123956300  14.91%   4.104%
 27   9.321   750  753  759 VV 2   61768   1534080   0.18%   0.051%
 28   9.415   759  767  782 VV   3340925  63245466   7.61%   2.094%
 29   9.537   782  784  788 VV 5   13584    293067   0.04%   0.010%
 30   9.633   792  798  803 VV    109721   2256182   0.27%   0.075%
 
 31   9.687   803  806  816 VV 5   30717   1048258   0.13%   0.035%
 32   9.921   831  840  849 VV     48211   1336163   0.16%   0.044%
 33  10.050   849  858  863 VV   2175907  39779728   4.79%   1.317%
 34  10.101   863  865  874 VV    144145   2639236   0.32%   0.087%
 35  10.287   881  892  894 VV    197328   4248623   0.51%   0.141%
 
 36  10.330   894  899  902 VV    803828  14745645   1.77%   0.488%
 37  10.375   902  905  913 VV    381904   7200178   0.87%   0.238%
 38  10.476   913  919  924 VV 2   43028    958784   0.12%   0.032%
 39  10.532   924  928  932 VV     33565    688578   0.08%   0.023%
 40  10.578   932  934  944 VV     20263    482926   0.06%   0.016%
 
 41  10.698   948  952  956 VV 7    5761    137137   0.02%   0.005%
 42  10.868   969  976  981 VV 5    6105    181677   0.02%   0.006%
 43  10.939   981  986  990 VV 5    7322    193099   0.02%   0.006%
 44  10.976   990  991  993 VV 2    6555     81251   0.01%   0.003%
 45  11.009   993  996 1004 VV 3   10947    273813   0.03%   0.009%
 
 46  11.117  1004 1012 1022 VV     74496   1803038   0.22%   0.060%
 47  11.226  1022 1027 1038 VV 2   73558   1549005   0.19%   0.051%
 48  11.350  1038 1045 1050 VV 8   11089    344674   0.04%   0.011%
 49  11.421  1050 1055 1073 VV 10   11879    567402   0.07%   0.019%
 50  11.716  1092 1098 1105 VV 5   19680    480333   0.06%   0.016%
 
 51  11.815  1105 1112 1116 VV 2    9782    250160   0.03%   0.008%
 52  11.882  1116 1122 1131 VV 2   17634    534271   0.06%   0.018%
 53  12.045  1141 1145 1156 VV 4   15426    367972   0.04%   0.012%
 54  12.185  1156 1165 1167 VV 6    6664    179475   0.02%   0.006%
 55  12.215  1167 1170 1174 VV 6    8318    189892   0.02%   0.006%
 
 56  12.276  1174 1179 1184 VV 4   15130    303770   0.04%   0.010%
 57  12.407  1189 1197 1203 VV 3   15783    465519   0.06%   0.015%
 58  12.555  1206 1219 1227 VV 4   28198    984112   0.12%   0.033%
 59  12.656  1227 1233 1235 VV 7    6409    154491   0.02%   0.005%
 60  12.720  1235 1242 1249 VV   4925300  82600139   9.94%   2.735%
 
 61  12.776  1249 1250 1257 VV 4   30596    655191   0.08%   0.022%
 62  12.858  1257 1262 1268 VV 4   13467    470264   0.06%   0.016%
 63  12.954  1268 1276 1285 VV 4   16857    807733   0.10%   0.027%
 64  13.065  1285 1292 1299 VV   1034238  18156889   2.18%   0.601%
 65  13.136  1299 1302 1308 VV 5   22253    571685   0.07%   0.019%
 
 66  13.227  1308 1315 1321 VV   2306042  39551143   4.76%   1.309%
 67  13.274  1321 1322 1336 VV 3  151321   3293918   0.40%   0.109%
 68  13.491  1341 1353 1370 VV 6  253874  12246782   1.47%   0.405%
 69  13.632  1370 1374 1380 VV 3   37347   1157076   0.14%   0.038%
 70  13.745  1380 1390 1397 VV 3  100752   3495912   0.42%   0.116%
 
 71  13.921  1397 1415 1423 VV    429242   9869360   1.19%   0.327%
 72  14.095  1435 1440 1446 VV 3   30385    895630   0.11%   0.030%
 73  14.175  1446 1452 1459 VV 3   41693   1101893   0.13%   0.036%
 74  14.265  1459 1465 1470 VV 2   28868    755801   0.09%   0.025%
 75  14.355  1470 1478 1488 VV    356607   7186089   0.86%   0.238%
 
 76  14.453  1488 1492 1494 VV 4   23478    472051   0.06%   0.016%
 77  14.499  1494 1498 1507 VV 2   52211   1741905   0.21%   0.058%
 78  14.614  1507 1515 1525 VV   1296778  25211020   3.03%   0.835%
 79  14.734  1525 1532 1536 VV    814296  15750360   1.89%   0.521%
 80  14.795  1536 1541 1558 VV   3086310  52851729   6.36%   1.750%
 
 81  14.978  1558 1567 1573 VV     20416    962396   0.12%   0.032%
 82  15.089  1573 1583 1589 VV    150176   3295525   0.40%   0.109%
 83  15.157  1589 1593 1598 VV 2   44602    984094   0.12%   0.033%
 84  15.276  1598 1610 1616 VV 3   72836   2616760   0.31%   0.087%
 85  15.353  1616 1621 1627 VV 3   67242   1470784   0.18%   0.049%
 
 86  15.433  1627 1633 1637 VV     37983   1004343   0.12%   0.033%
 87  15.497  1637 1642 1649 VV    170862   3514999   0.42%   0.116%
 88  15.585  1649 1655 1675 VV    250073   5385699   0.65%   0.178%
 89  15.818  1675 1688 1692 VV 2   47735   1433574   0.17%   0.047%
 90  15.864  1692 1695 1700 VV 5   26275    588405   0.07%   0.019%
 
 91  16.001  1700 1715 1720 VV 2  157847   4220985   0.51%   0.140%
 92  16.092  1720 1728 1737 VV   5410295  90372255  10.87%   2.992%
 93  16.184  1737 1741 1750 VV 2   51875   1800531   0.22%   0.060%
 94  16.296  1750 1757 1760 VV 5   38348   1117266   0.13%   0.037%
 95  16.358  1760 1766 1771 VV    996931  17629256   2.12%   0.584%
 
 96  16.426  1771 1776 1785 VV    199758   5793221   0.70%   0.192%
 97  16.525  1785 1790 1801 VV 2   76278   2363216   0.28%   0.078%
 98  16.722  1813 1818 1825 VV     43138   1009808   0.12%   0.033%
 99  16.823  1825 1833 1840 VV 3   63312   1787955   0.22%   0.059%
100  17.003  1840 1859 1865 VV   14227457 262066799  31.53%   8.676%
 
101  17.078  1865 1870 1875 VV 3  299301   6413601   0.77%   0.212%
102  17.181  1875 1884 1891 VV   9900966 182571026  21.97%   6.044%
103  17.247  1891 1894 1900 VV    391506   8696037   1.05%   0.288%
104  17.352  1900 1909 1913 VV   22198111 429274960  51.65%  14.212%
105  17.405  1913 1917 1929 VV   7111698 124034550  14.92%   4.106%
 
106  17.554  1929 1938 1941 VV 4 1800539  37768935   4.54%   1.250%
107  17.601  1941 1945 1953 VV   4618058  83909394  10.10%   2.778%
108  17.677  1953 1956 1961 VV 2   56459   1502675   0.18%   0.050%
109  17.727  1961 1963 1968 VV 5   33167    844390   0.10%   0.028%
110  17.797  1968 1973 1983 VV 5   35735   1626405   0.20%   0.054%
 
111  17.920  1983 1991 1998 VV 7   37596   1449072   0.17%   0.048%
112  18.010  1998 2004 2008 VV 8   36126   1054258   0.13%   0.035%
113  18.088  2008 2015 2020 VV    405227   7502656   0.90%   0.248%
114  18.141  2020 2023 2044 VV     42512   2193825   0.26%   0.073%
115  18.315  2044 2048 2050 VV 4   15236    313888   0.04%   0.010%
 
116  18.385  2050 2058 2059 VV 4   60250   1407340   0.17%   0.047%
117  18.432  2059 2065 2080 VV 5  133087   4876474   0.59%   0.161%
118  18.592  2080 2087 2096 VV     40953   1289604   0.16%   0.043%
119  18.732  2096 2108 2113 VV     83586   2262328   0.27%   0.075%
120  18.792  2113 2116 2124 VV 9   14204    468413   0.06%   0.016%
 
121  18.889  2124 2130 2138 VV 3  115676   2674678   0.32%   0.089%
122  18.955  2138 2140 2147 VV 5   12663    349180   0.04%   0.012%
123  19.092  2153 2159 2164 VV 2   55150   1312533   0.16%   0.043%
124  19.159  2164 2169 2179 VV 2   42079   1125077   0.14%   0.037%
125  19.381  2191 2201 2213 VV   3414758  82079894   9.88%   2.717%
 
126  19.504  2213 2219 2228 VV    166621   3724752   0.45%   0.123%
127  19.602  2228 2233 2238 VV 7   12863    419313   0.05%   0.014%
128  19.740  2247 2253 2263 VV 5   27728    821650   0.10%   0.027%
129  19.899  2263 2276 2282 VV     52788   1328310   0.16%   0.044%
130  20.008  2282 2291 2309 VV 7   29464   1199973   0.14%   0.040%
 
131  20.174  2309 2315 2322 VV 6   12799    386842   0.05%   0.013%
132  20.292  2322 2332 2337 VV 4   31328   1047686   0.13%   0.035%
133  20.351  2337 2341 2353 VV 2   41585   1171474   0.14%   0.039%
134  20.473  2353 2358 2368 VV 2    6644    283271   0.03%   0.009%
135  20.617  2371 2379 2390 VV 4   54389   1727177   0.21%   0.057%
 
136  20.826  2403 2409 2417 VV 7   18590    510069   0.06%   0.017%
137  20.933  2417 2424 2433 VV 7    7897    237406   0.03%   0.008%
138  21.060  2433 2443 2460 VV     83492   2333672   0.28%   0.077%
139  21.203  2460 2463 2470 VV 7    6803    204216   0.02%   0.007%
140  21.404  2487 2492 2500 VV 7    7985    191640   0.02%   0.006%
 
141  21.590  2508 2519 2525 VV 6    6522    246692   0.03%   0.008%
142  21.706  2528 2536 2544 VV 7    9017    311442   0.04%   0.010%
143  21.936  2561 2569 2570 VV 7    4723     90523   0.01%   0.003%
144  22.008  2573 2579 2586 VV 7   14759    375277   0.05%   0.012%
145  22.081  2586 2590 2596 VV 5    6034    135366   0.02%   0.004%
 
146  22.295  2616 2620 2629 PV 9   10356    255502   0.03%   0.008%
147  22.383  2629 2633 2637 VV 4    3936     99863   0.01%   0.003%
148  22.449  2637 2643 2654 VV 3   30120    722100   0.09%   0.024%
149  22.648  2667 2671 2673 VV 4   11161    160869   0.02%   0.005%
150  22.693  2673 2678 2686 VV    127384   2723953   0.33%   0.090%
 
151  22.781  2686 2690 2693 VV 5   16653    343259   0.04%   0.011%
152  22.825  2693 2697 2699 VV 2   28572    474074   0.06%   0.016%
153  22.876  2699 2704 2716 VV 5   57834   2085080   0.25%   0.069%
154  22.997  2716 2721 2730 VV 2   88293   1661133   0.20%   0.055%
155  23.143  2738 2742 2748 VV 6   15138    398567   0.05%   0.013%
 
156  23.212  2748 2752 2756 VV 3   23914    454696   0.05%   0.015%
157  23.254  2756 2758 2762 VV 5   19877    386175   0.05%   0.013%
158  23.351  2762 2772 2778 VV 8   57977   1745261   0.21%   0.058%
159  23.420  2778 2782 2786 VV    129582   2235412   0.27%   0.074%
160  23.468  2786 2789 2797 VV     69737   1334491   0.16%   0.044%
 
161  23.583  2797 2806 2818 VV 9   40269   1444466   0.17%   0.048%
162  23.698  2818 2822 2829 VV 9   10017    305057   0.04%   0.010%
163  23.825  2829 2841 2849 VV 2  270491   7554318   0.91%   0.250%
164  23.911  2849 2853 2859 VV 7   29571    756048   0.09%   0.025%
165  23.972  2859 2862 2864 VV 4   17040    301442   0.04%   0.010%
 
166  24.018  2864 2868 2874 VV 5   22930    553554   0.07%   0.018%
167  24.114  2877 2882 2889 VV 5   15050    471227   0.06%   0.016%
168  24.187  2889 2893 2897 VV 4   10855    273984   0.03%   0.009%
169  24.252  2897 2902 2904 VV 2   12442    283668   0.03%   0.009%
170  24.295  2904 2908 2914 VV 8   11635    401438   0.05%   0.013%
 
171  24.351  2914 2916 2918 VV 3   12513    197488   0.02%   0.007%
172  24.394  2918 2923 2926 VV 6   20904    406399   0.05%   0.013%
173  24.441  2926 2929 2935 VV 7   17468    427297   0.05%   0.014%
174  24.511  2935 2939 2945 VV 6   22654    559781   0.07%   0.019%
175  24.613  2948 2954 2959 VV 3   16483    414352   0.05%   0.014%
 
176  24.712  2963 2968 2973 VV 8   18334    486315   0.06%   0.016%
177  24.770  2973 2977 2982 VV 7    9530    265699   0.03%   0.009%
178  24.832  2982 2985 2988 VV 4    9425    203137   0.02%   0.007%
179  24.877  2988 2992 2996 VV 3   24806    479099   0.06%   0.016%
180  24.966  2996 3005 3039 VV 2 34761267 831168794 100.00%  27.517%
 
181  25.228  3039 3043 3049 VV 7   62527   2532478   0.30%   0.084%
182  25.322  3049 3056 3060 VV    367606   6490633   0.78%   0.215%
183  25.379  3060 3064 3071 VV    207172   4465279   0.54%   0.148%
184  25.450  3071 3074 3078 VV 4   48051   1262736   0.15%   0.042%
185  25.551  3078 3089 3097 VV 3  166603   6487907   0.78%   0.215%
 
186  25.619  3097 3099 3100 VV 2   39968    457882   0.06%   0.015%
187  25.666  3100 3105 3111 VV    334443   6698763   0.81%   0.222%
188  25.723  3111 3114 3119 VV 4  100237   2712171   0.33%   0.090%
189  25.772  3119 3121 3132 VV 3   70129   2445098   0.29%   0.081%
190  25.875  3132 3136 3140 VV 7   50800   1335118   0.16%   0.044%
 
191  25.916  3140 3142 3149 VV 8   36688   1331747   0.16%   0.044%
192  26.043  3153 3160 3167 VV 5   48788   2270084   0.27%   0.075%
193  26.146  3167 3175 3178 VV 3  116909   3034257   0.37%   0.100%
194  26.195  3178 3182 3191 VV 2  127664   3418310   0.41%   0.113%
195  26.277  3191 3193 3197 VV 5   31802    723425   0.09%   0.024%
 
196  26.321  3197 3200 3212 VV 5   29448   1463732   0.18%   0.048%
197  26.426  3212 3215 3218 VV 5   27675    627433   0.08%   0.021%
198  26.518  3218 3228 3231 VV     63635   1815613   0.22%   0.060%
199  26.551  3231 3233 3236 VV 4   34481    641750   0.08%   0.021%
200  26.644  3241 3246 3252 VV 9   28802   1144138   0.14%   0.038%
 
201  26.694  3252 3253 3257 VV 4   29351    545919   0.07%   0.018%
202  26.746  3257 3261 3263 VV     52918    940567   0.11%   0.031%
203  26.783  3263 3266 3271 VV 4   75713   1948658   0.23%   0.065%
204  26.849  3271 3276 3288 VV   1713456  30147648   3.63%   0.998%
205  26.946  3288 3290 3302 VV     57270   2415474   0.29%   0.080%
 
206  27.058  3302 3306 3308 VV 5   35182    751470   0.09%   0.025%
207  27.090  3308 3310 3312 VV 3   35916    599215   0.07%   0.020%
208  27.113  3312 3314 3319 VV 5   34828    849454   0.10%   0.028%
209  27.187  3319 3324 3333 VV 5   33301   1615084   0.19%   0.053%
210  27.283  3333 3338 3342 VV 7   39300   1114281   0.13%   0.037%
 
211  27.330  3342 3345 3347 VV 4   26725    462647   0.06%   0.015%
212  27.352  3347 3348 3359 VV 4   26265   1175152   0.14%   0.039%
213  27.489  3364 3368 3371 VV 6   25503    646908   0.08%   0.021%
214  27.545  3371 3376 3380 VV     62254   1377859   0.17%   0.046%
215  27.580  3380 3381 3385 VV 4   26273    568507   0.07%   0.019%
 
216  27.624  3385 3387 3389 VV 2   26067    385717   0.05%   0.013%
217  27.648  3389 3391 3395 VV 5   27316    570343   0.07%   0.019%
218  27.752  3404 3406 3410 VV 5   21094    487909   0.06%   0.016%
219  27.803  3410 3413 3418 VV 7   26016    747366   0.09%   0.025%
220  27.893  3418 3426 3434 VV 7   32584   1637207   0.20%   0.054%
 
221  27.972  3434 3437 3444 VV 9   21142    734695   0.09%   0.024%
222  28.078  3451 3453 3459 VV 7   20742    637915   0.08%   0.021%
223  28.212  3469 3472 3474 VV 4   25906    508276   0.06%   0.017%
224  28.243  3474 3476 3480 VV 5   24553    536375   0.06%   0.018%
225  28.297  3480 3484 3488 VV 6   26345    684513   0.08%   0.023%
 
226  28.354  3488 3492 3506 VV 6   19413   1372355   0.17%   0.045%
227  28.478  3506 3510 3518 VV 6   39094   1272514   0.15%   0.042%
228  28.579  3518 3525 3534 VV 5   48650   2093055   0.25%   0.069%
229  28.682  3534 3540 3548 VV 5   24333   1316799   0.16%   0.044%
230  28.755  3548 3550 3552 VV 3   24365    367067   0.04%   0.012%
 
231  28.776  3552 3553 3556 VV 3   23037    338895   0.04%   0.011%
232  28.896  3567 3570 3574 VV 6   21237    484936   0.06%   0.016%
233  29.070  3591 3595 3605 VV 6   18187    902673   0.11%   0.030%
234  29.236  3616 3619 3623 VV 6   17844    518058   0.06%   0.017%
235  29.288  3623 3627 3629 VV 5   18471    393806   0.05%   0.013%
 
236  29.343  3629 3635 3641 VV 10   19341    844505   0.10%   0.028%
237  29.435  3641 3648 3658 VV 6   30171   1289140   0.16%   0.043%
238  29.534  3658 3662 3664 VV 5   14560    329245   0.04%   0.011%
239  29.559  3664 3666 3668 VV 3   14601    204251   0.02%   0.007%
240  29.607  3668 3673 3678 VV 9   15301    541878   0.07%   0.018%
 
241  30.075  3737 3740 3750 VV 10   12052    484752   0.06%   0.016%
242  30.154  3750 3751 3758 VV 7    8842    213252   0.03%   0.007%
243  30.223  3758 3761 3763 VV 4    7617    135506   0.02%   0.004%
244  30.247  3763 3765 3767 VV 3    7998    125256   0.02%   0.004%
245  30.475  3789 3798 3801 VV 10    8045    319994   0.04%   0.011%
 
246  30.628  3813 3820 3822 VV 8    7560    225523   0.03%   0.007%
247  30.657  3822 3824 3834 VV 8    7854    320920   0.04%   0.011%
248  31.016  3873 3875 3877 VV 3    5780     82297   0.01%   0.003%
249  31.044  3877 3879 3884 VV 6    5901    133738   0.02%   0.004%
250  31.300  3914 3916 3918 VV 3    5084     64780   0.01%   0.002%
 
251  31.809  3985 3990 3995 VV 9    5071    159225   0.02%   0.005%
252  31.899  3999 4003 4005 VV 5    3932     52445   0.01%   0.002%
253  31.976  4005 4014 4021 PV 5    5369    187581   0.02%   0.006%
 
 
                        ͣ 3020596823
