                                                ٷֱȱ

  ·  : C:\MSDCHEM\1\DATA\HUANGWENJIE\20190916GF14B2019\
  ļ  : QC-20190916-f1.D                                    
  ɼ      : 18 Sep 2019  00:08
      : lvqi
  Ʒ      : QC-20190916-f1
        :  
  ALS Ʒƿ: 39   Ʒ˻: 1

  ֲ  : autoint1.e
      : ѧվ

      : C:\MSDCHEM\1\METHODS\20181120-Ŵ-DB35MS-FINAL.M
        :  

  źţTIC: QC-20190916-f1.D\data.ms

  ʱ ʼ 嶥 ֹ                       %
   #     ɨ ɨ ɨ             % ֵ   
 ---  ----- ----- ---- ---- ---  -------   -------  ------  -------
  1   4.325    25   34   46 PV 3   21033    471133   0.05%   0.015%
  2   4.516    46   62   71 PV 2   31330    992235   0.12%   0.032%
  3   4.617    71   76   79 VV 5    8159    189963   0.02%   0.006%
  4   4.659    79   82   90 VV 2   10508    249370   0.03%   0.008%
  5   4.908   110  118  123 PV     46508   1039109   0.12%   0.033%
 
  6   4.998   123  131  142 VV   1164146  25083511   2.93%   0.808%
  7   5.473   191  200  204 PV 2   18423    425689   0.05%   0.014%
  8   5.528   204  207  218 VV 3   10515    284121   0.03%   0.009%
  9   5.858   233  255  263 VV 3    4623    213435   0.02%   0.007%
 10   6.036   275  280  286 VV 7    4453    134142   0.02%   0.004%
 
 11   6.289   313  317  322 VV 4    4689    102654   0.01%   0.003%
 12   6.392   322  332  344 PV 2    9244    274038   0.03%   0.009%
 13   6.640   359  367  381 VV 2  144176   3413725   0.40%   0.110%
 14   7.182   438  445  453 PV    380110   7939260   0.93%   0.256%
 15   7.257   453  456  461 VV 7    7664    185056   0.02%   0.006%
 
 16   7.343   461  469  477 VV 2   31359    801333   0.09%   0.026%
 17   7.446   477  483  488 VV 5    4259    102454   0.01%   0.003%
 18   7.512   488  493  499 VV 6    6023    155388   0.02%   0.005%
 19   7.621   499  509  522 VV    431072   9347905   1.09%   0.301%
 20   7.763   522  529  539 VV     38018    810993   0.09%   0.026%
 
 21   7.882   539  546  554 VV    206598   4251066   0.50%   0.137%
 22   8.091   568  576  584 VV    411084   8522475   0.99%   0.274%
 23   8.172   584  588  596 VV     33132    859213   0.10%   0.028%
 24   8.313   596  608  622 VV    154288   3482785   0.41%   0.112%
 25   8.776   665  675  683 PV    168717   3495118   0.41%   0.113%
 
 26   8.973   683  703  709 VV    223958   4590027   0.54%   0.148%
 27   9.032   709  712  730 VV 6    9241    219808   0.03%   0.007%
 28   9.225   730  739  749 VV   6747549 128135671  14.96%   4.126%
 29   9.320   749  753  759 VV 2   65311   1657633   0.19%   0.053%
 30   9.415   759  767  780 VV   3362320  63677889   7.43%   2.051%
 
 31   9.536   780  784  792 VV 6   13487    477185   0.06%   0.015%
 32   9.631   792  798  803 VV    115053   2352674   0.27%   0.076%
 33   9.683   803  805  820 VV 5   33066   1236907   0.14%   0.040%
 34   9.921   833  840  846 VV     58081   1407935   0.16%   0.045%
 35  10.049   846  858  863 VV   2239405  40916724   4.78%   1.318%
 
 36  10.099   863  865  875 VV    146006   2713570   0.32%   0.087%
 37  10.286   880  892  894 VV    203834   4352669   0.51%   0.140%
 38  10.329   894  898  902 VV    897836  16602565   1.94%   0.535%
 39  10.374   902  905  912 VV    395743   7381727   0.86%   0.238%
 40  10.475   912  919  923 VV     42192    979378   0.11%   0.032%
 
 41  10.533   923  928  932 VV     36335    766119   0.09%   0.025%
 42  10.578   932  934  942 VV     19114    456119   0.05%   0.015%
 43  10.692   946  951  958 VV 9    5941    171050   0.02%   0.006%
 44  10.860   963  975  981 VV 6    6474    223672   0.03%   0.007%
 45  10.945   981  987  991 VV 6    6956    229965   0.03%   0.007%
 
 46  11.006   991  996 1002 VV 4   12154    325619   0.04%   0.010%
 47  11.118  1002 1012 1021 VV 2   75276   1838835   0.21%   0.059%
 48  11.226  1021 1027 1038 VV 2   74123   1571829   0.18%   0.051%
 49  11.350  1038 1045 1049 VV 7   12003    315525   0.04%   0.010%
 50  11.423  1049 1056 1064 VV 8   12622    513501   0.06%   0.017%
 
 51  11.716  1092 1098 1105 VV 4   19816    483390   0.06%   0.016%
 52  11.815  1105 1112 1116 VV 4    9948    239506   0.03%   0.008%
 53  11.883  1116 1122 1130 VV 3   18217    511435   0.06%   0.016%
 54  12.043  1141 1145 1153 VV 6   13999    319540   0.04%   0.010%
 55  12.215  1160 1170 1173 VV 8    8837    340090   0.04%   0.011%
 
 56  12.275  1173 1178 1185 VV 5   13765    337876   0.04%   0.011%
 57  12.406  1185 1197 1202 VV 5   17759    548259   0.06%   0.018%
 58  12.556  1208 1219 1226 VV 3   32324   1026964   0.12%   0.033%
 59  12.719  1234 1242 1249 VV   5057928  84664671   9.88%   2.726%
 60  12.773  1249 1250 1257 VV 2   30347    653111   0.08%   0.021%
 
 61  12.872  1257 1264 1270 VV 3   51876   1288326   0.15%   0.041%
 62  12.943  1270 1275 1285 VV 7   18859    815274   0.10%   0.026%
 63  13.064  1285 1292 1300 VV   1049027  18570195   2.17%   0.598%
 64  13.136  1300 1302 1308 VV 4   22017    563336   0.07%   0.018%
 65  13.227  1308 1315 1320 VV   2409121  40584805   4.74%   1.307%
 
 66  13.273  1320 1322 1333 VV 3  156999   3319520   0.39%   0.107%
 67  13.492  1338 1354 1369 VV 5  302025  14642551   1.71%   0.472%
 68  13.631  1369 1374 1378 VV 6   39139   1162284   0.14%   0.037%
 69  13.745  1378 1390 1400 VV 3  102677   4098215   0.48%   0.132%
 70  13.920  1400 1415 1423 VV    397356   9067237   1.06%   0.292%
 
 71  13.986  1423 1425 1430 VV 6   20703    527745   0.06%   0.017%
 72  14.095  1433 1440 1446 VV 5   30166   1015432   0.12%   0.033%
 73  14.175  1446 1452 1459 VV 2   41180   1116008   0.13%   0.036%
 74  14.266  1459 1465 1469 VV 4   27702    737806   0.09%   0.024%
 75  14.354  1469 1478 1488 VV    409723   8280409   0.97%   0.267%
 
 76  14.455  1488 1492 1494 VV 3   24243    461575   0.05%   0.015%
 77  14.499  1494 1498 1506 VV     57675   1745546   0.20%   0.056%
 78  14.613  1506 1515 1525 VV   1304280  25987029   3.03%   0.837%
 79  14.733  1525 1532 1536 VV    884048  17352083   2.03%   0.559%
 80  14.794  1536 1541 1559 VV   3113718  53099313   6.20%   1.710%
 
 81  14.992  1563 1569 1574 VV 5   41477   1218368   0.14%   0.039%
 82  15.089  1574 1583 1589 VV    157621   3412345   0.40%   0.110%
 83  15.157  1589 1593 1598 VV     47193    987972   0.12%   0.032%
 84  15.275  1598 1610 1615 VV 5   72305   2623621   0.31%   0.084%
 85  15.351  1615 1621 1627 VV     68281   1594106   0.19%   0.051%
 
 86  15.435  1627 1633 1637 VV     39725   1009350   0.12%   0.033%
 87  15.497  1637 1642 1648 VV    175271   3506368   0.41%   0.113%
 88  15.584  1648 1655 1668 VV    293983   6133886   0.72%   0.198%
 89  15.817  1679 1688 1692 VV     49261   1392098   0.16%   0.045%
 90  15.864  1692 1695 1702 VV 6   25303    615138   0.07%   0.020%
 
 91  16.001  1702 1715 1720 VV 2  162384   4300636   0.50%   0.138%
 92  16.092  1720 1728 1737 VV   5465155  89473278  10.44%   2.881%
 93  16.183  1737 1741 1751 VV 3   51857   1869704   0.22%   0.060%
 94  16.291  1751 1756 1760 VV 3   39717   1079957   0.13%   0.035%
 95  16.358  1760 1766 1771 VV   1022286  18150435   2.12%   0.585%
 
 96  16.425  1771 1776 1785 VV    211874   5974172   0.70%   0.192%
 97  16.525  1785 1790 1801 VV 2   77204   2393121   0.28%   0.077%
 98  16.722  1813 1818 1824 VV     45217   1055104   0.12%   0.034%
 99  16.820  1824 1832 1841 VV 5   69591   2176144   0.25%   0.070%
100  17.004  1841 1859 1865 VV   14404037 269498493  31.46%   8.679%
 
101  17.079  1865 1870 1875 VV 2  310001   6586819   0.77%   0.212%
102  17.181  1875 1884 1891 VV   10092594 187493030  21.88%   6.038%
103  17.248  1891 1894 1900 VV    396933   8988171   1.05%   0.289%
104  17.352  1900 1909 1913 VV   22760076 439685228  51.32%  14.159%
105  17.404  1913 1917 1929 VV   7303957 126473911  14.76%   4.073%
 
106  17.553  1929 1938 1941 VV 4 1828924  37839524   4.42%   1.219%
107  17.602  1941 1945 1952 VV   4736657  86119854  10.05%   2.773%
108  17.676  1952 1956 1961 VV 2   59802   1604405   0.19%   0.052%
109  17.728  1961 1963 1968 VV 6   32967    865762   0.10%   0.028%
110  17.800  1968 1973 1982 VV 10   38708   1587342   0.19%   0.051%
 
111  17.921  1982 1991 1998 VV 8   38634   1550146   0.18%   0.050%
112  18.012  1998 2004 2007 VV 4   36839   1000437   0.12%   0.032%
113  18.087  2007 2015 2020 VV    415564   7816686   0.91%   0.252%
114  18.140  2020 2022 2034 VV     42561   1662098   0.19%   0.054%
115  18.315  2043 2048 2050 VV 4   15012    396576   0.05%   0.013%
 
116  18.384  2050 2058 2059 VV 5   59507   1387732   0.16%   0.045%
117  18.430  2059 2064 2080 VV 6  164482   5741213   0.67%   0.185%
118  18.590  2080 2087 2095 VV     42736   1325211   0.15%   0.043%
119  18.676  2095 2100 2102 VV 6   13723    323323   0.04%   0.010%
120  18.732  2102 2108 2113 VV 2   86193   1998268   0.23%   0.064%
 
121  18.789  2113 2116 2123 VV 6   16295    480852   0.06%   0.015%
122  18.889  2123 2130 2139 VV 2  112473   2741789   0.32%   0.088%
123  18.961  2139 2141 2148 VV 7   12707    348758   0.04%   0.011%
124  19.092  2153 2159 2164 VV 2   55045   1264377   0.15%   0.041%
125  19.157  2164 2169 2178 VV 2   41672   1085823   0.13%   0.035%
 
126  19.381  2189 2201 2213 VV   3485445  84676264   9.88%   2.727%
127  19.503  2213 2219 2229 VV    176322   3881785   0.45%   0.125%
128  19.604  2229 2233 2239 VV 7   11459    359405   0.04%   0.012%
129  19.674  2239 2243 2246 VV 6    7663    165527   0.02%   0.005%
130  19.741  2246 2253 2264 VV 4   29635    880631   0.10%   0.028%
 
131  19.898  2264 2275 2283 VV     51945   1366275   0.16%   0.044%
132  20.006  2283 2291 2303 VV 5   33915   1240450   0.14%   0.040%
133  20.173  2308 2315 2322 VV 4   17138    482754   0.06%   0.016%
134  20.295  2322 2333 2335 VV 4   33452    919966   0.11%   0.030%
135  20.349  2335 2340 2353 VV 3   47817   1539486   0.18%   0.050%
 
136  20.488  2353 2360 2366 VV 10    7389    248558   0.03%   0.008%
137  20.617  2372 2379 2388 VV 5   56005   1730200   0.20%   0.056%
138  20.826  2402 2409 2417 VV 8   20064    561793   0.07%   0.018%
139  20.935  2417 2425 2436 VV 8    7720    293035   0.03%   0.009%
140  21.058  2436 2442 2453 VV     88196   2229545   0.26%   0.072%
 
141  21.143  2453 2455 2459 VV 5    6802    145297   0.02%   0.005%
142  21.204  2459 2463 2477 VV 5    7888    299649   0.03%   0.010%
143  21.403  2485 2492 2497 VV 9    6650    175233   0.02%   0.006%
144  21.589  2511 2519 2529 VV 6    8413    264982   0.03%   0.009%
145  21.705  2529 2535 2550 VV 7   10823    342675   0.04%   0.011%
 
146  21.877  2553 2560 2564 VV 7    5712    115606   0.01%   0.004%
147  21.934  2564 2568 2573 VV 8    4727    142026   0.02%   0.005%
148  22.007  2573 2579 2585 VV 8   14502    372888   0.04%   0.012%
149  22.086  2585 2590 2596 VV 8    5554    140895   0.02%   0.005%
150  22.298  2615 2621 2630 PV 10   11749    304596   0.04%   0.010%
 
151  22.383  2630 2633 2637 VV 5    4112     85343   0.01%   0.003%
152  22.450  2637 2643 2650 VV 5   32129    671736   0.08%   0.022%
153  22.512  2650 2652 2655 VV 4    6367    104013   0.01%   0.003%
154  22.647  2665 2671 2673 VV 6   12173    215982   0.03%   0.007%
155  22.693  2673 2678 2686 VV    127843   2781692   0.32%   0.090%
 
156  22.781  2686 2690 2693 VV 5   17615    364094   0.04%   0.012%
157  22.825  2693 2697 2699 VV 2   28928    490406   0.06%   0.016%
158  22.878  2699 2704 2715 VV 4   60898   2156685   0.25%   0.069%
159  22.998  2715 2722 2727 VV     90609   1670683   0.20%   0.054%
160  23.096  2730 2736 2739 VV 4   11920    312740   0.04%   0.010%
 
161  23.142  2739 2742 2748 VV 6   15519    393659   0.05%   0.013%
162  23.212  2748 2752 2756 VV 4   25396    512033   0.06%   0.016%
163  23.254  2756 2758 2761 VV 3   19561    350662   0.04%   0.011%
164  23.350  2761 2772 2778 VV 7   56908   1812499   0.21%   0.058%
165  23.420  2778 2782 2786 VV    129872   2298661   0.27%   0.074%
 
166  23.467  2786 2789 2796 VV 2   67402   1341044   0.16%   0.043%
167  23.581  2796 2805 2817 VV 5   39572   1476569   0.17%   0.048%
168  23.697  2817 2822 2829 VV 8   10963    336577   0.04%   0.011%
169  23.826  2829 2841 2849 VV 2  291098   7938364   0.93%   0.256%
170  23.910  2849 2853 2858 VV 7   29334    757413   0.09%   0.024%
 
171  23.972  2858 2862 2864 VV 4   16353    328382   0.04%   0.011%
172  24.018  2864 2868 2872 VV 6   24984    530138   0.06%   0.017%
173  24.115  2879 2882 2889 VV 8   14816    435033   0.05%   0.014%
174  24.189  2889 2893 2898 VV 6   10745    296862   0.03%   0.010%
175  24.246  2898 2901 2904 VV 3   13440    253083   0.03%   0.008%
 
176  24.290  2904 2907 2913 VV 8   11859    406126   0.05%   0.013%
177  24.352  2913 2916 2918 VV 4   12640    218486   0.03%   0.007%
178  24.394  2918 2922 2926 VV 3   20517    394068   0.05%   0.013%
179  24.442  2926 2929 2934 VV 5   18709    448967   0.05%   0.014%
180  24.516  2934 2940 2946 VV 6   24343    628217   0.07%   0.020%
 
181  24.616  2946 2954 2958 VV 2   17805    464225   0.05%   0.015%
182  24.716  2963 2969 2973 VV 8   18215    516582   0.06%   0.017%
183  24.769  2973 2976 2979 VV 5    8789    182620   0.02%   0.006%
184  24.832  2982 2985 2987 VV 4    8864    158826   0.02%   0.005%
185  24.875  2987 2992 2996 VV 6   31432    636723   0.07%   0.021%
 
186  24.966  2996 3005 3039 VV 2 35040710 856750238 100.00%  27.590%
187  25.229  3039 3043 3049 VV 8   63670   2466694   0.29%   0.079%
188  25.322  3049 3056 3060 VV    395281   7060981   0.82%   0.227%
189  25.380  3060 3064 3071 VV    214354   4487946   0.52%   0.145%
190  25.447  3071 3074 3079 VV 6   47405   1502655   0.18%   0.048%
 
191  25.511  3079 3083 3084 VV 2   72279   1207575   0.14%   0.039%
192  25.552  3084 3089 3101 VV 2  175321   5848761   0.68%   0.188%
193  25.667  3101 3106 3111 VV    344335   6936850   0.81%   0.223%
194  25.724  3111 3114 3119 VV 4  102787   2736998   0.32%   0.088%
195  25.770  3119 3121 3131 VV 5   72598   2428682   0.28%   0.078%
 
196  25.875  3131 3136 3140 VV 7   48567   1393070   0.16%   0.045%
197  25.923  3140 3142 3154 VV 7   38875   1979315   0.23%   0.064%
198  26.041  3154 3159 3167 VV 6   50171   2264549   0.26%   0.073%
199  26.147  3167 3175 3178 VV 3  120454   3209691   0.37%   0.103%
200  26.195  3178 3182 3190 VV 2  130108   3429089   0.40%   0.110%
 
201  26.277  3190 3193 3198 VV 7   33364    875643   0.10%   0.028%
202  26.424  3212 3215 3219 VV 6   29023    743910   0.09%   0.024%
203  26.467  3219 3221 3222 VV 2   23735    264749   0.03%   0.009%
204  26.519  3222 3228 3238 VV 3   65070   2319009   0.27%   0.075%
205  26.595  3238 3239 3241 VV 2   24685    352500   0.04%   0.011%
 
206  26.646  3241 3246 3250 VV 8   30583   1004541   0.12%   0.032%
207  26.683  3250 3252 3256 VV 4   27180    623957   0.07%   0.020%
208  26.747  3256 3261 3263 VV     57249   1046323   0.12%   0.034%
209  26.782  3263 3266 3271 VV 5   78461   1999195   0.23%   0.064%
210  26.850  3271 3276 3288 VV   1823261  31314411   3.66%   1.008%
 
211  26.947  3288 3290 3296 VV 5   61638   1578058   0.18%   0.051%
212  27.056  3303 3306 3308 VV 4   35207    699620   0.08%   0.023%
213  27.090  3308 3310 3318 VV 9   37642   1348104   0.16%   0.043%
214  27.186  3318 3324 3329 VV 10   32017   1306628   0.15%   0.042%
215  27.287  3329 3339 3342 VV 10   37508   1563324   0.18%   0.050%
 
216  27.321  3342 3344 3345 VV 2   26754    307779   0.04%   0.010%
217  27.493  3365 3368 3372 VV 6   24844    583816   0.07%   0.019%
218  27.545  3372 3376 3384 VV     63528   1768789   0.21%   0.057%
219  27.614  3384 3386 3388 VV 3   25534    440154   0.05%   0.014%
220  27.644  3388 3390 3398 VV 8   28149    895934   0.10%   0.029%
 
221  27.744  3402 3405 3408 VV 5   21945    512167   0.06%   0.016%
222  27.809  3411 3414 3418 VV 6   27253    664600   0.08%   0.021%
223  27.894  3418 3426 3432 VV 9   34874   1454305   0.17%   0.047%
224  27.990  3432 3440 3448 VV 9   20398   1240305   0.14%   0.040%
225  28.083  3448 3453 3461 VV 9   22411   1024262   0.12%   0.033%
 
226  28.165  3461 3465 3469 VV 7   19515    557384   0.07%   0.018%
227  28.217  3469 3473 3475 VV 4   26211    542544   0.06%   0.017%
228  28.246  3475 3477 3480 VV 4   25296    451754   0.05%   0.015%
229  28.292  3480 3483 3488 VV 6   27236    785854   0.09%   0.025%
230  28.478  3505 3510 3515 VV 5   40829   1088944   0.13%   0.035%
 
231  28.584  3515 3525 3534 VV 5   49272   2322590   0.27%   0.075%
232  28.658  3534 3536 3543 VV 7   23396    886031   0.10%   0.029%
233  28.717  3543 3545 3548 VV 4   23957    467165   0.05%   0.015%
234  28.757  3548 3550 3553 VV 4   22658    390027   0.05%   0.013%
235  28.799  3553 3556 3563 VV 9   22526    855968   0.10%   0.028%
 
236  28.893  3567 3570 3574 VV 6   19582    535020   0.06%   0.017%
237  29.087  3588 3598 3605 VV 6   17362   1112522   0.13%   0.036%
238  29.150  3605 3607 3615 VV 9   17533    638360   0.07%   0.021%
239  29.234  3615 3619 3623 VV 7   18227    551331   0.06%   0.018%
240  29.282  3623 3626 3630 VV 6   17392    453842   0.05%   0.015%
 
241  29.348  3630 3635 3642 VV 10   18054    768738   0.09%   0.025%
242  29.434  3642 3648 3656 VV 6   32605   1107766   0.13%   0.036%
243  29.549  3660 3664 3669 VV 8   13278    450988   0.05%   0.015%
244  29.595  3669 3671 3679 VV 9   14952    535324   0.06%   0.017%
245  30.080  3734 3741 3747 VV 10   12031    477217   0.06%   0.015%
 
246  30.466  3793 3796 3798 VV 4    7545    137305   0.02%   0.004%
247  30.508  3798 3802 3810 VV 10    9171    326709   0.04%   0.011%
248  30.672  3813 3826 3831 VV 10    7462    467573   0.05%   0.015%
249  31.490  3940 3944 3953 VV 10    4428    124505   0.01%   0.004%
250  31.781  3982 3986 3988 PV 4    3106     45914   0.01%   0.001%
 
251  31.813  3988 3990 4006 VV 4    4487    171209   0.02%   0.006%
252  31.960  4006 4011 4012 VV 5    4670     77571   0.01%   0.002%
253  31.981  4012 4014 4023 VV 9    6862    145070   0.02%   0.005%
 
 
                        ͣ 3105291052
