

                       INSTRUMENT CONTROL PARAMETERS:    Instrument #1
                       -----------------------------------------------

   C:\MSDCHEM\1\METHODS\kath.m

Control Information
------- -----------
       Sample Inlet : GC
   Injection Source : GC/ALS
 Injection Location : ALS
             Use MS : Yes

=============================================================================
                                6890 GC METHOD
=============================================================================

OVEN
   Initial temp:  60 'C (On)               Maximum temp:  325 'C
   Initial time:  1.00 min                 Equilibration time:  3.00 min
   Ramps:
      #  Rate  Final temp  Final time
      1 10.00      180        0.00
      2  4.00      300       15.00
      3   0.0(Off)
   Post temp:  60 'C
   Post time:  0.00 min
   Run time:  58.00 min

FRONT INLET (SPLIT/SPLITLESS)           BACK INLET (UNKNOWN)
   Mode:  Splitless
   Initial temp:  250 'C (On)
   Pressure:  8.11 psi (On)
   Purge flow:  50.0 mL/min
   Purge time:  2.00 min
   Total flow:  53.7 mL/min
   Gas saver:  On
   Saver flow:  20.0 mL/min
   Saver time:  2.00 min
   Gas type:  Helium

COLUMN 1                                COLUMN 2
   Capillary Column                        (not installed)
   Model Number:  Agilent 19091S-433
   HP-5MS  5% Phenyl Methyl Siloxane
   Max temperature:  325 'C
   Nominal length:  30.0 m
   Nominal diameter:  250.00 um
   Nominal film thickness:  0.25 um
   Mode:  constant flow
   Initial flow:  1.0 mL/min
   Nominal init pressure:  8.12 psi
   Average velocity:  36 cm/sec
   Inlet:  Front Inlet
   Outlet:  MSD
   Outlet pressure:  vacuum

FRONT DETECTOR (FID)                    BACK DETECTOR (NO DET)
   Temperature:  250 'C (Off)
   Hydrogen flow:  40.0 mL/min (Off)
   Air flow:  450.0 mL/min (Off)
   Mode:  Constant makeup flow
   Makeup flow:  45.0 mL/min (Off)
   Makeup Gas Type: Nitrogen
   Flame:  Off
   Electrometer:  Off
   Lit offset:  2.0

SIGNAL 1                                SIGNAL 2
   Data rate:  20 Hz                       Data rate:  20 Hz
   Type:  test plot                        Type:  test plot
   Save Data:  Off                         Save Data:  Off
   Zero:  0.0 (Off)                        Zero:  0.0 (Off)
   Range:  0                               Range:  0
   Fast Peaks:  Off                        Fast Peaks:  Off
   Attenuation:  0                         Attenuation:  0

COLUMN COMP 1                           COLUMN COMP 2
   (No Detectors Installed)                (No Detectors Installed)

THERMAL AUX 2
   Use:  MSD Transfer Line Heater
   Description:  MSD Xfer
   Initial temp:  280 'C (On)
   Initial time:  0.00 min
      #  Rate  Final temp  Final time
      1   0.0(Off)

                                        POST RUN
                                           Post Time: 0.00 min

TIME TABLE
   Time       Specifier                     Parameter & Setpoint


                               GC Injector


     Front Injector:
        Sample Washes                 0
        Sample Pumps                  6
        Injection Volume           1.00 microliters
        Syringe Size               10.0 microliters
        PreInj Solvent A Washes       6
        PreInj Solvent B Washes       0
        PostInj Solvent A Washes      6
        PostInj Solvent B Washes      0
        Viscosity Delay               0 seconds
        Plunger Speed              Fast
        PreInjection Dwell         0.00 minutes
        PostInjection Dwell        0.00 minutes

     Back Injector:
No parameters specified

 Column 1 Inventory Number : AB002
 Column 2 Inventory Number :  

                                MS ACQUISITION PARAMETERS


General Information
------- -----------

Tune File                : atune.u
Acquistion Mode          : Scan


MS Information
-- -----------

Solvent Delay            : 4.00 min

EM Absolute              : False
EM Offset                : 0
Resulting EM Voltage     : 1882.4

[Scan Parameters]

Low Mass                 : 50.0
High Mass                : 650.0
Threshold                : 300
Sample #                 : 2       A/D Samples    4
Plot 2 low mass          : 50.0
Plot 2 high mass         : 650.0

[MSZones]

MS Quad                  : 150 C   maximum 200 C
MS Source                : 230 C   maximum 250 C


                             END OF MS ACQUISITION PARAMETERS


                              TUNE PARAMETERS for SN: US53921132
                        -----------------------------

 EMISSION    :      34.610
 ENERGY      :      69.922
 REPELLER    :      34.814
 IONFOCUS    :      90.157
 ENTRANCE_LE :      28.500
 EMVOLTS     :    1882.353
 AMUGAIN     :    2083.000
 AMUOFFSET   :     120.563
 FILAMENT    :       2.000
 DCPOLARITY  :       0.000
 ENTLENSOFFS :      17.569
 MASSGAIN    :    -529.000   
 MASSOFFSET  :     -42.000   


                           END OF TUNE PARAMETERS
                      ------------------------------------



                            END OF INSTRUMENT CONTROL PARAMETERS
                            ------------------------------------

