                      INSTRUMENT CONTROL PARAMETERS:    GC MSD
                      ----------------------------------------

   D:\MassHunter\GCMS\1\methods\1ul_Feihn_10_1splitM.M
      Fri Feb 07 17:32:18 2020

Control Information
------- -----------

Sample Inlet             : GC
Injection Source         : GC ALS
Injection Location:  Front
Mass Spectrometer        : Enabled


 No Sample Prep method has been assigned to this method.


GC
GC Summary
Run Time                                     37.5 min
Post Run Time                                0 min

Oven
Temperature
Setpoint                                     On
(Initial)                                    60 °C
Hold Time                                    1 min
Post Run                                     50 °C
Program
#1 Rate                                      10 °C/min
#1 Value                                     325 °C
#1 Hold Time                                 10 min


Equilibration Time                           0.2 min
Max Temperature                              350 °C
Maximum Temperature Override                 Disabled
Slow Fan                                     Disabled

ALS
Front Injector
Syringe Size                                 10 μL
Injection Volume                             1 μL
Solvent A Washes (PreInj)                    1
Solvent A Washes (PostInj)                   2
Solvent A Volume                             4 μL
Solvent B Washes (PreInj)                    1
Solvent B Washes (PostInj)                   2
Solvent B Volume                             4 μL
Sample Washes                                1
Sample Wash Volume                           1 μL
Sample Pumps                                 5
Dwell Time (PreInj)                          0 min
Dwell Time (PostInj)                         0 min
Solvent Wash Draw Speed                      300 μL/min
Solvent Wash Dispense Speed                  3000 μL/min
Sample Wash Draw Speed                       300 μL/min
Sample Wash Dispense Speed                   3000 μL/min
Injection Dispense Speed                     6000 μL/min
Viscosity Delay                              0 sec
Sample Depth                                 Disabled
Injection Type                               Standard
L1 Airgap                                    0 μL
Solvent Wash Mode                            A, B

Sample Overlap
Mode                                         Sample overlap is not enabled

ALS Errors                                   Pause for user interaction

Front SS Inlet He
Mode                                         Split
Heater                                       On    250 °C
Pressure                                     On    2.7803 psi
Total Flow                                   On    9.391 mL/min
Septum Purge Flow                            On    3 mL/min
Pre-Run Flow Test                            Off
Gas Saver                                    On    30 After 2 min mL/min
Split Ratio                                  10 :1
Split Flow                                   5.81 mL/min
Liner                                        A Liner has not been selected.

Column
Column #1
Flow
Setpoint                                     On
(Initial)                                    0.581 mL/min
Post Run                                     1 mL/min

Column Information                           Agilent 19091S-433UI: T741023H
HP-5MS UI                                    
Temperature Range                            -60 °C—325 °C (350 °C)
Dimensions                                   30 m x 250 μm x 0.25 μm
Column lock                                  Locked
In                                           Front SS Inlet He
Out                                          MSD 
(Initial)                                    60 °C
Pressure                                     2.7803 psi
Flow                                         0.581 mL/min
Average Velocity                             27.915 cm/sec
Holdup Time                                  1.7911 min
Control Mode                                 Constant Flow

Column Outlet Pressure                       0 psi

Detector Evaluation
Perform Detector Evaluation Test             Off
Signal Selected                              No Signal Selected
Checkout Sample                              No Checkout Sample Selected


MSD Transfer Line
Temperature
Setpoint                                     On
(Initial)                                    290 °C



Signals
Signal #1:  Test Plot
Description                                  Test Plot
Save                                         Off
Data Rate                                    50 Hz

Signal #2: 
Description                                  None

Signal #3: 
Description                                  None

Signal #4: 
Description                                  None

Signal #5: 
Description                                  None

Signal #6: 
Description                                  None

Signal #7: 
Description                                  None

Signal #8: 
Description                                  None




MS Information
-- -----------


General Information
------- -----------


Acquisition Mode         : Scan
Solvent Delay (minutes)  : 5.9
Tune file                : D:\MassHunter\GCMS\1\5977\atune.u
EM Setting mode Gain     : 1.000000

Normal or Fast Scanning  : Normal Scanning
Trace Ion Detection      : Off
Run Time (if MS only)    : 10 minutes 

[Scan Parameters]
Start Time               : 5.9
Low Mass                 : 50
High Mass                : 550
Threshold                : 150
A/D Samples:             : 2


[MSZones]

MS Source                   : 230 C   maximum 250 C
MS Quad                     : 150 C   maximum 200 C

Timed Events
----- ------
Number Events= 0



                     END OF MS ACQUISITION PARAMETERS


                        TUNE PARAMETERS for SN: US1948R019
                        ---------------------------------

 Trace Ion Detection is OFF.

    34.593   :   EMISSION     
    70.007   :   ENERGY       
    34.899   :   REPELLER     
    84.408   :   IONFOCUS     
    22.672   :   ENTRANCE_LENS
   812.855   :   EMVOLTS      
                              926.8  : Actual EMV 
                               1.00   : GAIN FACTOR 
  2418.000   :   AMUGAIN      
   137.750   :   AMUOFFSET    
     1.000   :   FILAMENT     
     0.000   :   DCPOLARITY   
    13.071   :   ENTLENSOFFSET
     0.000   :   Ion_Body     
     0.000   :   EXTLENS      
   -11.000   :  MASSGAIN        
   -24.000   :  MASSOFFSET      

                        END OF TUNE PARAMETERS
                        ----------------------



                        END OF INSTRUMENT CONTROL PARAMETERS
                        ------------------------------------
