                      INSTRUMENT CONTROL PARAMETERS:    lab
                      -------------------------------------

   D:\MassHunter\GCMS\1\METHODS\.M
      Wed Jun 12 12:57:57 2024

Control Information
------- -----------

Sample Inlet             : GC
Injection Source         : Manual
Mass Spectrometer        : Enabled


 No Sample Prep method has been assigned to this method.


GC
Oven
Temperature
Setpoint                                     On
(Initial)                                    60 °C
Hold Time                                    5 min
Post Run                                     50 °C
Program
#1 Rate                                      20 °C/min
#1 Value                                     300 °C
#1 Hold Time                                 5 min


Equilibration Time                           3 min
Max Temperature                              320 °C
Maximum Temperature Override                 Disabled
Slow Fan                                     Disabled
Cryo                                         Off

Front SS Inlet He
Mode                                         Split
Heater                                       On    300 °C
Pressure                                     On    8.2318 psi
Total Flow                                   On    9 mL/min
Septum Purge Flow                            On    3 mL/min
Gas Saver                                    Off
Split Ratio                                  5 :1
Split Flow                                   5 mL/min

Thermal Aux 2 (MSD Transfer Line)
Temperature
Setpoint                                     On
(Initial)                                    300 °C
Post Run                                     0 °C


Column
Column #1
Flow
Setpoint                                     Off
(Initial)                                    1 mL/min
Post Run                                     0.43242 mL/min

Agilent 19091S-433UI                         
HP-5ms Ultra Inert                           
0 °C—325 °C (350 °C): 30 m x 250 μm x 0.25 μm
Column lock                                  Unlocked
In                                           Front SS Inlet He
Out                                          MSD 
(Initial)                                    60 °C
Pressure                                     8.2318 psi
Flow                                         1 mL/min
Average Velocity                             36.623 cm/sec
Holdup Time                                  1.3653 min

Column Outlet Pressure                       0 psi

Valve 1
Other                                        Off

PCM C
PCM C He
Pressure
Setpoint                                     Off
(Initial)                                    10 psi
Post Run                                     0 psi

                                             ***Excluded from Affecting GC's Readiness State***

Aux PCM C N2
Pressure
Setpoint                                     Off
(Initial)                                    10 psi
Post Run                                     0 psi

                                             ***Excluded from Affecting GC's Readiness State***


Valve Box
                                             ***Excluded from Affecting GC's Readiness State***
Heater                                       Off

Signals
Signal #1:  Test Plot
Description                                  Test Plot
Details                                      
Save                                         Off
Data Rate                                    50 Hz
Dual Injection Assignment                    Front Sample

Signal #2:  Test Plot
Description                                  Test Plot
Details                                      
Save                                         Off
Data Rate                                    50 Hz
Dual Injection Assignment                    Back Sample

Signal #3:  Test Plot
Description                                  Test Plot
Details                                      
Save                                         Off
Data Rate                                    50 Hz
Dual Injection Assignment                    Back Sample

Signal #4:  Test Plot
Description                                  Test Plot
Details                                      
Save                                         Off
Data Rate                                    50 Hz
Dual Injection Assignment                    Back Sample




MS Information
-- -----------


General Information
------- -----------

Acquisition Mode         : Scan
Solvent Delay (minutes)  : 8
Tune file                : D:\MassHunter\GCMS\1\5977\15122021.u
EM Setting mode Delta    : 0.000000

Normal or Fast Scanning  : Normal Scanning
Trace Ion Detection      : Off
Run Time (if MS only)    : 650 minutes 

[Scan Parameters]
Start Time               : 8
Low Mass                 : 50
High Mass                : 550
Threshold                : 150
A/D Samples:             : 4


[MSZones]

MS Source                   : 230 C   maximum 250 C
MS Quad                     : 150 C   maximum 200 C

Timed Events
----- ------
Number Events= 0



                     END OF MS ACQUISTION PARAMETERS


                        TUNE PARAMETERS for SN: US1620L401
                        ---------------------------------

 Trace Ion Detection is OFF.

 EMISSION    :      34.593
 ENERGY      :      70.007
 REPELLER    :      33.106
 IONFOCUS    :      90.331
 ENTRANCE_LE :      20.181
 EMVOLTS     :    1417.872
                               Actual EMV :  1417.9
                               GAIN FACTOR :   0.31
 AMUGAIN     :    1625.000
 AMUOFFSET   :     125.563
 FILAMENT    :       2.000
 DCPOLARITY  :       0.000
 ENTLENSOFFS :      15.312
 Ion_Body    :       0.000
 EXTLENS     :       0.005
 MASSGAIN    :    -233.000   
 MASSOFFSET  :     -37.000   

                        END OF TUNE PARAMETERS
                        ----------------------



                      END OF INSTRUMENT CONTROL PARAMETERS
                      ------------------------------------
