Return to study ST002000 main page
MB Sample ID: SA186908
| Local Sample ID: | AB014_008 |
| Subject ID: | SU002081 |
| Subject Type: | Human |
| Subject Species: | Homo sapiens |
| Taxonomy ID: | 9606 |
Select appropriate tab below to view additional metadata details:
Subject:
| Subject ID: | SU002081 |
| Subject Type: | Human |
| Subject Species: | Homo sapiens |
| Taxonomy ID: | 9606 |
Factors:
| Local Sample ID | MB Sample ID | Factor Level ID | Level Value | Factor Name |
|---|---|---|---|---|
| AB014_008 | SA186908 | FL023122 | case | treatment |
Collection:
| Collection ID: | CO002074 |
| Collection Summary: | Human plasma were collected and flash-frozen. |
| Sample Type: | Blood (plasma) |
Treatment:
| Treatment ID: | TR002093 |
| Treatment Summary: | blinded |
Sample Preparation:
| Sampleprep ID: | SP002087 |
| Sampleprep Summary: | Human plasma from cases and controls were collected and flash-frozen. |
Combined analysis:
| Analysis ID | AN003263 |
|---|---|
| Analysis type | MS |
| Chromatography type | GC |
| Chromatography system | Gerstel CIS4 –with dual MPS Injector/ Agilent 6890 GC- Pegasus III TOF MS |
| Column | Rtx-5Sil MS |
| MS Type | EI |
| MS instrument type | GC-TOF |
| MS instrument name | Leco Pegasus IV TOF |
| Ion Mode | UNSPECIFIED |
| Units | normalized peak height |
Chromatography:
| Chromatography ID: | CH002407 |
| Chromatography Summary: | Gas Chromatography conditions: A 30 m long, 0.25 mm i.d. Rtx-5Sil MS column (0.25 μm 95% dimethyl 5% diphenyl polysiloxane film) with additional 10 m integrated guard column is used (Restek, Bellefonte PA). 99.9999% pure Helium with built-in purifier (Airgas, Radnor PA) is set at constant flow of 1 ml/min. The oven temperature is held constant at 50°C for 1 min and then ramped at 20°C/min to 330°C at which it is held constant for 5 min. |
| Instrument Name: | Gerstel CIS4 –with dual MPS Injector/ Agilent 6890 GC- Pegasus III TOF MS |
| Column Name: | Rtx-5Sil MS |
| Chromatography Type: | GC |
MS:
| MS ID: | MS003035 |
| Analysis ID: | AN003263 |
| Instrument Name: | Leco Pegasus IV TOF |
| Instrument Type: | GC-TOF |
| MS Type: | EI |
| MS Comments: | Mass spectrometer settings: A Leco Pegasus IV time of flight mass spectrometer is controlled by the Leco ChromaTOF software vs. 2.32 (St. Joseph, MI). The transfer line temperature between gas chromatograph and mass spectrometer is set to 280°C. Electron impact ionization at 70V is employed with an ion source temperature of 250°C. Acquisition rate is 17 spectra/second, with a scan mass range of 85-500 Da. |
| Ion Mode: | UNSPECIFIED |
