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MB Sample ID: SA265209

Local Sample ID:90444016808
Subject ID:SU002778
Subject Type:Mammal
Subject Species:Rattus norvegicus
Taxonomy ID:10116

Select appropriate tab below to view additional metadata details:

Subject:

Subject ID:SU002778
Subject Type:Mammal
Subject Species:Rattus norvegicus
Taxonomy ID:10116

Factors:

Local Sample IDMB Sample IDFactor Level IDLevel ValueFactor Name
90444016808SA265209FL034699TrainingGroup
90444016808SA265209FL0346992 weeks of trainingTimepoint
90444016808SA265209FL034699MaleSex

Collection:

Collection ID:CO002771
Collection Summary:-
Sample Type:Liver

Treatment:

Treatment ID:TR002787
Treatment Summary:-

Sample Preparation:

Sampleprep ID:SP002784
Sampleprep Summary:See SOP
Sampleprep Protocol Filename:pass1b_experimental_design_metabolomics.pdf

Combined analysis:

Analysis ID AN004348
Analysis type MS
Chromatography type Reversed phase
Chromatography system Agilent 1290 Infinity II
Column Agilent ZORBAX RRHD Extend C18 (150 x 2.1mm, 1.8µm,80A,1200 bar)
MS Type ESI
MS instrument type QTOF
MS instrument name Agilent 6530 QTOF
Ion Mode NEGATIVE
Units peak area

Chromatography:

Chromatography ID:CH003254
Methods Filename:pass1b_rpneg_rppos_ionpneg_methods.pdf
Instrument Name:Agilent 1290 Infinity II
Column Name:Agilent ZORBAX RRHD Extend C18 (150 x 2.1mm, 1.8µm,80A,1200 bar)
Column Temperature:35C
Flow Gradient:t=0 min: 100%/0% (%A/%B) @ 0.25 ml/min | t=2 min: 100%/0% (%A/%B) @ 0.25 ml/min | t=12 min: 1%/99% (%A/%B) @ 0.25 ml/min | t=18 min: 1%/99% (%A/%B) @ 0.25 ml/min | t=28 min: 100%/0% (%A/%B) @ 0.40 ml/min | t=29.9 min: 100%/0% (%A/%B) @ 0.40 ml/min | t=30 min: 100%/0% (%A/%B) @ 0.25 ml/min
Flow Rate:0.25 ml/min; 0.4 ml/min
Solvent A:97% water/3% methanol; 15 mM tributylamine; 10 mM acetic
Solvent B:100% methanol; 15 mM tributylamine; 10 mM acetic acid
Chromatography Type:Reversed phase

MS:

MS ID:MS004095
Analysis ID:AN004348
Instrument Name:Agilent 6530 QTOF
Instrument Type:QTOF
MS Type:ESI
Ion Mode:NEGATIVE
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