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MB Sample ID: SA174914

Local Sample ID:210514_IJ4colmo_1.cdf
Subject ID:SU001956
Subject Type:Plant
Subject Species:Saccharum spp

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Combined analysis:

Analysis ID AN003039
Analysis type MS
Chromatography type GC
Chromatography system Agilent 7890A
Column Agilent DB5 (20m x 0.18 mm i.d. x 0.18 μm)
MS Type EI
MS instrument type GC x GC-TOF
MS instrument name Leco Pegasus 4D GCxGC TOF
Ion Mode UNSPECIFIED
Units relative intensity

Chromatography:

Chromatography ID:CH002254
Chromatography Summary:One microliter of each derivatized sample was injected splitless into a gas chromatograph 7890A (Agilent Technologies, Santa Clara, USA) coupled with a Comb-xt Autosampler (Leap Technologies, Carrboro, USA). A 20m x 0.18 mm i.d. x 0.18 μm film thickness, DB5 GC capillary column (Agilent Technologies) was used as the primary column and the secondary GC columns was a 0.69 m x 0.1 mm i.d. x 0.1 μm film thickness (Rxi-17 Restek, Bellefonte, USA). The injector temperature was 280°C, the septum purge flow rate was 20 ml min-1 and the purge was turned on after 60 s. The gas helium flow rate through the column was 1 ml min-1, the column temperature was held at 80°C for 2 min, then increased by 15°C min-1 to 305°C, and held there for 10 min.
Instrument Name:Agilent 7890A
Column Name:Agilent DB5 (20m x 0.18 mm i.d. x 0.18 μm)
Chromatography Type:GC
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