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MB Sample ID: SA176342

Local Sample ID:KA-012
Subject ID:SU001980
Subject Type:Mammal
Subject Species:Homo sapiens
Taxonomy ID:9606

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Combined analysis:

Analysis ID AN003093 AN003094
Analysis type MS MS
Chromatography type HILIC HILIC
Chromatography system Q Exactive Q Exactive
Column Luna 3 mm NH2 100 A Luna 3 mm NH2 100 A
MS Type API API
MS instrument type Orbitrap Orbitrap
MS instrument name Thermo Q Exactive Orbitrap Thermo Q Exactive Orbitrap
Ion Mode POSITIVE NEGATIVE
Units area area

Chromatography:

Chromatography ID:CH002284
Chromatography Summary:Mobile phase A was 5 mM ammonium acetate (NH4AcO), pH 9.9, B was acetonitrile and the separation achieved on a Luna 3 mm NH2 100 A column (150 × 2.0 mm, Phenomenex). The flow was 200 μL/min, and the gradient ran from 15% A to 95% A in 18 min, followed by an isocratic step for 9 min and re-equilibration for 7 min.
Instrument Name:Q Exactive
Column Name:Luna 3 mm NH2 100 A
Flow Rate:200 uL/min
Solvent A:100% water; 5 mM ammonium acetate, pH 9.9
Solvent B:100% acetonitrile
Chromatography Type:HILIC
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