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MB Sample ID: SA176342
Local Sample ID: | KA-012 |
Subject ID: | SU001980 |
Subject Type: | Mammal |
Subject Species: | Homo sapiens |
Taxonomy ID: | 9606 |
Select appropriate tab below to view additional metadata details:
Combined analysis:
Analysis ID | AN003093 | AN003094 |
---|---|---|
Analysis type | MS | MS |
Chromatography type | HILIC | HILIC |
Chromatography system | Q Exactive | Q Exactive |
Column | Luna 3 mm NH2 100 A | Luna 3 mm NH2 100 A |
MS Type | API | API |
MS instrument type | Orbitrap | Orbitrap |
MS instrument name | Thermo Q Exactive Orbitrap | Thermo Q Exactive Orbitrap |
Ion Mode | POSITIVE | NEGATIVE |
Units | area | area |
Chromatography:
Chromatography ID: | CH002284 |
Chromatography Summary: | Mobile phase A was 5 mM ammonium acetate (NH4AcO), pH 9.9, B was acetonitrile and the separation achieved on a Luna 3 mm NH2 100 A column (150 × 2.0 mm, Phenomenex). The flow was 200 μL/min, and the gradient ran from 15% A to 95% A in 18 min, followed by an isocratic step for 9 min and re-equilibration for 7 min. |
Instrument Name: | Q Exactive |
Column Name: | Luna 3 mm NH2 100 A |
Flow Rate: | 200 uL/min |
Solvent A: | 100% water; 5 mM ammonium acetate, pH 9.9 |
Solvent B: | 100% acetonitrile |
Chromatography Type: | HILIC |