Return to study ST001993 main page
MB Sample ID: SA186732
| Local Sample ID: | 64 |
| Subject ID: | SU002074 |
| Subject Type: | Human |
| Subject Species: | Homo sapiens |
| Taxonomy ID: | 9606 |
Select appropriate tab below to view additional metadata details:
Combined analysis:
| Analysis ID | AN003250 |
|---|---|
| Analysis type | MS |
| Chromatography type | Unspecified |
| Chromatography system | 7100 capillary electrophoresis (CE) |
| Column | fused-silica capillary from Agilent Technologies (total length,100 cm; inner diameter,50um) |
| MS Type | ESI |
| MS instrument type | Other |
| MS instrument name | Agilent 6230 TOF |
| Ion Mode | POSITIVE |
| Units | Peak Area |
Chromatography:
| Chromatography ID: | CH002395 |
| Chromatography Summary: | Metabolite separation was carried out using a previously developed method in a fused-silica capillary from Agilent Technologies (total length, 100 cm; inner diameter, 50 µm) 1. Before each analysis, the capillary was flushed with background electrolyte (BGE) (1 M formic acid in 10% MeOH) for 5 min at 950 mbar. Samples were injected over 50 s at 50 mbar, and to improve the analysis reproducibility, BGE was injected for 10 s at 100 mbar after each sample injection. The separation was performed with an internal pressure of 25 mbar and 30 kV voltage, and the current observed under these conditions was 30 µA. The total analytical run time was 35 min. |
| Instrument Name: | 7100 capillary electrophoresis (CE) |
| Column Name: | fused-silica capillary from Agilent Technologies (total length,100 cm; inner diameter,50um) |
| Chromatography Type: | Unspecified |
