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MB Sample ID: SA187420

Local Sample ID:GH024_156
Subject ID:SU002084
Subject Type:Human
Subject Species:Homo sapiens
Taxonomy ID:9606

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Combined analysis:

Analysis ID AN003266
Analysis type MS
Chromatography type HILIC
Chromatography system Agilent 6600
Column Waters Acquity UPLC BEH amide,(150 x 2.1mm,1.7um)
MS Type ESI
MS instrument type TTOF
MS instrument name Agilent 6560 Ion Mobility
Ion Mode POSITIVE
Units normalized peak height

Chromatography:

Chromatography ID:CH002410
Chromatography Summary:The LC/QTOFMS analyses are performed using an Agilent 1290 Infinity LC system (G4220A binary pump, G4226A autosampler, and G1316C Column Thermostat) coupled to a SCIEX Triple TOF mass spectrometer. Polar compounds are separated on an Acquity UPLC BEH Amide Column, 130Å, 1.7 µm, 2.1 mm X 150 mm maintained at 45°C at a flow-rate of 0.4 mL/min. Solvent pre-heating (Agilent G1316) was used. The mobile phases consist of: Water, 10 mM Ammonium Formate, 0.125% Formic Acid (A) and Acetonitrile: Water (95/5, v/v), 10 mM Ammonium Formate, 0.125% Formic Acid (B)
Instrument Name:Agilent 6600
Column Name:Waters Acquity UPLC BEH amide,(150 x 2.1mm,1.7um)
Column Temperature:45
Flow Rate:0.4 mL/min
Solvent A:100% water; 0.125% formic acid; 10 mM ammonium formate
Solvent B:95% acetonitrile/5% water; 0.125% formic acid; 10 mM ammonium formate
Chromatography Type:HILIC
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