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MB Sample ID: SA214327
| Local Sample ID: | Patient_Negative_OP_33 |
| Subject ID: | SU002329 |
| Subject Type: | Human |
| Subject Species: | Homo sapiens |
| Taxonomy ID: | 9606 |
Select appropriate tab below to view additional metadata details:
Combined analysis:
| Analysis ID | AN003661 | AN003662 |
|---|---|---|
| Analysis type | MS | MS |
| Chromatography type | Reversed phase | Reversed phase |
| Chromatography system | Thermo Dionex Ultimate 3000 | Thermo Dionex Ultimate 3000 |
| Column | Thermo Accucore C18 (100 x 2.1mm,2.6um) | Thermo Accucore C18 (100 x 2.1mm,2.6um) |
| MS Type | ESI | ESI |
| MS instrument type | Orbitrap | Orbitrap |
| MS instrument name | Thermo Q Exactive HF hybrid Orbitrap | Thermo Q Exactive HF hybrid Orbitrap |
| Ion Mode | POSITIVE | NEGATIVE |
| Units | intensity | intensity |
Chromatography:
| Chromatography ID: | CH002713 |
| Instrument Name: | Thermo Dionex Ultimate 3000 |
| Column Name: | Thermo Accucore C18 (100 x 2.1mm,2.6um) |
| Column Temperature: | 35 |
| Flow Gradient: | 0 min, 90% A; 1 min, 90% A; 4 min, 60% A; 12 min, 25% A; 21 min, 1% A; 24 min, 1% A; 24.1 min, 90% A; 28 min, 90%. |
| Flow Rate: | 0.4 ml/min |
| Injection Temperature: | 4 |
| Solvent A: | 50% acetonitrile/50% water; 0.1% formic acid; 10 mM ammonium formate |
| Solvent B: | 10% acetonitrile/88% isopropanol/2% water; 0.02% formic acid; 2 mM ammonium formate |
| Analytical Time: | 28min |
| Chromatography Type: | Reversed phase |
