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MB Sample ID: SA255553
| Local Sample ID: | BH3_009 |
| Subject ID: | SU002640 |
| Subject Type: | Cultured cells |
| Subject Species: | Homo sapiens |
| Taxonomy ID: | 9606 |
Select appropriate tab below to view additional metadata details:
Combined analysis:
| Analysis ID | AN004185 |
|---|---|
| Analysis type | MS |
| Chromatography type | GC |
| Chromatography system | Agilent 7890C with Leco Pegasus HT |
| Column | Restek Rtx-5Sil (30m x 0.25mm,0.25um) |
| MS Type | EI |
| MS instrument type | GC x GC-TOF |
| MS instrument name | Agilent 7890C |
| Ion Mode | POSITIVE |
| Units | Peak height |
Chromatography:
| Chromatography ID: | CH003101 |
| Chromatography Summary: | Column name: Restek corporation Rtx-5Sil MS (30 m length x 0.25 mm internal diameter with 0.25 μm film made of 95% dimethyl/5%diphenylpolysiloxane) |
| Methods Filename: | majd-et-al-csc-protocol.pdf |
| Instrument Name: | Agilent 7890C with Leco Pegasus HT |
| Column Name: | Restek Rtx-5Sil (30m x 0.25mm,0.25um) |
| Column Temperature: | The GC oven was set to hold at 50C for 1 min then ramped to 20C/min to 330C and then held for 5 min |
| Flow Gradient: | helium flow |
| Flow Rate: | 1 mL/min |
| Solvent A: | 1mL of 3:3:2 ACN:IPA:H2O (v/v/v) |
| Solvent B: | 10 uL of 40 mg/mL of Methoxyamine in pyridine then Then 91 uL of MSTFA + FAMEs |
| Chromatography Type: | GC |
