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MB Sample ID: SA256771
| Local Sample ID: | sample_0130 |
| Subject ID: | SU002655 |
| Subject Type: | Human |
| Subject Species: | Homo sapiens |
| Taxonomy ID: | 9606 |
| Gender: | Not applicable |
Select appropriate tab below to view additional metadata details:
Combined analysis:
| Analysis ID | AN004206 |
|---|---|
| Analysis type | MS |
| Chromatography type | Reversed phase |
| Chromatography system | Agilent 1290 Infinity II |
| Column | Waters ACQUITY UPLC BEH C18 (100 x 2.1mm,1.7um) |
| MS Type | ESI |
| MS instrument type | QTOF |
| MS instrument name | Agilent 6545 QTOF |
| Ion Mode | NEGATIVE |
| Units | ng/ml |
Chromatography:
| Chromatography ID: | CH003117 |
| Instrument Name: | Agilent 1290 Infinity II |
| Column Name: | Waters ACQUITY UPLC BEH C18 (100 x 2.1mm,1.7um) |
| Column Temperature: | 50 |
| Flow Gradient: | from min 0-1.5, the percentage of phase B was increased from 5% to 30%, from min 1.5-4.5, the percentage of B was increased to 70%, from min 4.5-7.5 the percentage of B was increased to 100% and held for 5.5 mins. A post-time of 5 min was used to regain the initial conditions for the next analysis. |
| Flow Rate: | 0.4 mL/min |
| Solvent A: | 70% water/30% methanol; 2mM ammonium acetate |
| Solvent B: | 100% methanol; 2mM ammonium acetate |
| Chromatography Type: | Reversed phase |
