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MB Sample ID: SA257309

Local Sample ID:B4_RP_pos
Subject ID:SU002659
Subject Type:Human
Subject Species:Homo sapiens
Taxonomy ID:9606
Age Or Age Range:82
Gender:Female

Select appropriate tab below to view additional metadata details:


Combined analysis:

Analysis ID AN004214 AN004215 AN004216 AN004217
Analysis type MS MS MS MS
Chromatography type HILIC HILIC Reversed phase Reversed phase
Chromatography system Thermo Dionex Ultimate 3000 Thermo Dionex Ultimate 3000 Thermo Dionex Ultimate 3000 Thermo Dionex Ultimate 3000
Column Agilent InfinityLab Poroshell 120 HILIC-Z (150 x 2.1mm,2.7um) Agilent InfinityLab Poroshell 120 HILIC-Z (150 x 2.1mm,2.7um) Thermo Accucore C18 (150 x 2.1mm,2.6um) Thermo Accucore C18 (150 x 2.1mm,2.6um)
MS Type ESI ESI ESI ESI
MS instrument type QTOF QTOF QTOF QTOF
MS instrument name ABI Sciex 6600 TripleTOF ABI Sciex 6600 TripleTOF ABI Sciex 6600 TripleTOF ABI Sciex 6600 TripleTOF
Ion Mode POSITIVE NEGATIVE POSITIVE NEGATIVE
Units area integration area integration area integration area integration

Chromatography:

Chromatography ID:CH003124
Chromatography Summary:Hilic ESI+
Instrument Name:Thermo Dionex Ultimate 3000
Column Name:Agilent InfinityLab Poroshell 120 HILIC-Z (150 x 2.1mm,2.7um)
Column Temperature:50 °C
Flow Gradient:0 min 98% B 3 min 98% B 23 min 5% B 24 min 5% B 24 min 98% B
Flow Rate:0.25 ml/min
Sample Injection:5 μL
Solvent A:10 mM ammonium formate and 0.1 % formic acid in water
Solvent B:9:1 acetonitrile / 10 mM ammonium formate and 0.1 % formic acid in water
Chromatography Type:HILIC
  
Chromatography ID:CH003125
Chromatography Summary:Hilic ESI-
Instrument Name:Thermo Dionex Ultimate 3000
Column Name:Agilent InfinityLab Poroshell 120 HILIC-Z (150 x 2.1mm,2.7um)
Column Temperature:50 °C
Flow Gradient:0 min 96% B 2 min 96% B 22 min 65% B 24 min 65% B 24 min 96% B
Flow Rate:0.25 ml/min
Sample Injection:5 μL
Solvent A:10 mM ammonium acetate, pH 9 with ammonium hydroxide and 10 µM medronic acid
Solvent B:85:15 acetonitrile / 10 mM ammonium acetate, pH 9 with ammonium hydroxide and 10 µM medronic acid in water
Chromatography Type:HILIC
  
Chromatography ID:CH003126
Chromatography Summary:RP ESI+
Instrument Name:Thermo Dionex Ultimate 3000
Column Name:Thermo Accucore C18 (150 x 2.1mm,2.6um)
Column Temperature:40 °C
Flow Gradient:0 min 5% B 1 min 5% B 8 min 100% B 10 min 100% B 10 min 5% B
Flow Rate:0.3 ml/min
Sample Injection:5 μL
Solvent A:0.1 % formic acid in water
Solvent B:0.1 % formic acid in 98:2 acetonitrile / water
Chromatography Type:Reversed phase
  
Chromatography ID:CH003127
Chromatography Summary:RP ESI-
Instrument Name:Thermo Dionex Ultimate 3000
Column Name:Thermo Accucore C18 (150 x 2.1mm,2.6um)
Column Temperature:40 °C
Flow Gradient:0 min 5% B 1 min 5% B 8 min 100% B 10 min 100% B 10 min 5% B
Flow Rate:0.3 ml/min
Sample Injection:5 μL
Solvent A:0.1 % formic acid in water
Solvent B:0.1 % formic acid in 98:2 acetonitrile / water
Chromatography Type:Reversed phase
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