Return to study ST002558 main page
MB Sample ID: SA257309
| Local Sample ID: | B4_RP_pos |
| Subject ID: | SU002659 |
| Subject Type: | Human |
| Subject Species: | Homo sapiens |
| Taxonomy ID: | 9606 |
| Age Or Age Range: | 82 |
| Gender: | Female |
Select appropriate tab below to view additional metadata details:
Combined analysis:
| Analysis ID | AN004214 | AN004215 | AN004216 | AN004217 |
|---|---|---|---|---|
| Analysis type | MS | MS | MS | MS |
| Chromatography type | HILIC | HILIC | Reversed phase | Reversed phase |
| Chromatography system | Thermo Dionex Ultimate 3000 | Thermo Dionex Ultimate 3000 | Thermo Dionex Ultimate 3000 | Thermo Dionex Ultimate 3000 |
| Column | Agilent InfinityLab Poroshell 120 HILIC-Z (150 x 2.1mm,2.7um) | Agilent InfinityLab Poroshell 120 HILIC-Z (150 x 2.1mm,2.7um) | Thermo Accucore C18 (150 x 2.1mm,2.6um) | Thermo Accucore C18 (150 x 2.1mm,2.6um) |
| MS Type | ESI | ESI | ESI | ESI |
| MS instrument type | QTOF | QTOF | QTOF | QTOF |
| MS instrument name | ABI Sciex 6600 TripleTOF | ABI Sciex 6600 TripleTOF | ABI Sciex 6600 TripleTOF | ABI Sciex 6600 TripleTOF |
| Ion Mode | POSITIVE | NEGATIVE | POSITIVE | NEGATIVE |
| Units | area integration | area integration | area integration | area integration |
Chromatography:
| Chromatography ID: | CH003124 |
| Chromatography Summary: | Hilic ESI+ |
| Instrument Name: | Thermo Dionex Ultimate 3000 |
| Column Name: | Agilent InfinityLab Poroshell 120 HILIC-Z (150 x 2.1mm,2.7um) |
| Column Temperature: | 50 °C |
| Flow Gradient: | 0 min 98% B 3 min 98% B 23 min 5% B 24 min 5% B 24 min 98% B |
| Flow Rate: | 0.25 ml/min |
| Sample Injection: | 5 μL |
| Solvent A: | 10 mM ammonium formate and 0.1 % formic acid in water |
| Solvent B: | 9:1 acetonitrile / 10 mM ammonium formate and 0.1 % formic acid in water |
| Chromatography Type: | HILIC |
| Chromatography ID: | CH003125 |
| Chromatography Summary: | Hilic ESI- |
| Instrument Name: | Thermo Dionex Ultimate 3000 |
| Column Name: | Agilent InfinityLab Poroshell 120 HILIC-Z (150 x 2.1mm,2.7um) |
| Column Temperature: | 50 °C |
| Flow Gradient: | 0 min 96% B 2 min 96% B 22 min 65% B 24 min 65% B 24 min 96% B |
| Flow Rate: | 0.25 ml/min |
| Sample Injection: | 5 μL |
| Solvent A: | 10 mM ammonium acetate, pH 9 with ammonium hydroxide and 10 µM medronic acid |
| Solvent B: | 85:15 acetonitrile / 10 mM ammonium acetate, pH 9 with ammonium hydroxide and 10 µM medronic acid in water |
| Chromatography Type: | HILIC |
| Chromatography ID: | CH003126 |
| Chromatography Summary: | RP ESI+ |
| Instrument Name: | Thermo Dionex Ultimate 3000 |
| Column Name: | Thermo Accucore C18 (150 x 2.1mm,2.6um) |
| Column Temperature: | 40 °C |
| Flow Gradient: | 0 min 5% B 1 min 5% B 8 min 100% B 10 min 100% B 10 min 5% B |
| Flow Rate: | 0.3 ml/min |
| Sample Injection: | 5 μL |
| Solvent A: | 0.1 % formic acid in water |
| Solvent B: | 0.1 % formic acid in 98:2 acetonitrile / water |
| Chromatography Type: | Reversed phase |
| Chromatography ID: | CH003127 |
| Chromatography Summary: | RP ESI- |
| Instrument Name: | Thermo Dionex Ultimate 3000 |
| Column Name: | Thermo Accucore C18 (150 x 2.1mm,2.6um) |
| Column Temperature: | 40 °C |
| Flow Gradient: | 0 min 5% B 1 min 5% B 8 min 100% B 10 min 100% B 10 min 5% B |
| Flow Rate: | 0.3 ml/min |
| Sample Injection: | 5 μL |
| Solvent A: | 0.1 % formic acid in water |
| Solvent B: | 0.1 % formic acid in 98:2 acetonitrile / water |
| Chromatography Type: | Reversed phase |
