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MB Sample ID: SA258032
| Local Sample ID: | 2021-11-29_005_H2_E2 |
| Subject ID: | SU002668 |
| Subject Type: | Human |
| Subject Species: | Homo sapiens |
| Taxonomy ID: | 9606 |
| Gender: | Male |
Select appropriate tab below to view additional metadata details:
Combined analysis:
| Analysis ID | AN004228 |
|---|---|
| Analysis type | MS |
| Chromatography type | Reversed phase |
| Chromatography system | Agilent 6530 qTOF |
| Column | Agilent Zorbax Extend C18 (150 x 2.1mm, 1.8um) with matched guard column |
| MS Type | ESI |
| MS instrument type | QTOF |
| MS instrument name | Agilent 6530 QTOF |
| Ion Mode | NEGATIVE |
| Units | EicCoreArea/Peak Area |
Chromatography:
| Chromatography ID: | CH003137 |
| Methods Filename: | experiment_metadata |
| Instrument Name: | Agilent 6530 qTOF |
| Column Name: | Agilent Zorbax Extend C18 (150 x 2.1mm, 1.8um) with matched guard column |
| Column Temperature: | 35°C |
| Flow Gradient: | 0-2min hold 100/0/0 (%A/%B/%C); 2-12 min linear to 1/99/0, 12-20 min hold 1/99/0, 20-20.5 min linear to 5/0/95, 20.5-26.1 5/0/95, 26.1-26.3 min linear to 100/0/0, 26.3-33 min hold 100/0/0 |
| Flow Rate: | 0-20.5 min hold 0.25mL/min, [18 min switch flow direction to backflush], 20.5-21.5 linear to 0.4mL/min, 21.5-22.3 linear to 0.8 mL/min, [26 min switch flow direction to forward] 26-26.1 linear to 0.6mL/min, 26.1-26.3 linear to 0.4 mL/min, 26.3-31.8 min hold 0.4mL/min, 31.8-32 min linear to 0.25mL/min |
| Solvent A: | 97% water/3% methanol; 10 mM tributylamine; 5mM acetic acid |
| Solvent B: | 100% methanol; 10 mM tributylamine; 5mM acetic acid |
| Chromatography Type: | Reversed phase |
