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MB Sample ID: SA264604
Local Sample ID: | 90217016606 |
Subject ID: | SU002771 |
Subject Type: | Mammal |
Subject Species: | Rattus norvegicus |
Taxonomy ID: | 10114 10116 |
Select appropriate tab below to view additional metadata details:
Combined analysis:
Analysis ID | AN004341 |
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Analysis type | MS |
Chromatography type | Reversed phase |
Chromatography system | Agilent 1290 Infinity II |
Column | Agilent ZORBAX RRHD Extend C18 (150 x 2.1mm, 1.8µm,80A,1200 bar) |
MS Type | ESI |
MS instrument type | QTOF |
MS instrument name | Agilent 6530 QTOF |
Ion Mode | NEGATIVE |
Units | peak area |
Chromatography:
Chromatography ID: | CH003247 |
Methods Filename: | pass1b_rpneg_rppos_ionpneg_methods.pdf |
Instrument Name: | Agilent 1290 Infinity II |
Column Name: | Agilent ZORBAX RRHD Extend C18 (150 x 2.1mm, 1.8µm,80A,1200 bar) |
Column Temperature: | 35C |
Flow Gradient: | t=0 min: 100%/0% (%A/%B) @ 0.25 ml/min | t=2 min: 100%/0% (%A/%B) @ 0.25 ml/min | t=12 min: 1%/99% (%A/%B) @ 0.25 ml/min | t=18 min: 1%/99% (%A/%B) @ 0.25 ml/min | t=28 min: 100%/0% (%A/%B) @ 0.40 ml/min | t=29.9 min: 100%/0% (%A/%B) @ 0.40 ml/min | t=30 min: 100%/0% (%A/%B) @ 0.25 ml/min |
Flow Rate: | 0.25 ml/min; 0.4 ml/min |
Solvent A: | 97% water/3% methanol; 15 mM tributylamine; 10 mM acetic |
Solvent B: | 100% methanol; 15 mM tributylamine; 10 mM acetic acid |
Chromatography Type: | Reversed phase |