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MB Sample ID: SA264675
| Local Sample ID: | 90280016606 |
| Subject ID: | SU002771 |
| Subject Type: | Mammal |
| Subject Species: | Rattus norvegicus |
| Taxonomy ID: | 10114 10116 |
Select appropriate tab below to view additional metadata details:
Combined analysis:
| Analysis ID | AN004341 |
|---|---|
| Analysis type | MS |
| Chromatography type | Reversed phase |
| Chromatography system | Agilent 1290 Infinity II |
| Column | Agilent ZORBAX RRHD Extend C18 (150 x 2.1mm, 1.8µm,80A,1200 bar) |
| MS Type | ESI |
| MS instrument type | QTOF |
| MS instrument name | Agilent 6530 QTOF |
| Ion Mode | NEGATIVE |
| Units | peak area |
Chromatography:
| Chromatography ID: | CH003247 |
| Methods Filename: | pass1b_rpneg_rppos_ionpneg_methods.pdf |
| Instrument Name: | Agilent 1290 Infinity II |
| Column Name: | Agilent ZORBAX RRHD Extend C18 (150 x 2.1mm, 1.8µm,80A,1200 bar) |
| Column Temperature: | 35C |
| Flow Gradient: | t=0 min: 100%/0% (%A/%B) @ 0.25 ml/min | t=2 min: 100%/0% (%A/%B) @ 0.25 ml/min | t=12 min: 1%/99% (%A/%B) @ 0.25 ml/min | t=18 min: 1%/99% (%A/%B) @ 0.25 ml/min | t=28 min: 100%/0% (%A/%B) @ 0.40 ml/min | t=29.9 min: 100%/0% (%A/%B) @ 0.40 ml/min | t=30 min: 100%/0% (%A/%B) @ 0.25 ml/min |
| Flow Rate: | 0.25 ml/min; 0.4 ml/min |
| Solvent A: | 97% water/3% methanol; 15 mM tributylamine; 10 mM acetic |
| Solvent B: | 100% methanol; 15 mM tributylamine; 10 mM acetic acid |
| Chromatography Type: | Reversed phase |
