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MB Sample ID: SA305845
| Local Sample ID: | 10 |
| Subject ID: | SU002936 |
| Subject Type: | Human |
| Subject Species: | Homo sapiens |
| Taxonomy ID: | 9606 |
| Gender: | Female |
Select appropriate tab below to view additional metadata details:
Combined analysis:
| Analysis ID | AN004614 | AN004615 | AN004616 |
|---|---|---|---|
| Analysis type | MS | MS | MS |
| Chromatography type | HILIC | HILIC | Reversed phase |
| Chromatography system | Waters Acquity I-Class | Waters Acquity I-Class | Waters Acquity I-Class |
| Column | Phenomenex Luna NH2 (150 x 2mm,3um) | Waters Atlantis HILIC (150 x 2.1 mm, 3um) | Prosphere HP C4 (150 x 3.0 mm, 3um) |
| MS Type | API | API | API |
| MS instrument type | QTRAP | QTRAP | QTRAP |
| MS instrument name | ABI Sciex API 4000 QTrap | ABI Sciex API 4000 QTrap | ABI Sciex API 4000 QTrap |
| Ion Mode | NEGATIVE | POSITIVE | POSITIVE |
| Units | Peak Area | Peak Area | Peak Area |
Chromatography:
| Chromatography ID: | CH003470 |
| Methods Filename: | La_Frano_Lab_Methods_Doc_VA_v9[2].pdf |
| Instrument Name: | Waters Acquity I-Class |
| Column Name: | Phenomenex Luna NH2 (150 x 2mm,3um) |
| Column Temperature: | 30 °C |
| Flow Gradient: | 0-10 min: 90%, 10-11 min: 5%, 11-13 min: 5%, 13-15: 90%, |
| Flow Rate: | 0.3 mL/min |
| Sample Injection: | 5µl |
| Solvent A: | 100% water; 20 mM ammonium acetate; 20 mM ammonium hydroxide |
| Solvent B: | 75% acetonitrile/25% methanol; 10 mM ammonium hydroxide |
| Randomization Order: | Excel generated |
| Chromatography Type: | HILIC |
| Chromatography ID: | CH003471 |
| Methods Filename: | La_Frano_Lab_Methods_Doc_VA_v9[2].pdf |
| Instrument Name: | Waters Acquity I-Class |
| Column Name: | Waters Atlantis HILIC (150 x 2.1 mm, 3um) |
| Column Temperature: | 30°C |
| Flow Gradient: | 0-1 min: 95%, 1-11 min: 95%, 11-13 min: 40%, 13-15 min: 95% |
| Flow Rate: | 0.25 mL/min |
| Sample Injection: | 5µl |
| Solvent A: | 100% water; 10 mM ammonium formate; 0.1% formic acid |
| Solvent B: | 100% acetonitrile; 0.1% formic acid |
| Randomization Order: | Excel generated |
| Chromatography Type: | HILIC |
| Chromatography ID: | CH003472 |
| Methods Filename: | La_Frano_Lab_Methods_Doc_VA_v9[2].pdf |
| Instrument Name: | Waters Acquity I-Class |
| Column Name: | Prosphere HP C4 (150 x 3.0 mm, 3um) |
| Column Temperature: | 30 °C |
| Flow Gradient: | 0-2 min: 20%, 2-3 min: 20%, 3-7 min: 80%, 7-10 min: 100%, 10-11 min: 100%, 11-15 min: 20% |
| Flow Rate: | 0.35 mL/min |
| Sample Injection: | 5µl |
| Solvent A: | 95% water/5% methanol; 0.1% acetic acid; 10 mM ammonium acetate |
| Solvent B: | 100% methanol; 0.1% acetic acid |
| Randomization Order: | Excel generated |
| Chromatography Type: | Reversed phase |
