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MB Sample ID: SA317691

Local Sample ID:d_AD_FA_37
Subject ID:SU003037
Subject Type:Human
Subject Species:Homo sapiens
Taxonomy ID:9606
Gender:Not applicable
Human Race:Pacific asian

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Combined analysis:

Analysis ID AN004794 AN004795
Analysis type MS MS
Chromatography type Reversed phase Reversed phase
Chromatography system Agilent 1290 Infinity Agilent 1290 Infinity
Column Agilent Pursuit 5 C18 (150 x 2.0 mm, 5um) Agilent Pursuit 5 C18 (150 x 2.0 mm, 5um)
MS Type ESI ESI
MS instrument type QTRAP QTRAP
MS instrument name ABI Sciex 5500 QTrap ABI Sciex 5500 QTrap
Ion Mode POSITIVE POSITIVE
Units pmol/mg pmol/mg

Chromatography:

Chromatography ID:CH003625
Chromatography Summary:Ceramides, sphingomyelines, sphinganine, sphingosine
Instrument Name:Agilent 1290 Infinity
Column Name:Agilent Pursuit 5 C18 (150 x 2.0 mm, 5um)
Column Temperature:35
Flow Gradient:50 % of B at 0 min, 50 % of B for 5 min, 50-70 % of B for 3 min, 70 % of B for 7 min, 70-90 % of B for 7 min, 90 % of B for 3 min, 90-50 % of B for 0.1 min, 50 % of B for 4.9 min
Flow Rate:200 uL/min
Solvent A:5 mM ammonium formate/MeOH/tetrahydrofuran (500/200/300, v/v/v)
Solvent B:5 mM ammonium formate/MeOH/ tetrahydrofuran (100/200/700, v/v/v)
Chromatography Type:Reversed phase
  
Chromatography ID:CH003626
Chromatography Summary:diacylglycerols
Instrument Name:Agilent 1290 Infinity
Column Name:Agilent Pursuit 5 C18 (150 x 2.0 mm, 5um)
Column Temperature:35
Flow Gradient:90 % of B for 0 min, 90 % of B for 6 min, 90 to 95 % of B for 0.6 min, 95 % of B for 3.4 min, 95 to 90 % of B for 0.1 min, and 90 % of B for 1.9 min
Flow Rate:200 uL/min
Solvent A:5 mM ammonium formate/MeOH/tetrahydrofuran (500/200/300, v/v/v)
Solvent B:5 mM ammonium formate/MeOH/ tetrahydrofuran (100/200/700, v/v/v)
Chromatography Type:Reversed phase
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