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MB Sample ID: SA328069

Local Sample ID:measured concentration(Data07-BQ-ZY20221130-600MRM-RZZ-Sample-23)
Subject ID:SU003141
Subject Type:Human
Subject Species:Homo sapiens
Taxonomy ID:9606

Select appropriate tab below to view additional metadata details:

Combined analysis:

Analysis ID AN004962 AN004963
Analysis type MS MS
Chromatography type Normal phase Reversed phase
Chromatography system Waters Acquity H-Class Waters Acquity H-Class
Column Waters ACQUITY UPLC BEH HILIC (150 x 2.1mm,1.7um) Waters ACQUITY UPLC BEH HILIC (150 x 2.1mm,1.7um)
MS Type EI ESI
MS instrument type Triple quadrupole Triple quadrupole
MS instrument name ABI Sciex 6500 QTrap ABI Sciex 6500 QTrap
Ion Mode POSITIVE NEGATIVE
Units m/z m/z

Chromatography:

Chromatography ID:CH003745
Instrument Name:Waters Acquity H-Class
Column Name:Waters ACQUITY UPLC BEH HILIC (150 x 2.1mm,1.7um)
Column Temperature:475°C
Flow Gradient:85% (vol/vol) B: 0.0 min, 85% B to 30% B:3.0 min, 30% B to 2% B:12.0 min, 2% B:15.0 min, 2% B to 85% B: 16.0 min, 85%: 23.0 min
Flow Rate:Approximately 350–400 µl/min (back pressure should not exceed ~3,000 p.s.i. at 2% (vol/vol) B)
Solvent A:ddH2O:Acetonitrile=8:2, 10 mmol/LAmmonium acetate
Solvent B:Acetonitrile:ddH2O=9:1, 10 mmol/LAmmonium acetate
Chromatography Type:Normal phase
  
Chromatography ID:CH003746
Instrument Name:Waters Acquity H-Class
Column Name:Waters ACQUITY UPLC BEH HILIC (150 x 2.1mm,1.7um)
Column Temperature:475°C
Flow Gradient:85% (vol/vol) B: 0.0 min, 85% B to 30% B:3.0 min, 30% B to 2% B:12.0 min, 2% B:15.0 min, 2% B to 85% B: 16.0 min, 85%: 23.0 min
Flow Rate:Approximately 350–400 µl/min (back pressure should not exceed ~3,000 p.s.i. at 2% (vol/vol) B)
Solvent A:ddH2O:Acetonitrile=8:2, 10 mmol/LAmmonium acetate
Solvent B:Acetonitrile:ddH2O=9:1, 10 mmol/LAmmonium acetate
Chromatography Type:Reversed phase
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