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MB Sample ID: SA333220

Local Sample ID:P2
Subject ID:SU003207
Subject Type:Human
Subject Species:Homo sapiens
Taxonomy ID:9606
Gender:Male and female

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Combined analysis:

Analysis ID AN005060 AN005061
Analysis type MS MS
Chromatography type CE CE
Chromatography system Agilent CE-TOFMS system Agilent CE-TOFMS system
Column Capillary: Fused silica capillary i.d. 50 μm × 80 cm Capillary: Fused silica capillary i.d. 50 μm × 80 cm
MS Type ESI ESI
MS instrument type Other Other
MS instrument name Agilent CE-TOFMS system Agilent CE-TOFMS system
Ion Mode UNSPECIFIED UNSPECIFIED
Units Relative peak area Relative peak area

Chromatography:

Chromatography ID:CH003821
Chromatography Summary:The compounds were measured in the Cation and Anion modes of CE-TOFMS based metabolome analysis.
Instrument Name:Agilent CE-TOFMS system
Column Name:Capillary: Fused silica capillary i.d. 50 μm × 80 cm
Column Temperature:20 ℃
Flow Gradient:10 μL/min
Flow Rate:10 μL/min
Sample Injection:Pressure injection 50 mbar, 10 sec
Solvent A:50% acetonitrile/50% water; internal standards (20 μM)
Solvent B:-
Capillary Voltage:4,000 V (Cation Mode); 3,500 V (Anion Mode)
Running Buffer:Cation Buffer Solution (p/n : H3301-1001); Anion Buffer Solution (p/n : I3302-1023)
Running Voltage:30 kV
Sheath Liquid:HMT Sheath Liquid (p/n : H3301-1020)
Washing Buffer:Cation Buffer Solution (p/n : H3301-1001); Anion Buffer Solution (p/n : I3302-1023)
Chromatography Type:CE
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