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MB Sample ID: SA082719

Local Sample ID:NEG S-2
Subject ID:SU001258
Subject Type:Human
Subject Species:Homo sapiens
Taxonomy ID:9606

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Combined analysis:

Analysis ID AN001983
Analysis type MS
Chromatography type HILIC
Chromatography system Agilent 1290
Column
MS Type ESI
MS instrument type QTOF
MS instrument name ABI Sciex 5600 TripleTOF
Ion Mode NEGATIVE
Units intensity

MS:

MS ID:MS001836
Analysis ID:AN001983
Instrument Name:ABI Sciex 5600 TripleTOF
Instrument Type:QTOF
MS Type:ESI
MS Comments:The ESI source conditions after HILIC chromatographic separation are as follows: Ion Source Gas1 (Gas1): 60, Ion Source Gas 2 (Gas 2): 60, Curtain gas (CUR): 30, source temperature: 600 ° C, Ion Sapary Voltage Floating (ISVF) ± 5500 V (Positive and negative modes); TOF MS scan m/z range: 60-1000 Da, product ion scan m/z range: 25-1000 Da, TOF MS scan accumulation time 0.20 s/spectra, product ion scan accumulation time 0.05 s/spectra; secondary mass spectrometry is obtained using information dependent acquisition (IDA), and uses high sensitivity mode, Declustering potential (DP): ±60 V (both positive and negative modes), Collision Energy: 35±15 eV, IDA settings are as follows Exclude isotopes within 4 Da, Candidate ions to monitor per cycle: 6
Ion Mode:NEGATIVE
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