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MB Sample ID: SA138153
| Local Sample ID: | 2-A2-PS |
| Subject ID: | SU001709 |
| Subject Type: | Mammal |
| Subject Species: | Rattus norvegicus |
| Taxonomy ID: | 10116 |
| Genotype Strain: | Sprague-Dawley |
| Age Or Age Range: | 6 weeks-age |
| Weight Or Weight Range: | 200 ± 10 |
| Gender: | Male |
| Animal Animal Supplier: | Vital River Laboratories Co., Ltd (Beijng, China) |
| Animal Housing: | 25 ± 2℃, 50±5% relative humidity |
| Animal Light Cycle: | 12 h light/12 h dark photoperiod |
Select appropriate tab below to view additional metadata details:
Combined analysis:
| Analysis ID | AN002667 | AN002668 |
|---|---|---|
| Analysis type | MS | MS |
| Chromatography type | Reversed phase | Reversed phase |
| Chromatography system | Agilent 1100 | Thermo Accela 1250 |
| Column | Peeke C8 SR (150×3.0mm, 3μm) | Waters Xterra MS C8 (100 x 2.1mm,3.5um) |
| MS Type | ESI | ESI |
| MS instrument type | Triple quadrupole | LTQ-FT |
| MS instrument name | Agilent 6410 QQQ | Thermo LTQ-FT |
| Ion Mode | POSITIVE | UNSPECIFIED |
| Units | pmol/ml(PL) & pmol/mg(HL) | pmol/ml(PS) & pmol/mg(HS) |
MS:
| MS ID: | MS002466 |
| Analysis ID: | AN002667 |
| Instrument Name: | Agilent 6410 QQQ |
| Instrument Type: | Triple quadrupole |
| MS Type: | ESI |
| MS Comments: | The parameters for electrospray ionization tandem MS in positive ion mode were as follows: gas temperature, 350 ℃; gas flow rate, 10 l/min; nebulizer, 30 psi; and capillary voltage, 4000V. Multiple reaction monitoring was performed using the characteristic precursor-to-product ion transitions, optimized fragmentor voltages, and collision energies. |
| Ion Mode: | POSITIVE |
| MS ID: | MS002467 |
| Analysis ID: | AN002668 |
| Instrument Name: | Thermo LTQ-FT |
| Instrument Type: | LTQ-FT |
| MS Type: | ESI |
| MS Comments: | The LTQ-FT was run in full-scan mode at 100000 resolution from m/z50–1200 with MS parameters: sheath gas flow rate, 50 arb; aux gas flow rate, 20 arb; sweep gas flow rate, 3 arb; capillary temperature, 275 ℃ in both positive and negative mode. And spray voltage, 4.5kV; capillary voltage, 35.0V; tube lens, 120V were used for the positive mode. Spray voltage, -4.0kV; capillary voltage, -35.0V; tube lens, -120V were used for the negative mode. |
| Ion Mode: | UNSPECIFIED |
