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MB Sample ID: SA249146

Local Sample ID:sample_0119
Subject ID:SU002588
Subject Type:Human
Subject Species:Homo sapiens
Taxonomy ID:9606
Gender:Male and female

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Combined analysis:

Analysis ID AN004092
Analysis type MS
Chromatography type Reversed phase
Chromatography system Agilent 7890B
Column Waters ACQUITY UPLC BEH C18 (100 x 2.1mm,1.7um)
MS Type EI
MS instrument type QTOF
MS instrument name Agilent 7200 QTOF
Ion Mode NEGATIVE
Units Raw output from software

MS:

MS ID:MS003839
Analysis ID:AN004092
Instrument Name:Agilent 7200 QTOF
Instrument Type:QTOF
MS Type:EI
MS Comments:MassHunter B.06.01 software (Agilent Technologies, Santa Clara, CA, USA) was used for all data acquisition. Identification of compounds was done by in-house spectral library using MS (and retention time), MS/MS information. Quantitation was based on a matrix matched calibration curve spiked with native compounds. The calibration curve consisted of concentrations ranging from 0 – 1600 ng mL -1 for BAs. The RSD for the BAs was on average 17.8 % for the QC samples and 19.4 % for the NIST samples.
Ion Mode:NEGATIVE
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