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MB Sample ID: SA250527

Local Sample ID:GC-TBI-33
Subject ID:SU002597
Subject Type:Human
Subject Species:Homo sapiens
Taxonomy ID:9606
Gender:Male and female

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Combined analysis:

Analysis ID AN004107 AN004108 AN004109
Analysis type MS MS MS
Chromatography type GC Reversed phase Reversed phase
Chromatography system Agilent 7890A Thermo TSQ Vantage HPLC-MS/MS Thermo TSQ Vantage HPLC-MS/MS
Column Agilent DB-5ms (30m x 0.25mm, 0.25um) Waters ACQUITY UPLC BEH C8 (100 x 2.1mm,1.7um) Waters ACQUITY UPLC HSS T3 (100 x 2.1mm,1.8um)
MS Type EI ESI ESI
MS instrument type Single quadrupole Triple quadrupole Triple quadrupole
MS instrument name Agilent 5977 Thermo TSQ Vantage Thermo TSQ Vantage
Ion Mode UNSPECIFIED POSITIVE NEGATIVE
Units pmoles/l pmoles/l pmoles/l

MS:

MS ID:MS003854
Analysis ID:AN004107
Instrument Name:Agilent 5977
Instrument Type:Single quadrupole
MS Type:EI
MS Comments:Detector voltage was set at 1.25kV, EI electron impact 70eV. The solvent cutting time was set at 3.5 min.
Ion Mode:UNSPECIFIED
  
MS ID:MS003855
Analysis ID:AN004108
Instrument Name:Thermo TSQ Vantage
Instrument Type:Triple quadrupole
MS Type:ESI
MS Comments:350℃capillary temperature, 300℃ vaporize temperature, 40 arbitrary units sheath gas flow rate, 20 arbitrary units auxiliary gas flow rate, 3.0 kV capillary voltage
Ion Mode:POSITIVE
  
MS ID:MS003856
Analysis ID:AN004109
Instrument Name:Thermo TSQ Vantage
Instrument Type:Triple quadrupole
MS Type:ESI
MS Comments:350℃capillary temperature, 300℃ vaporize temperature, 40 arbitrary units sheath gas flow rate, 20 arbitrary units auxiliary gas flow rate, -2.5 kV capillary voltage
Ion Mode:NEGATIVE
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