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MB Sample ID: SA258057

Local Sample ID:2021-10-01_035_F3_E1
Subject ID:SU002668
Subject Type:Human
Subject Species:Homo sapiens
Taxonomy ID:9606
Gender:Male

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Combined analysis:

Analysis ID AN004228
Analysis type MS
Chromatography type Reversed phase
Chromatography system Agilent 6530 qTOF
Column Agilent Zorbax Extend C18 (150 x 2.1mm, 1.8um) with matched guard column
MS Type ESI
MS instrument type QTOF
MS instrument name Agilent 6530 QTOF
Ion Mode NEGATIVE
Units EicCoreArea/Peak Area

MS:

MS ID:MS003975
Analysis ID:AN004228
Instrument Name:Agilent 6530 QTOF
Instrument Type:QTOF
MS Type:ESI
MS Comments:MS acquisition was performed in negative ion mode, scan rate 2 spectra/sec, mass range 50-1200 m/z. Source parameters were: drying gas temperature 250°C, drying gas flow rate 13 L/min, nebulizer pressure 35 psig, sheath gas temp 325°C and flow 12 l/min, capillary voltage 3500V, internal reference mass correction enabled. Data analysis was performed using Agilent Profinder 10.0 software in batch isotopologue extraction mode with automated natural isotope abundance correction enabled. Compound identification was performed by matching accurate mass and retention time to those of authentic standards analyzed using the same method.
Ion Mode:NEGATIVE
Capillary Voltage:3500V
Dry Gas Flow:13L/min
Dry Gas Temp:250 C
Fragment Voltage:150V
Nebulizer:35 psig
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